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High sensitivity pressure measurements are reported using two intrinsic optical fibre methods: Fibre Bragg Gratings and Fibre Segment Interferometry. The optical fibres sensors are surface mounted onto a composite membrane and respective sensitivities of 79.2 µɛ/kPa and 65.8 µɛ/kPa have been achieved at resolutions of 0.79 µɛ and 0.04 µɛ.

Multiplexed optical fibre sensors were embedded into a carbon-fibre-reinforced-preform during the industrial production of a full-sized, one-piece tail cone assembly for a regional jet aircraft. Optical fibre Fresnel sensors monitored both the infusion of the resin, via measurement of the refractive index-dependent attenuation in the reflected light signal, and the degree of cure of the resin, via measurement of the chemical cure reaction-dependent change in refractive index. The resin cure was also monitored by optical fibre Bragg gratings (FBGs) fabricated in high linearly birefringent optical fibre, which measured through-thickness strain development, while FBGs in standard single mode optical fibre measured longitudinal strain development. The magnitudes and profiles of the transverse and longitudinal strains developed during the curing process were consistent across different locations on the tail cone. Typical transverse and longitudinal strains, related to cure reaction-induced shrinkage, were −1500 ± 17 μepsilon and −500 ± 5 μepsilon, respectively. Post-production, the same embedded FBG sensors were used subsequently to monitor structural strains when the tail cone was subjected to vacuum pressure loading. The longitudinal strains measured using the embedded FBG sensors were generally in good agreement with the longitudinal strains measured by the surface-bonded resistance foil strain gauge (RFSG) sensors, both qualitatively and quantitatively. The in-plane transverse and circumferential strains, oriented collinearly, were measured by the embedded FBGs and appropriately oriented surface-bonded RFSG sensors, respectively, and were, qualitatively, in good agreement

Long period gratings (LPGs) as a sensing platform have the potential for multi-parameter measurement through the utilization of 2nd order coupling resonance bands. Although the current literature has produced LPGs with 2nd order resonance bands, the fabrication parameters required to generate these features have not been elucidated. Here, using UV irradiation via the point-by-point method, it is shown that by varying the duty cycle it is possible to fabricate LPGs that exhibit 2nd, 3rd, and 4th order coupling resonance bands. Fabrication of LPGs with a 25% or 75% duty cycle produces distinct 2nd order resonance bands, which are not observed when a 50% duty cycle is adopted.

This paper reports on the development of a new, non-contact, cost-effective and widely-applicable optical sensor for the measurement of the three degrees of translational freedom of a robotic end-effector. The workpiece positioning sensor (wPOS) tracks the relative position between the workpiece and end-effector in real-time, using laser speckle correlation for the measurement of in-plane position and Range-Resolved Interferometry for out-of-plane positioning. The sensing principles of the techniques and the development of the instrument are discussed along with example results for applications in robotic additive manufacturing for tool speed and layer height measurements.

We describe a combination of Tunable Diode Laser Spectroscopy and Range Resolved Interferometry that enables multipoint gas detection using a single laser and photodetector. Tunable Diode Laser Spectroscopy (TDLS) permits gas detection via the measurement of its optical absorption while a diode laser is tuned through an absorption line. Range Resolved Interferometry (RRI) employs a signal processing technique previously used for position sensing and vibrometry. The principle of operation is the sinusoidal modulation of the emission wavelength of a laser which is coupled into a network of interferometers. The detected signal is demodulated to give the signal amplitude within each interferometer. Signals from different interferometers can be distinguished based on the optical path length difference, enabling continuous interrogation of multiple measurement channels simultaneously. In this work, a number of gas cells are combined with optical fibre to create systems of nested interferometers, including a combination of gas cells and a common local oscillator. The laser wavelength was modulated with a combination of fast sinusoidal (49kHz) and slow (2Hz) ramp wave forms, the ramp sweeping the central wavelength of the laser through the methane absorption line at 1653nm. The intensity signal for each cell was extracted using the RRI technique in order to measure the methane concentration within each cell A Mach-Zehnder topology allows the measurement of methane at concentrations as low as 200ppm. We discuss the potential performance of other topologies that are more suitable for field deployment.

A dual beam optical coherence tomography (OCT) instrument has been developed for flow measurement that offers advantages over microscope derived imaging techniques. It requires only a single optical access port, allows simultaneous imaging of the microfluidic channel, does not require fluorescent seed particles, and can provide a millimetre-deep depth-section velocity profile (as opposed to horizontal-section). The dual beam instrument performs rapid re-sampling of particle positions, allowing measurement of faster flows. In this paper, we develop the methods and processes necessary to make 2D quantitative measurements of the flow-velocity using dual beam OCT and present exemplar results in a microfluidic chip. A 2D reference measurement of the Poiseuille flow in a microfluidic channel is presented over a spanwise depth range of 700 m and streamwise length of 1600 m with a spatial resolution of 10 m , at velocities up to 50 m m / s . A measurement of a more complex flow field is also demonstrated in a sloped microfluidic section.

The process of fabricating tapered long period gratings (TLPGs) using a CO2 laser is described. The objective of this work is to optimize the CO2 laser based fabrication of TLPGs so that their transmission spectra are comparable with those made using the arc-discharge technique, which typically exhibits transmission losses below 2 dB. The losses currently observed with CO2 laser fabricated TLPGs are typically greater than 10 dB over the spectral waveband 650-1100 nm. In this work, the reduction in transmission loss was achieved by optimizing the micro-taper geometry and the duty-cycle of the device. TLPGs with a period of 378 μm were fabricated. The 6-period TLPGs exhibited a pass-band transmission loss of 0.6 dB, resonance band extinction values of 3 dB and had a physical length of 2.27 mm. The refractive index sensitivity of a 6 period TPLG was measured and found to be 372 nm/ RI.

This paper compares two fibre optic sensing techniques for vibration characterisation: (a) optical fibre Bragg grating (FBG) strain gauges and (b) a novel direct fibre optic shape sensing (DFOSS) approach based on differential interferometric strain measurements between multiple fibres within the same fibre arrangement. Operational mode shapes and frequency measurements of an Airbus Helicopters H135 bearingless main rotor blade (5.1 m radius) were acquired during a series of ground vibration tests undertaken in a controlled laboratory environment. Data recorded by the fibre optic instrumentation systems were validated using commercially available accelerometers and compared against a baseline finite element model. Both fibre optic sensing systems proved capable of identifying the natural frequencies of the blade in the frequency range of interest (0–100 Hz). The data from the FBG sensors exhibited a dependency on their position relative to the neutral axes of the blade, which meant that full characterisation of the flapping and lagging modes required careful consideration of sensor location in the chordwise direction. The DFOSS system was able to identify all structural dynamics, despite being located on the neutral axis in the lagging direction, due to its sensitivity to angle changes, rather than strain, and its biaxial measurement capability. The DFOSS system also allowed the operational mode shapes of the blade to be determined directly, without the requirement for strain transfer from the blade to the sensor and without the requirement for a model of the underlying structure. The accuracy of obtained natural frequencies and operational mode shapes is assessed, demonstrating the potential of the use of both fibre optic sensing systems for determining blade structural dynamics.

The development of an optical fiber based pressure sensor, created using a Fiber Bragg Grating (FBG) and a glass fiber reinforced polymer membrane for use in aerodynamic applications, is reported. The FBG was co-bonded on the surface of the membrane to measure the strain induced by the deflection of the diaphragm with applied pressure. The sensor exhibited high sensitivities of 56.7 pm/kPa, with a minimum resolution of 21 Pa over a 0 to 35 kPa range. The outputs from a mathematical model, Finite Element analysis and the experimental results are compared and discussed.

The use of optical fibre Bragg gratings (FBGs) and direct fibre optic shape sensing (DFOSS) in the ground vibration testing of a full size helicopter rotor blade has been evaluated, with the performance benchmarked against measurements made using accelerometers. An array of FBGs was used to monitor the amplitudes of the mode frequencies at specific locations along the blade and DFOSS was used to measure directly the shape of the blade and to characterise its modal frequencies. While it was possible to measure modal frequencies using both approaches, DFOSS proved capable of detecting modal frequencies using a single sensor array located along the longitudinal axis of the blade.

Confocal scanning combined with low-coherence interferometry is used to provide remote refractive index and thickness measurements of transparent materials. The influence of lens aberrations in the confocal measurement is assessed through ray-trace modeling of the axial point-spread functions generated using optical configurations comprised of paired aspherics and paired achromats. Off-axis parabolic mirrors are suggested as an alternative to lenses and are shown to exhibit much more symmetric profiles provided the system numerical aperture is not too high. The modeled results compare favorably with experimental data generated using an optical instrument comprised of a broadband source and line-scan spectrometer. Refractive index and thickness measurements are made with each configuration with most mirror pairings offering better than twice the repeatability and accuracy of either lens pairing.

Many applications of precision interferometry suffer from uncertainties in knowing the values of the air refractive index or the laser wavelength and often require the use of complex setups or costly components to mitigate these effects. In this work, using range-resolved interferometric measurements, we show how differential measurements along a single optical beam can be used to perform displacement measurements with drastically reduced systematic errors. In a proof-ofprinciple experiment, a semi-transparent target mounted on a moving stage is placed centrally between a window and a mirror, forming two air paths around the target that are arranged to be of nominally equal length. The evaluation of the interferometric phase signals at multiple locations along the measurement beam then allows the simultaneous measurement of changes in the length of the two air paths on either side of the target. The difference of the air path length changes yields the desired target displacement measurement, while influences that are common to both air paths such as air refractive index changes or laser wavelength drift are strongly suppressed.

In this work, using our range-resolved interferometry (RRI) signal processing technique, we present a novel approach to multidimensional displacement measurements using only a single optical access port and very simple optical setup. By utilising surface reflections from a stage-mounted moving beamsplitter and two orthogonal stationary reference mirrors, two interferometers for the two Cartesian measurement directions are formed. With RRI, the interferometric phase signals of both interferometers can be independently demodulated, allowing simultaneous measurements of displacement in both dimensions using a single continuous-wave laser diode source and a single photodetector. In this paper, the capabilities of this approach are demonstrated using a proof-of-concept experiment with a multidimensional Piezoelectric stage performing a variety of stage movements. Measurements of displacements over a nominal stage working range of ±50μm are presented, demonstrating independent, simultaneous displacement measurements of two dimensions. The presented measurements show nanometer-level displacement resolutions with typical noise densities of 0.02 nm/√Hz over a 21 kHz bandwidth. It is thought that this approach could offer an interesting alternative to existing interferometric techniques for multi-dimensional metrology, benefiting from both simplicity and cost-effectiveness whilst maintaining the advantages that make optical techniques attractive to scientific and industrial applications.

Low-coherence interferometry is combined with confocal scanning to provide remote refractive index and thickness measurements of transparent materials. The influence of lens aberrations in the confocal measurement is assessed through investigation of the axial point-spread functions (APSFs) generated using optical configurations comprised of paired aspherics and paired achromats. Off-axis parabolic mirrors are suggested as an alternative to lenses and are shown to exhibit much more symmetric APSFs provided the system numerical aperture is not too high. Refractive index and thickness measurements are made with each configuration with most mirror pairings offering better than twice the repeatability and accuracy of either lens pairing.

This work describes a novel system to control the stability of a 1583 nm telecommunications laser diode via measurement of junction voltage. This electronic technique dispenses with the optical components used in conventional wavelength locking schemes and shifts wavelength control to system level electronic instrumentation. The approach employs real-time measurement of diode series resistance (Rs), which is used to compensate the measured forward voltage (Vf) and recover the junction voltage (Vj) of the laser. Control of Vj provides wavelength control without introducing a significant error when the package temperature varies. This was implemented by measuring Rs as the dynamic resistance, δV/δI, by modulating the injection current. Recent work has reduced the modulation amplitude and noise in the electronics. Using a frequency deviation of 1 GHz, we achieved a centre wavelength variation of ± 2 pm over a package temperature variation of 20-55 °C. This gives a wavelength/ temperature coefficient of 0.03 pm/ °C, which is an improvement on 0.34 pm/ °C, as typically achieved for optical locking systems. The system has been further developed using board-level components within a compact demonstrator unit. Work is on-going to further enhance this performance over a package temperature variation of 0-70 °C.

A pressure sensor specified for aerodynamic applications and based on optical fibre strain sensors mounted on a circular glass fibre reinforced polymer membrane is presented. The use of two fibre optic strain sensing technologies is explored, the novel intrinsic fibre segment interferometry (FSI) approach and fibre Bragg gratings (FBGs), with the use of FSI shown to offer a pressure resolution that is 15 times larger than that achieved using an FBG. A number of design and fabrication issues are considered, including the position of the fibres relative to the neutral axis of the membrane and the influence of the membrane support structure on the thermal and pressure sensitivities of the sensor, with particular regards to pressure and temperature discrimination.

When used as samples cells for optical absorbance measurements, integrating spheres offer increased pathlengths compared to single pass cells combined with tolerance to misalignment. This makes them attractive during alignment of optical instruments and in challenging environments subject to vibration. However, integrating spheres can suffer problems when used in sensitive and / or accurate absorbance measurement. We present our work to date to address these issues in high resolution laser spectroscopy. Firstly, optical interference effects include both random laser speckle and structured interference fringes created by optical feedback to the laser. Secondly, the sphere’s optical pathlength is a combination of multiple paths that take an exponential pathlength distribution. At low values of absorbance, the measured signal is linear with concentration, but at higher absorbances signals follow a nonlinear but predictable function of absorbance. Thirdly, our most recent work concerns calibration of the optical pathlength, which is a sensitive function of its internal reflectivity. In-situ calibration is needed if the sphere is to be used in dirty environments or with condensing samples. Measurements from multiple independent sources and / or detectors are combined to provide compensation from fouling of the sphere walls and windows. Results are presented for an integrating sphere used in the measurement of methane. The emission from a tunable DFB laser at 1651nm was tuned across the gas absorption line to measure its concentration. Reduced sphere reflectivity was simulated by applying small areas of black tape on the inner surface. Finally, we give an example of one application where our results are being put into practice: use of an integrating sphere with a tunable laser at 3.3μm to measure atmospheric methane, installed on a two seater light aircraft.

Measurement of the refractive index and thickness of transparent plates is demonstrated using combined low-coherence interferometry and confocal scanning. The low-coherence measurement provides a quantity related to the group index and the confocal scan provides a parameter related to the phase index. Calculation of both the phase and group indices also requires a measurement of the confocal parameter at multiple wavelengths. This is achieved using a broadband source and a line-scan spectrometer to interrogate different regions of the spectrum. Measurements are made on a range of transparent optical materials with the mean percentage errors of each measurand being 0.08%, 0.06%, and 0.12% for n p , n g , and thickness t respectively.

A dual-beam Optical Coherence Tomography system has been developed, using a bespoke dual optical fibre, to simultaneously image microfluidic channel structures and measure high velocity flows (presently 250μm/s) from a single optical access point.

In a proof-of-principle experiment, the vibrations of a set of three tuning folk resonators are simultaneously interrogated along a single optical beam using range-resolved interferometry. Measurements with noise standard deviations in the nm levels over bandwidths of many kHz are possible. In addition, a high degree of environmental noise rejection is inherently achievable because only differential measurements between the vibrating tuning folk prong pairs are evaluated. Employing only highly coherent, robust and cost-effective diode lasers, this approach could be useful for a wide range of mechanical sensor interrogation tasks.

The detection of Campylobacter jejuni by sensitising the surface of an optical fibre long period grating (LPG) with a covalently attached rabbit polyclonal antibody is explored. Previous reports have exploited the use bacteriophages as recognition elements for bacterial detection, while antibodies have been used to detect biochemical interactions. However, to date the use of antibodies for bacterial detection has not been explored widely. It is shown that it is possible to detect bacteria using antibody concentrations as low as 10 μg/ml.

Dynamic fiber-optic shape sensing, often also referred to as curvature or bend sensing, is demonstrated using fiber segment interferometry, where chains of fiber segments, separated by broadband Bragg grating reflectors, are interrogated using range-resolved interferometry. In this paper, the theory of interferometric curvature sensing using fiber segments is developed in detail, including techniques to infer lateral displacements from the measured differential strain data and methods for directional calibration of the sensor. A proof-of-concept experiment is performed, where four fiber strings, each containing four fiber segments of gauge length 20 cm each, are attached to the opposing sides of a flexible support structure and the resulting differential strain measurements are used to determine the lateral displacements of a 0.8 m cantilever test object in two dimensions. Dynamic tip displacement measurements at $ \mathbf{40}\;\mathbf{nm}\cdot \mathbf{Hz}^{-0.5}$ noise levels over a 21 kHz bandwidth demonstrate the suitability of this approach for highly sensitive and cost-effective fiber-optic lateral displacement or vibration measurements.

The diameter of long-period fiber gratings (LPFGs) fabricated in optical fibers with a low cutoff wavelength was be reduced by hydrofluoric acid etching, enhancing the sensitivity to refractive index by more than a factor of 3, to 2611 nm/refractive index unit in the range from 1.333 to 1.4278. The grating period selected for the LPFGs allowed access to the dispersion turning point at wavelengths close to the visible range of the optical spectrum, where optical equipment is less expensive. As an example of an application, a pH sensor based on the deposition of a polymeric coating was analyzed in two situations: with an LPFG without diameter reduction and with an LPFG with diameter reduction. Again, a sensitivity increase of a factor of near 3 was obtained, demonstrating the ability of this method to enhance the sensitivity of thin-film-coated LPFG chemical sensors. This work was supported by the Spanish Agencia Estatal de Investigación (AEI) and Fondo Europeo de Desarrollo Regional (FEDER) (TEC2016-79367-C2-2-R, TEC2016-78047-R), by the Government of Navarre through the project with reference 2017/PI044 and with funding from the Engineering and Physical Sciences Research Council (EPSRC) UK, EP/L010437/1.

A non-contact speckle correlation sensor for the measurement of robotic tool speed is presented for use in robotic manufacturing and is capable of measuring the in-plane relative velocities between a robot end-effector and the workpiece or other surface. The sensor performance was assessed in the laboratory with the sensor accuracies found to be better than 0:01 mm/s over a 70 mm/s velocity range. Finally an example of the sensors application to robotic manufacturing is presented where the sensor was applied to tool speed measurement for path planning in the wire and arc additive manufacturing process using a KUKA KR150 L110/2 industrial robot.

An array of three long period gratings (LPGs) fabricated in a single optical fibre and multiplexed in the wavelength domain was used to measure simultaneously temperature, relative humidity (RH) and volatile organic compounds (VOCs). Each LPG sensor was designed to optimize its response to a desired measurand. The LPGs were fabricated with periods such that they operated at or near the phase matching turning point. The sensors were calibrated in the laboratory and the simultaneous measurement of the key indoor air quality parameters was undertaken in laboratory and office environments. It was demonstrated successfully that the data produced by the LPG sensor array under real conditions was in a good agreement with that produced by commercially available sensors. Further, the potential application of fibre optic sensors for VOCs detection at high levels has been demonstrated.

The use of optical fibre Bragg gratings (FBGs) to monitor the Interface Pressure Distribution (IPD) on an automotive disc brake pad under a variety of loading conditions is studied. The results demonstrate successful strain transfer from the brake pads to the attached FBG sensors under static loading, with a linear response to increasing pressure, and with the measured IPD showing good agreement with that recorded using pressure sensitive paper. Results are also presented demonstrating that changes in the IPD as a result of torque acting on the brake pads can be monitored by the FBG sensors.

The process of fabricating tapered long period gratings (TLPGs) using a CO 2 laser is described. TLPGs with a period spacing of 378 μm, were fabricated by optimization of the taper waist diameter and careful control of the duty-cycle and its uniformity along the length of the grating. The 6-period TLPGs exhibited a pass-band insertion loss of 0.6 dB, resonance band extinction values of 3 dB and had a physical length of 2.27 mm.

The use of an optical fibre long period grating (LPG) as a soil moisture sensor is reported. Characterization of the device in both clay and sandy soils revealed a sensitivity to moisture levels in the range 10-50%, and the results were compared with the output from a Theta probe, the standard soil moisture sensor, which measures the impedance of the soil. © (2017) COPYRIGHT Society of Photo-Optical Instrumentation Engineers (SPIE). Downloading of the abstract is permitted for personal use only.

Dynamic fibre-optic curvature sensing is demonstrated by interrogating chains of fibre segments, separated by broadband Bragg grating reflectors, using range-resolved interferometry (RRI). Four fibre strings, containing four fibre segments each of gauge length 20 cm, are attached to the opposing sides of a support structure and the resulting differential strain measurements allow inference of lateral displacements of a cantilever test object. Dynamic tip displacement resolutions in the micrometre range at an interferometric bandwidth of 21 kHz demonstrate the suitability of this approach for highly sensitive and cost-effective fibre-optic directional vibration measurements of smart structures. © (2017) COPYRIGHT Society of Photo-Optical Instrumentation Engineers (SPIE). Downloading of the abstract is permitted for personal use only

Laser spectroscopy provides the basis of instrumentation developed for the diagnosis of infectious disease, via quantification of organic biomarkers that are produced by associated bacteria. The technology is centred on a multichannel pulsed quantum cascade laser system that allows multiple lasers with different wavelengths to be used simultaneously, each selected to monitor a different diagnostic biomarker. The instrument also utilizes a hollow silica waveguide (HSW) gas cell which has a very high ratio of interaction pathlength to internal volume. This allows sensitive detection of low volume gas species from small volume biological samples. The spectroscopic performance of a range of HSW gas cells with different lengths and bore diameters has been assessed using methane as a test gas and a best-case limit of detection of 0.26 ppm was determined. The response time of this cell was measured as a 1,000 sccm flow of methane passed through it and was found to be 0.75 s. These results are compared with those obtained using a multi-pass Herriot cell. A prototype instrument has been built and approved for clinical trials for detection of lung infection in acute-care patients via analysis of ventilator breath. Demonstration of the instrument for headspace gas analysis is made by monitoring the methane emission from bovine faeces. The manufacture of a hospital-ready device for monitoring biomarkers of infection in the exhaled breath of intensive care ventilator patients is also presented.

In this study, an optical fibre long period grating (LPG) sensor functionalised with a mesoporous thin film was employed for the identification and quality assessment of beverages. The principle of the discrimination of beverages using an LPG sensor is based on the measurement of the change in refractive index of a sensitive film, induced by the binding of the chemical compounds present in the beverage. The sensitive film deposited onto the LPG consisted of poly(allylamine hydrochloride) (PAH) and silica nanospheres (SiO2 NPs) with diameters ranging from 40 nm to 50 nm. PAH imparts selectivity, while the SiO2 NPs endow the film with high porosity and enhanced sensitivity. In this study, five different types of beverages, red and white wines, brandy, nihonshyu (sake, a Japanese rice wine), and shochu (a Japanese distilled beverage), prepared via distillation and fermentation, were used to assess the capability of the sensor to identify the origin of the beverages. In addition, a selection of red wines was used to evaluate the use of the sensor in the assessment of the quality of beverages. The results obtained were benchmarked against those obtained using gas chromatography–mass spectrometry for the determination of volatile compounds contributing to the flavours of a set of red wines. Principal component analysis (PCA) was employed for data analysis. This approach enabled both quality assessment of beverages and identification of the methods and materials used for their preparation. Keywords: Long period grating, Mesoporous thin film, Layer-by-layer, Quality assessment, Beverages

The fabrication of optical fibre long period gratings (LPGs) displaying 2nd order resonant bands operating at the phase matching turning point (PMTP) is explored. Previous reports that exploited 2nd order attenuation bands in sensing schemes did not access the highly sensitive PMTP region. To overcome this limitation, LPGs with periods between 167–177 μm were fabricated using UV irradiation. The spectra acquired were subsequently analyzed and the development of the 2nd order PMTP was identified utilizing peak tracking software. This work has provided the platform for LPG design focused on the prospect of sensitive multi-parameter discrimination.

A novel range-resolved interferometric signal processing technique that uses sinusoidal optical frequency modulation is applied to multi-surface vibrometry, demonstrating simultaneous optical measurements of vibrations on two surfaces using a single, collimated laser beam, with a minimum permissible distance of 3.5 cm between surfaces. The current system, using a cost-effective laser diode and a fibre-coupled, downlead insensitive setup, allows an interferometric fringe rate of up to 180 kHz to be resolved with typical displacement noise levels of 8 pm · Hz−0 5. In this paper, the system is applied to vibrometry measurements of a table-top cryostat, with concurrent measurements of the optical widow and the sample holder target inside. This allows the separation of common-mode vibrations of the whole cryostat from differential vibrations between the window and the target, allowing any resonances to be identified.

The development of an ammonia sensor, formed by the deposition of a functionalised titanium dioxide film onto a tapered optical fibre is presented. The titanium dioxide coating allows the coupling of light from the fundamental core mode to a lossy mode supported by the coating, thus creating lossy mode resonance (LMR) in the transmission spectrum. The porphyrin compound that was used to functionalise the coating was removed from the titanium dioxide coating upon exposure to ammonia, causing a change in the refractive index of the coating and a concomitant shift in the central wavelength of the lossy mode resonance. Concentrations of ammonia as small as 1ppm was detected with a response time of less than 1min. © (2016) COPYRIGHT Society of Photo-Optical Instrumentation Engineers (SPIE). Downloading of the abstract is permitted for personal use only.

Detection of methane at 3.3μm using a DFB Interband Cascade Laser and gold coated integrating sphere is performed. A 10cm diameter sphere with effective path length of 54.5cm was adapted for use as a gas cell. A comparison between this system and one using a 25cm path length single-pass gas cell is made using direct TDLS and methane concentrations between 0 and 1000 ppm. Initial investigations suggest a limit of detection of 1.0ppm for the integrating sphere and 2.2ppm for the single pass gas cell. The system has potential applications in challenging or industrial environments subject to high levels of vibration.

The use of optical fibre Bragg grating (FBG) strain sensors to monitor the condition of safety critical rail components is investigated. Fishplates, switchblades and stretcher bars on the Stagecoach Supertram tramway in Sheffield in the UK have been instrumented with arrays of FBG sensors. The dynamic strain signatures induced by the passage of a tram over the instrumented components have been analysed to identify features indicative of changes in the condition of the components.

Optical coherence tomography (OCT) is an interferometric technique using near-infra-red light to probe the internal structures of semi-transparent samples. Images with a spatial resolution of 3-20 µm can be generated, mapping sub-surface structure to a depth of 1-2 mm, and allowing individual cells to be resolved. Onion (Allium cepa L.) tissue has been investigated using a Thorlabs OCT system based on a broadband 930 nm source. The specified depth resolution was ca. 7 µm and the lateral resolution ca. 10 µm. OCT real-time imaging to a depth of about 0.5 mm was achieved in onion tissue. Acquired images showed the cell-level structure of healthy tissue from several cultivars of stored onion, which were contrasted with images of samples suffering from fungal neck rot (Botrytis allii) or bacterial soft rot (Pseudomonas spp.). The variation in cell structure between different sites in the onion bulb was evident, and clear differences were also seen between images obtained from healthy and diseased tissue. Furthermore, images of tissue affected by neck rot exhibited different features from those showing symptoms of bacterial rot. Initial results demonstrated that OCT can offer an adaptable, real-time tissue-mapping capability, through rapid acquisition of high-resolution histological images. Comparable images obtained using a conventional microscope would require samples to undergo a lengthy slide-mounting procedure. Used alongside other diagnostic methods, OCT will be a significant aid in improving the understanding of both histological and pathological changes in fruit and vegetable crops during growth, harvest and storage.

Shearography is a full-field interferometric speckle technique used to determine displacement derivatives. Measurement of surface strain is possible using shearography if six components of displacement gradient are calculated. This can be achieved using shearography instrumentation that incorporates at least three measurement channels combined with two orthogonal shear directions. This paper presents a laser shearography instrument that utilizes coherent imaging fibre bundles to port four spatially multiplexed speckle images to a single CCD camera via a shearing Michelson interferometer. The four images are spatially multiplexed onto the sensor of a CCD camera. Wrapped phase maps are derived from the recorded speckle interferograms using temporal phase stepping. The unwrapped phase maps are combined with the measurement channel sensitivity vectors using a matrix operation to determine the required displacement derivatives. Results from an out-of-plane displacement of a flat aluminium plate are presented and compared with a computational model. Results from a second test object that show in-plane and out-of-plane strain components are also shown.

An experimental and theoretical study of locally transverse loaded fibre Bragg gratings (FBGs) for pressure sensing purposes is presented. When a load is applied to a short section of an FBG, a spectral hole is generated in the reflection spectrum, which exhibits a redshift in wavelength as the load is increased. This effect has been modelled using Rouard's method and has been characterized experimentally. Two techniques for analysing the spectrum for pressure measurements at constant temperature are considered, one based on measurement of the wavelength shift of the spectral hole, and the other on measurement of peak reflectivities either side of the hole. Normalized pressure sensitivities of 3.30 ± 7.93 × 10−2 MPa−1 and 4.97 × 10−4 ± 1.37 × 10−5 MPa−1 were obtained for the reflectivity and wavelength measurement, respectively. A pressure resolution of 1.3 kPa, over a range of 745 kPa, was achieved when using a tunable laser of 1 pm wavelength resolution to interrogate the sensor. For pressure measurements in the presence of temperature changes, a technique based on the measurement of the position of the spectral hole within the Bragg envelope is presented. This technique allows the opportunity to discriminate pressure and temperature using a single FBG sensor element.

The performance of two complementary optical strain measurement techniques, speckle shearing interferometry (shearography) and fibre Bragg grating (FBG) sensors, is compared with that of resistance foil strain gauges (RFSGs) and with theoretical predictions. The test object used for the surface strain measurements was a hydrostatically loaded ABS pipe. A multi-component shearography instrument, capable of full surface strain measurement, was used to determine the displacement gradient components, from which the surface strain components were calculated. Six surface mounted wavelength division multiplexed FBG sensors were used to measure the axial and the hoop strains. RFSGs located on the surface of the pipe, adjacent to the FBGs, were used for comparison. Reasonable agreement between theory and the axial and hoop strains determined by the different techniques was found. Issues associated with deploying and comparing the techniques are discussed.

A range-resolved interferometric signal processing technique using sinusoidal optical frequency modulation is applied to fibre segment interferometry. Here, six optical fibre segments of gauge length 12.5 cm are used as interferometric strain sensors and are formed between seven weak, broadband fibre Bragg gratings, acting as in-fibre partial reflectors. In a very simple and cost-effective optical setup using injection current modulation of a laser diode source, interferometric measurement of acoustic wave propagation in a metal rod is used to demonstrate the capabilities of the technique.

A method for the preparation of a sensor consisting of an optical fibre long period grating coated with human hemoglobin is described. The utility of this sensor in detecting dissolved oxygen in phosphate buffered saline solution, by the conversion of the coated hemoglobin from deoxyhemoglobin to oxyhemoglobin, is described. The sensor shows good repeatability with a %CV of less than 1% for oxygenated and deoxygenated states and no drift or hysteresis with repeated cycling.

An optical fibre long period grating (LPG) modified with a thin film of ZIF-8, a zeolitic immidazol framework (ZIF) material, a subgroup of the metal organic framework (MOF) family, was employed for the detection of organic vapours. ZIF-8 film was deposited onto the surface of the LPG using an in-situ crystallization technique. The sensing mechanism is based on the measurement of the refractive index (RI) change induced by the penetration of the chemical molecules into the ZIF-8 pores. An LPG modified with 5 growth cycles of ZIF-8 responded to exposure to methanol and ethanol vapours.

Full-text not yet available due to publisher embargo. We present the results of a detailed analysis of the noise behavior of two CCD spectrometers in common use, an AvaSpec-3648 CCD UV spectrometer and an Ocean Optics S2000 Vis spectrometer. Light sources used include a deuterium UV/Vis lamp and UV and visible LEDs. Common noise phenomena include source fluctuation noise, photoresponse nonuniformity, dark current noise, fixed pattern noise, and read noise. These were identified and characterized by varying light source, spectrometer settings, or temperature. A number of noise-limiting techniques are proposed, demonstrating a best-case spectroscopic noise equivalent absorbance of 3.5×10−4 AU for the AvaSpec-3648 and 5.6×10−4 AU for the Ocean Optics S2000 over a 30 s integration period. These techniques can be used on other CCD spectrometers to optimize performance.

A Long period grating (LPG) with a period of 111 μm was fabricated in the highly birefringent (Hi-Bi) optical fibre with the aim of developing a sensor for chirality measurements. The LPG sensor was exposed to different concentrations of glucose D(+) and fructose D(-) in water, which have similar structures but exhibit opposite optical rotations, i.e. chirality. The behaviour of the resonance bands of the submodes corresponding to the two orthogonal polarization states was different depending on the chirality of the compound, thus allowing discrimination between two compounds.

Two highly sensitive ammonia sensors, formed by depositing coatings composed of titanium dioxide (TiO2) onto the cladding of an optical fibre sensing platform, are evaluated. A long period grating (LPG) of period 111 μm was fabricated in the core of an optical fibre so that the LPG operates at or near the phase matching turning point (PMTP). The first coating that was investigated was composed of TiO2 nanoparticles deposited by liquid phase deposition. The sensor showed high sensitivity and allowed low concentrations of ammonia in water (0.01 ppm) to be detected with a response time of less than 60 sec. The second coating was composed of TiO2 with subsequent layers of poly (allyamine hydrochloride) (PAH), and SiO2 nanospheres infused with a sensitive element composed of porphine. The ammonia adsorption to the porphine compound led to the changes in the LPG’s transmission spectrum and allowed 0.1 ppm of ammonia in water to be detected with a response time of less than 60 sec.

The use of bacteriorhodopsin (Br) coatings to create photosensitive optical fibre long period gratings (LPGs) is described. The response of the coated LPGs both sustained and pulsed illumination at a wavelength of 532 nm is monitored. The results show a clear response to the illumination and full recovery of the optical properties of the coating. This technique could allow the use of LPG for typifying photosensitive compounds and to develop optically controlled chemical sensors.

A self-referenced optical fiber refractometer using a ball lens as a sensor head has been developed and characterized. A 350-μm ball lens created at the tip of a single mode fiber has been coated with a 40-nm optically thin layer of palladium that reacts with hydrogen to form a hydride, which has a lower reflectivity than pure palladium. Optical reflectance measurements from the tip of the ball lens were performed to determine the hydrogen response. The change in reflectivity is proportional to the hydrogen concentration in the range 0% to 1% hydrogen in air with a detection limit down to 10 ppm (1σ) in air. This technique offers a simple sensor head arrangement, with a larger sampling area (∼40 times) than a typical single-mode fiber core. A statistical image analysis of a palladium film, with cracks created by accelerated failure, confirms that the anticipated sensor area for a ball lens sensor head has a more predictable reflectivity than that of a bare fiber core.

In this paper, the transmission characteristics of hollow silica waveguides with bore diameters of 300 and 1000 μm are investigated using a 7.8-μm quantum cascade laser system. We show that the bore diameter, coiling and launch conditions have an impact on the number of supported modes in the waveguide. Experimental verification of theoretical predictions is achieved using a thermal imaging camera to monitor output intensity distributions from waveguides under a range of conditions. The thermal imaging camera allowed for more detailed images than could be obtained with a conventionally used beam profiler. The results show that quasi-single-mode transmission is achievable under certain conditions although guided single-mode transmission in coiled waveguides requires a smaller bore diameter-to-wavelength ratio than is currently available. Assessment of mode population is made by investigating the spatial frequency content of images recorded at the waveguide output using Fourier transform techniques.