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Despite numerous studies on nanofluids in microchannel heat sinks (MCHSs), they are not yet commercialized due to long-term stability issues and high maintenance costs. Therefore, this study explores the impact of nanofluids and nanoparticle clustering on single-phase convective heat transfer inside microchannels under laminar conditions. Water and commercially available water-based nanosuspensions, including Al 2 O 3 -water (30–60 nm), TiO 2 -water (5–30 nm), and polystyrene-water (50 nm), are circulated through silicon MCHS having rectangular channels integrated into a closed flow loop. To assess the in situ and real-time nanoparticle clustering during heat transfer experiments, Light Extinction Spectroscopy (LES) is applied as a non-intrusive measurement technique on nanofluids without any fluid sampling. Our findings reveal the appearance of nanofluid discoloration with no measurable increase in heat transfer coefficient. This unexpected change is attributed to the interplay of abrasion, erosion, and corrosion phenomena, likely triggered by the clustering of nanoparticles within the silicon microchannels—a novel insight into the complex dynamics of nanofluid behavior (an increase in the De Brouckere mean diameter from 11 nm to 107.3 nm over a 2.5 h period for TiO 2 nanoparticles). The resulting material loss could not be mitigated by altering the nanoparticle material, which may impede heat transfer enhancement under tested conditions. [ABSTRACT FROM AUTHOR]

For more than 20 years, the use of nanofluids to enhance heat transfer in microchannel heat sinks (MCHSs) has been the subject of a large number of scientific articles. Despite the great potentialities reported in several works, the presence of controversial results and the lack of understanding of heat transfer enhancement mechanisms prevent further advancement in the use of nanofluids as coolants. This article reviews the scientific literature focused on several aspects of nanofluids that have a role in the heat transfer enhancement within the MCHSs: nanofluid stability, thermal conductivity, and particle clustering, as well as the particle–surface interactions, i.e., abrasion, erosion, and corrosion. We also include the most relevant works on the convective heat transfer and MCHSs operated with nanofluids in our review. [ABSTRACT FROM AUTHOR]