1. A Novel Approach for Accelerated Fabrication of Calcium Hydroxyapatite Thin Films
- Author
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Pranas Usinskas, Justinas Čeponkus, Gediminas Niaura, Aivaras Kareiva, and Živilė Stankevičiūtė
- Subjects
lcsh:TN1-997 ,Materials science ,thin film ,Scanning electron microscope ,hydroxyapatite ,Polyvinyl alcohol ,Dip-coating ,Contact angle ,chemistry.chemical_compound ,sol–gel ,chemistry ,Chemical engineering ,Triethanolamine ,medicine ,General Materials Science ,Fourier transform infrared spectroscopy ,Thin film ,dip–coating ,lcsh:Mining engineering. Metallurgy ,medicine.drug ,Sol-gel - Abstract
In this study we demonstrate, that sol–gel route is suitable to quicker obtain calcium hydroxyapatite (Ca10(PO4)6(OH)2, CHAp) coatings on crystalline Si substrate by modified dip-coating technique. The substrate was dip-coated by precursor and dried for 10 minutes at 200 °C with following cooling using the heating block for 110 min and annealing at 650 °C. Ethylendiamintetraacetic acid and 1,2-ethandiol, and triethanolamine and polyvinyl alcohol were used as complexing agents and as gel network forming agents, respectively. The obtained coatings were characterized by X-ray diffraction (XRD) analysis, scanning electron microscopy (SEM), FTIR spectroscopy and contact angle measurements (CAM).
- Published
- 2019