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Suspensions containing 8 and 10 wt% polyacrylonitrile (PAN) and 1, 2, 3, 5, 7 and 10 wt% graphene oxide (GO) were prepared using a special mixing routine and fibres were generated from these mixtures by pressurised gyration. The combination of pressure and gyration speed was effective in controlling the fibre morphology and fibre diameter which ranged from 1 to 20 μm. Fibres were pyrolysed to remove the polymer and only the 10 wt% PAN fibres survived. The microstructure of the pre- and post-pyrolysis products were characterised by scanning electron microscopy, both with and without focussed ion beam etching, Fourier-transformed infrared and Raman spectroscopies. Pyrolysed fibre electrical conductivities were measured and only those containing 1 and 2 wt% GO were conductive.

A simple and effective process combining pressure and gyration has been developed and used to jet-out composite fibres containing graphene nanoplatelets. Thermoplastic polyurethane and phenolic resin polymers were used as matrices. Processing parameters such as rotation speed, pressure and polymer concentration had a marked influence on the composite fibre diameter. Focussed ion beam milling and etching verified the effective incorporation of the graphene nanoplatelets into the composite fibres. Morphological, rheological, physico-chemical and thermal properties of the composite fibres were evaluated to identify possible applications for them.

Flux Core Arc Welding (FCAW) is an arc welding process that using continuous flux-cored filler wire. The flux is used as a welding protection from the atmosphere environment. This project is study about the effect of FCAW process on different parameters by using robotic welding with the variables in welding current, speed and arc voltage. The effects are on welding penetration, microstructural and hardness measurement. Mild steel with 6 mm thickness is used in this study as a base metal. For all experiments, the welding currents were chosen are 90A, 150A and 210A and the arc voltage is 22 V, 26 V and 30 V respectively. 20, 40 and 60 cm/min were chosen for the welding speed. The effect will studied and measured on the penetration, microstructure and hardness for all specimens after FCAW process. From the study, the result shown increasing welding current will influenced the value depth of penetration increased. Other than that, the factors that can influence the value of depth of penetration are arc voltage and welding speed.

Gas Metal Arc Welding (GMAW) process is leading in the development in arc welding process which is higher productivity and good in quality. In this study, the effects of different parameters on welding penetration, microstructural and hardness measurement in mild steel that having the 6 mm thickness of base metal by using the robotic gas metal arc welding are investigated. The variables that choose in this study are arc voltage, welding current and welding speed. The arc voltage and welding current were chosen as 22, 26 and 30 V and 90, 150 and 210 A respectively. The welding speed was chosen as 20, 40 and 60 cm/min. The penetration, microstructure and hardness were measured for each specimen after the welding process and the effect of it was studied. As a result, it obvious that increasing the parameters value of welding current increased the value of depth of penetration. Other than that, arc voltage and welding speed is another factor that influenced the value of depth of penetration. The microstructure shown the different grain boundaries of each parameters that affected of the welding parameters.