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1. Synthesis of fused and bridged bicyclic diazenium salts by intramolecular cycloaddition.

Author

Javed MI, Wyman JM, and Brewer M

Subjects
Alkenes chemistry, Azo Compounds chemistry, Bridged Bicyclo Compounds chemistry, Combinatorial Chemistry Techniques, Cyclization, Models, Molecular, Molecular Structure, Salts, Alkenes chemical synthesis, Azo Compounds chemical synthesis, Bridged Bicyclo Compounds chemical synthesis
Abstract

Bicyclic diazenium salts were efficiently prepared by a Lewis acid mediated intramolecular cycloaddition. Terminal olefins provided mixtures of fused and bridged bicyclic diazenium salts. The alpha-chloroazo cycloaddition precursors were conveniently prepared from the corresponding phenyl hydrazones by treatment with chlorodimethylsulfonium chloride.

Published
2009
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