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1. The SuperCam Instrument Suite on the Mars 2020 Rover: Science Objectives and Mast-Unit Description

Author

Maurice, S., Wiens, R. C., Bernardi, P., Caïs, P., Robinson, S., Nelson, T., Gasnault, O., Reess, J.-M., Deleuze, M., Rull, F., Manrique, J.-A., Abbaki, S., Anderson, R. B., André, Y., Angel, S. M., Arana, G., Battault, T., Beck, P., Benzerara, K., Bernard, S., Berthias, J.-P., Beyssac, O., Bonafous, M., Bousquet, B., Boutillier, M., Cadu, A., Castro, K., Chapron, F., Chide, B., Clark, K., Clavé, E., Clegg, S., Cloutis, E., Collin, C., Cordoba, E. C., Cousin, A., Dameury, J.-C., D’Anna, W., Daydou, Y., Debus, A., Deflores, L., Dehouck, E., Delapp, D., De Los Santos, G., Donny, C., Doressoundiram, A., Dromart, G., Dubois, B., Dufour, A., Dupieux, M., Egan, M., Ervin, J., Fabre, C., Fau, A., Fischer, W., Forni, O., Fouchet, T., Frydenvang, J., Gauffre, S., Gauthier, M., Gharakanian, V., Gilard, O., Gontijo, I., Gonzalez, R., Granena, D., Grotzinger, J., Hassen-Khodja, R., Heim, M., Hello, Y., Hervet, G., Humeau, O., Jacob, X., Jacquinod, S., Johnson, J. R., Kouach, D., Lacombe, G., Lanza, N., Lapauw, L., Laserna, J., Lasue, J., Le Deit, L., Le Mouélic, S., Le Comte, E., Lee, Q.-M., Legett, IV, C., Leveille, R., Lewin, E., Leyrat, C., Lopez-Reyes, G., Lorenz, R., Lucero, B., Madariaga, J. M., Madsen, S., Madsen, M., Mangold, N., Manni, F., Mariscal, J.-F., Martinez-Frias, J., Mathieu, K., Mathon, R., McCabe, K. P., McConnochie, T., McLennan, S. M., Mekki, J., Melikechi, N., Meslin, P.-Y., Micheau, Y., Michel, Y., Michel, J. M., Mimoun, D., Misra, A., Montagnac, G., Montaron, C., Montmessin, F., Moros, J., Mousset, V., Morizet, Y., Murdoch, N., Newell, R. T., Newsom, H., Nguyen Tuong, N., Ollila, A. M., Orttner, G., Oudda, L., Pares, L., Parisot, J., Parot, Y., Pérez, R., Pheav, D., Picot, L., Pilleri, P., Pilorget, C., Pinet, P., Pont, G., Poulet, F., Quantin-Nataf, C., Quertier, B., Rambaud, D., Rapin, W., Romano, P., Roucayrol, L., Royer, C., Ruellan, M., Sandoval, B. F., Sautter, V., Schoppers, M. J., Schröder, S., Seran, H.-C., Sharma, S. K., Sobron, P., Sodki, M., Sournac, A., Sridhar, V., Standarovsky, D., Storms, S., Striebig, N., Tatat, M., Toplis, M., Torre-Fdez, I., Toulemont, N., Velasco, C., Veneranda, M., Venhaus, D., Virmontois, C., Viso, M., Willis, P., and Wong, K. W.

Published
2021
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2. SuperCam Calibration Targets: Design and Development

Author

Manrique, J. A., Lopez-Reyes, G., Cousin, A., Rull, F., Maurice, S., Wiens, R. C., Madsen, M. B., Madariaga, J. M., Gasnault, O., Aramendia, J., Arana, G., Beck, P., Bernard, S., Bernardi, P., Bernt, M. H., Berrocal, A., Beyssac, O., Caïs, P., Castro, C., Castro, K., Clegg, S. M., Cloutis, E., Dromart, G., Drouet, C., Dubois, B., Escribano, D., Fabre, C., Fernandez, A., Forni, O., Garcia-Baonza, V., Gontijo, I., Johnson, J., Laserna, J., Lasue, J., Madsen, S., Mateo-Marti, E., Medina, J., Meslin, P.-Y., Montagnac, G., Moral, A., Moros, J., Ollila, A. M., Ortega, C., Prieto-Ballesteros, O., Reess, J. M., Robinson, S., Rodriguez, J., Saiz, J., Sanz-Arranz, J. A., Sard, I., Sautter, V., Sobron, P., Toplis, M., and Veneranda, M.

Published
2020
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3. Petrological traverse of the olivine cumulate Séítah formation at Jezero crater, Mars : A perspective from SuperCam onboard Perseverance

Author

Beyssac, O., Forni, O., Cousin, A., Udry, A., Kah, L.C., Mandon, L., Clavé, E., Liu, Y., Poulet, F., Quantin Nataf, C., Gasnault, O., Johnson, J., Benzerara, K., Beck, P., Dehouck, E., Mangold, N., Alvarez Llamas, C., Anderson, R., Arana, G., Barnes, R., Bernard, S., Bosak, T., Brown, A.J., Castro, K., Chide, B., Clegg, S., Cloutis, E., Fouchet, T., Gabriel, T., Gupta, S., Lacombe, G., Lasue, J., Le Mouelic, S., Lopez‐Reyes, G., Madariaga, J.M., McCubbin, F.M., McLennan, S., Manrique, J.A., Meslin, P.Y., Montmessin, F., Núñez, J., Ollila, A.M., Ostwald, A., Pilleri, P., Pinet, P., Royer, C., Sharma, S.K., Schröder, Susanne, Simon, J.I., Toplis, M.J., Veneranda, M., Willis, P.A., Maurice, S., Wiens, R.C., Institut de minéralogie, de physique des matériaux et de cosmochimie (IMPMC), Muséum national d'Histoire naturelle (MNHN)-Institut de recherche pour le développement [IRD] : UR206-Sorbonne Université (SU)-Centre National de la Recherche Scientifique (CNRS), Institut de recherche en astrophysique et planétologie (IRAP), Université Toulouse III - Paul Sabatier (UT3), Université de Toulouse (UT)-Université de Toulouse (UT)-Institut national des sciences de l'Univers (INSU - CNRS)-Observatoire Midi-Pyrénées (OMP), Institut de Recherche pour le Développement (IRD)-Université Toulouse III - Paul Sabatier (UT3), Université de Toulouse (UT)-Université de Toulouse (UT)-Institut national des sciences de l'Univers (INSU - CNRS)-Centre National d'Études Spatiales [Toulouse] (CNES)-Centre National de la Recherche Scientifique (CNRS)-Météo-France -Institut de Recherche pour le Développement (IRD)-Institut national des sciences de l'Univers (INSU - CNRS)-Centre National d'Études Spatiales [Toulouse] (CNES)-Centre National de la Recherche Scientifique (CNRS)-Météo-France -Centre National de la Recherche Scientifique (CNRS), Department of Geoscience [Las Vegas], University of Nevada [Las Vegas] (WGU Nevada), Department of Earth and Planetary Sciences [Knoxville], The University of Tennessee [Knoxville], Laboratoire d'études spatiales et d'instrumentation en astrophysique = Laboratory of Space Studies and Instrumentation in Astrophysics (LESIA), Institut national des sciences de l'Univers (INSU - CNRS)-Observatoire de Paris, Université Paris sciences et lettres (PSL)-Université Paris sciences et lettres (PSL)-Sorbonne Université (SU)-Centre National de la Recherche Scientifique (CNRS)-Université Paris Cité (UPCité), Centre d'Etudes Lasers Intenses et Applications (CELIA), Université de Bordeaux (UB)-Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-Centre National de la Recherche Scientifique (CNRS), Jet Propulsion Laboratory (JPL), NASA-California Institute of Technology (CALTECH), Institut d'astrophysique spatiale (IAS), Institut national des sciences de l'Univers (INSU - CNRS)-Université Paris-Saclay-Centre National de la Recherche Scientifique (CNRS)-Centre National d’Études Spatiales [Paris] (CNES), Laboratoire de Géologie de Lyon - Terre, Planètes, Environnement (LGL-TPE), École normale supérieure de Lyon (ENS de Lyon)-Université Claude Bernard Lyon 1 (UCBL), Université de Lyon-Université de Lyon-Institut national des sciences de l'Univers (INSU - CNRS)-Université Jean Monnet - Saint-Étienne (UJM)-Centre National de la Recherche Scientifique (CNRS), Johns Hopkins University Applied Physics Laboratory [Laurel, MD] (APL), Laboratoire de Planétologie et Géosciences - Angers (LPG-ANGERS), Laboratoire de Planétologie et Géosciences [UMR_C 6112] (LPG), Université d'Angers (UA)-Institut national des sciences de l'Univers (INSU - CNRS)-Centre National de la Recherche Scientifique (CNRS)-Nantes université - UFR des Sciences et des Techniques (Nantes univ - UFR ST), Nantes Université - pôle Sciences et technologie, Nantes Université (Nantes Univ)-Nantes Université (Nantes Univ)-Nantes Université - pôle Sciences et technologie, Nantes Université (Nantes Univ)-Nantes Université (Nantes Univ)-Université d'Angers (UA)-Institut national des sciences de l'Univers (INSU - CNRS)-Centre National de la Recherche Scientifique (CNRS)-Nantes université - UFR des Sciences et des Techniques (Nantes univ - UFR ST), Nantes Université (Nantes Univ)-Nantes Université (Nantes Univ), Department of Analytical Chemistry [Malaga], Universidad de Málaga [Málaga] = University of Málaga [Málaga], Astrogeology Science Center [Flagstaff], United States Geological Survey [Reston] (USGS), Department of Analytical Chemistry [Leioa], University of the Basque Country/Euskal Herriko Unibertsitatea (UPV/EHU), Department of Earth Science and Engineering [Imperial College London], Imperial College London, Department of Earth, Atmospheric and Planetary Sciences [MIT, Cambridge] (EAPS), Massachusetts Institute of Technology (MIT), Plancius Research LLC, Los Alamos National Laboratory (LANL), University of Winnipeg, Laboratoire Energie Signal Images et Automatique [Univ Ngaoundéré] (LESIA), Université de Ngaoundéré/University of Ngaoundéré [Cameroun] (UN), Universidad de Valladolid [Valladolid] (UVa), NASA Johnson Space Center (JSC), NASA, Department of Geosciences [Stony Brook], Stony Brook University [SUNY] (SBU), State University of New York (SUNY)-State University of New York (SUNY), PLANETO - LATMOS, Laboratoire Atmosphères, Milieux, Observations Spatiales (LATMOS), Université de Versailles Saint-Quentin-en-Yvelines (UVSQ)-Institut national des sciences de l'Univers (INSU - CNRS)-Sorbonne Université (SU)-Centre National de la Recherche Scientifique (CNRS)-Université de Versailles Saint-Quentin-en-Yvelines (UVSQ)-Institut national des sciences de l'Univers (INSU - CNRS)-Sorbonne Université (SU)-Centre National de la Recherche Scientifique (CNRS), Hawaii Institute of Geophysics and Planetology (HIGP), University of Hawai‘i [Mānoa] (UHM), DLR Institute of Optical Sensor Systems, Deutsches Zentrum für Luft- und Raumfahrt [Berlin] (DLR), Department of Earth, Atmospheric, and Planetary Sciences [West Lafayette] (EAPS), and Purdue University [West Lafayette]

Subjects
spectroscopy, LIBS, m2020, Mars, Perseverance, Jezero, Jezero crater, reflectance spectroscopy, in-situ, [SDU]Sciences of the Universe [physics], rover, Seitah, VisIR, Raman, in-situ science
Abstract

International audience; Séítah is the stratigraphically lowest formation visited by Perseverance in the Jezero crater floor. We present the data obtained by SuperCam: texture by imagery, chemistry by LIBS, and mineralogy by VISIR and Raman spectroscopy. The Séítah formation consists of igneous, weakly altered, rocks dominated by millimeter-size grains of olivine with the presence of low-Ca and high-Ca pyroxenes, and other primary minerals (e.g., plagioclase, Cr-Fe-Ti oxides, phosphates). Along a ∼140 m long section in Séítah, SuperCam analyses showed evidence of geochemical and mineralogical variations, from the contact with the overlying Máaz formation, going deeper in the formation. Bulk rock and olivine Mg#, grain size, olivine content increase gradually further from the contact. Along the section, olivine Mg# are not in equilibrium with the bulk rock Mg#, indicating local olivine accumulation. These observations are consistent with Séítah being the deep ultramafic member of a cumulate series derived from the fractional crystallization and slow cooling of the parent magma at depth. Possible magmatic processes and exhumation mechanisms of Séítah are discussed. Séítah rocks show some affinity with some rocks at Gusev crater, and with some martian meteorites suggesting that such rocks are not rare on the surface of Mars. Séítah is part of the Nili Fossae regional olivine-carbonate unit observed from orbit. Future exploration of Perseverance on the rim and outside of the crater will help determine if the observations from the crater floor can be extrapolated to the whole unit, or if this unit is composed of distinct sub-units with various origins.

Published
2023
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4. Developing Tailored Data Combination Strategies to Optimize the SuperCam Classification of Carbonate Phases on Mars.

Author

Veneranda, M., Manrique, J. A., Lopez‐Reyes, G., Julve‐Gonzalez, S., Rull, F., Alvarez Llamas, C., Delgado Pérez, T., Gibbons, E., Clavé, E., Cloutis, E., Huidobro, J., Castro, K., Madariaga, J. M., Randazzo, N., Brown, A., Willis, P., Maurice, S., and Wiens, R. C.

Subjects
LASER-induced breakdown spectroscopy, CARBONATE minerals, FISHER discriminant analysis, MARS (Planet), PRINCIPAL components analysis, DISCRIMINANT analysis, GEOLOGICAL modeling, NAIVE Bayes classification
Abstract

The SuperCam instrument onboard the Mars 2020 Perseverance rover investigates Martian geological targets by a combination of multiple spectroscopic techniques. As Raman, Visible‐Infrared Spectroscopy, and Laser‐Induced Breakdown Spectroscopy (LIBS) spectra deliver complementary information about the interrogated sample, the multivariate analysis of combined spectroscopic data sets is here proposed as a tool to optimize the SuperCam capability to discriminate mineral phases on Mars. For this purpose, the laboratory study of carbonate phases within the Ca‐Mg‐Fe ternary system were selected as representative case of study. After the characterization of model samples, the discrimination capability of mono analytical Raman, VISIR, and LIBS data sets was evaluated by applying a chemometric approach based on the combination of principal component analysis (for sample clustering) and Linear Discriminant Analysis (for mineral classification). Afterward, the low‐level combination (LL) of Raman, VISIR, and LIBS data was achieved by concatenating their spectra into a single data matrix. The mineral classification achieved by LL data sets outperformed the mono analytical ones, thus proving the complementarity between molecular and elemental spectroscopic techniques. Mineral classification was further improved by using a mid‐level data combination strategy. After evaluating benefits and limitations afforded by the proposed combination strategies, future developments are finally outlined. As such, the final objective of this research line is to develop a classification model based on data combination to optimize the capability of SuperCam in discriminating relevant minerals on Mars, this being a key requirement for the selection of the optimal targets to be cached for the future Mars Sample Return Mission. Plain Language Summary: The SuperCam instrument onboard the Perseverance rover is capable of analyzing Martian rocks and soils by a combination of Laser‐Induced Breakdown Spectroscopy (LIBS), Raman and Visible‐Infrared Spectroscopy (VISIR). Learning from terrestrial applications, the complementary information provided by the three spectroscopic techniques can be correlated to obtain a more accurate interpretation of the analyzed target. This approach could be particularly useful to discriminate carbonates, which are interesting minerals where to look for traces of past life. Having this in mind, several carbonate samples have been analyzed with laboratory Raman, LIBS, and VISIR instrument. After evaluating the advantages and limitations of each technique, their data were merged by using low‐level and mid‐level strategies that were successfully used previous works. This work proved that, when spectra are combined, the discrimination of carbonate phases is more accurate than when each technique is interpreted separately. This suggests the scientific results obtained by SuperCam on Mars could benefit from the development of tailored classification models based on data combination. Key Points: Data combination of Raman, Visible‐Infrared Spectroscopy, and Laser‐Induced Breakdown Spectroscopy spectra collected by SuperCam is proposedLow‐ and mid‐level data combination strategies based on principal component analysis (discrimination) + PC‐Linear Discriminant Analysis (classification are evaluated and compared)The low‐level combination method outperformed the mono analytical discrimination. The mid‐level one further improved the results [ABSTRACT FROM AUTHOR]

Published
2023
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5. Carbonate Detection with SuperCam in Igneous Rocks on the floor of Jezero Crater, Mars

Author

Clavé, E., Benzerara, K., Meslin, P.‐Y., Forni, O., Royer, C., Mandon, L., Beck, P., Quantin‐Nataf, C., Beyssac, O., Cousin, A., Bousquet, B., Wiens, R.C., Maurice, S., Dehouck, E., Schröder, Susanne, Gasnault, O., Mangold, N., Dromart, G., Bosak, T., Bernard, S., Udry, A., Anderson, R.B., Arana, G., Brown, A.J., Castro, K., Clegg, S.M., Cloutis, E., Fairén, A.G., Flannery, D.T., Gasda, P.J., Johnson, J.R., Lasue, J., Lopez‐Reyes, G., Madariaga, J.M., Manrique, J.A., Le Mouélic, S., Núñez, J.I., Ollila, A.M., Pilleri, P., Pilorget, C., Pinet, P., Poulet, F., Veneranda, M., and Wolf, Z.U.

Subjects
spectroscopy, LIBS, M2020, Mars 2020, Mars, carbonates, Perseverance, VISIR, exploration, Geophysics, SuperCam, in-situ, Space and Planetary Science, Geochemistry and Petrology, Earth and Planetary Sciences (miscellaneous), Raman
Published
2022
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6. Caracterización multianalítica de meteorito marciano NWA2975 mediante CF-LIBS, fluorescencia de rayos X y espectroscopía Raman

Author

Delgado, Tomás, Laserna Vázquez, J. Javier, Cabalin-Robles, Luisa Maria, García-Gómez, Laura, Fortes, Francisco Javier, Dell'Aglio, M., Poblacion, I., Torre-Fernandez, I., Aramendia, J., Lopez-Reyes, G., Madariaga, J.M., Rull, F., De Giacomo, A., Carrizo, D., Martínez- Frías, J., Belenguer, T., Taravillo, J., Huidobro, J., Manrique, J.A., Arana, G., Castro, K., and Veneranda, M.

Subjects
LIBS, Martian, Meteoritos
Abstract

La caracterización isotópica y elemental de los meteoritos de Marte ha permitido determinar la cronología de los procesos de formación del planeta y avanzar en la comprensión de su evolución biogeoquímica e hidrológica. Los meteoritos más abundantes son las rocas de origen ígneo, como las shergottitas. Los estudios petrológicos y geoquímicos previos del meteorito Northwest Africa 2975 (NWA 2975), revelaron que se trata de una roca volcánica de grano medio, entre subofítica y granular, compuesta predominantemente por piroxenos (57,3 vol.%) y plagioclasa (38,3 vol. %) completamente enmascarados con fases opacas (2,7 vol.%) y fosfatos (1,7 vol.%) [1]. El instrumento SuperCam a bordo del rover Perseverance (misión MARS 2020 de la NASA) está equipado con técnicas atómicas y moleculares (incluyendo LIBS y Raman) para la detección y análisis a distancia de muestras geológicas en la superficie del Planeta Rojo. La capacidad de estas técnicas se ha demostrado ampliamente en la caracterización de rocas, minerales y suelos en varias misiones espaciales. En el presente trabajo, se analizó un fragmento del meteorito NWA 2975 mediante un sistema de micro-LIBS con el objetivo de revelar su composición química elemental. Debido a la heterogeneidad intrínseca de la muestra, se analizaron diferentes posiciones de su superficie. El análisis cuantitativo de los elementos principales (Si, Al, Fe, Mg, Mn, Ca y O) y de otros elementos menores se llevó a cabo utilizando la metodología Calibration-Free [2]. Los resultados sugieren la presencia de piroxenos como principal componente mineral en las posiciones inspeccionadas, aunque también se pueden encontrar otras fases minerales como la plagioclasa. La información extraída del análisis LIBS se ha comparado con la de fluorescencia de rayos X (XRF) y la espectroscopia Raman. El uso combinado de diferentes técnicas espectroscópicas ha permitido obtener una mejor interpretación de los resultados composicionales. Universidad de Málaga. Campus de Excelencia Internacional Andalucía Tech.

Published
2022

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