Search

The microstructural evolution during solution treatment at 500 °C of a cast AlSi12Cu4Ni2 piston alloy is evaluated by two dimensional and three dimensional imaging methods aiming at identifying the microstructural features affecting the processes of damage formation and accumulation under tensile deformation. Highly interconnected networks of aluminides and Si undergo a local loss of connecting branches within these networks owing to the partial dissolution of Cu-rich aluminides and a slight Si spheroidisation. The damage by tensile deformation is studied using synchrotron tomography during in situ tensile tests. In both studied heat treatment conditions (0 h and 4 h solution treated) damage initiates in the form of micro-cracks in clusters of primary Si particles and debonding at the interface between Si and the matrix. These micro-cracks grow through intermetallic phases in the last stages of deformation. Final failure occurs by coalescence of these cracks mainly through the rigid phases. The loss of connectedness of the Si-intermetallics network during solution treatment allows the alloy to accommodate more damage and plastic strain resulting in an increase of ductility with respect to the as cast condition. [ABSTRACT FROM AUTHOR]

The 3D microstructure and its effect on damage formation and accumulation during tensile deformation at 300 °C for cast, near eutectic AlSi12Cu4Ni2Mg and AlSi12Cu4Ni3Mg alloys has been investigated using in-situ synchrotron micro-tomography, complemented by conventional 2D characterization methods. An increase of Ni from 2 to 3 wt.% leads to a higher local connectivity, quantified by the Euler number χ, at constant global interconnectivity of rigid 3D networks formed by primary and eutectic Si and intermetallics owing to the formation of the plate-like Al-Ni-Cu-rich δ-phase. Damage initiates as micro-cracks through primary Si particles agglomerated in clusters and as voids at matrix/rigid phase interfaces. Coalescence of voids leads to final fracture with the main crack propagating along damaged rigid particles as well as through the matrix. The lower local connectivity of the rigid 3D network in the alloy with 2 wt.% Ni permits localized plastification of the matrix and helps accommodating more damage resulting in an increase of ductility with respect to AlSi12Cu4Ni3Mg. A simple load partition approach that considers the evolution of local connectivity of rigid networks as a function of strain is proposed based on in-situ experimental data. [ABSTRACT FROM AUTHOR]

Two Ti–6Al–6V–2Sn alloys, with globular and lamellar microstructures, are deformed at 750 °C during tensile and compression tests. The lamellar microstructure shows softening and higher peak stress values than the globular microstructure as a consequence of the Hall–Petch effect. In-situ high energy synchrotron diffraction experiments allow characterization of the load partition between α- and β-phases, plastic deformation mechanisms and texture evolution. The α-phase deforms mainly by rotation while the β-phase deforms by misorientation formation, acting merely as load transfer agent. The Taylor factor evolution of the α-phase and the annihilation of dislocations are analyzed qualitatively and quantitatively. The Taylor factor is connected to both the softening observed in the alloy with the lamellar microstructure and the texture development. [ABSTRACT FROM AUTHOR]