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4. Mg deposition observed by in situ electrochemical Mg K-edge X-ray absorption spectroscopy

Author

Arthur, Timothy S., Glans, Per-Anders, Matsui, Masaki, Zhang, Ruigang, Ma, Biwu, and Guo, Jinghua

Subjects
*X-ray absorption near edge structure, *MAGNESIUM, *ELECTROPLATING, *ELECTROCHEMISTRY, *ELECTROLYTIC reduction, *MAGNESIUM compounds
Abstract

Abstract: The electrochemical deposition of magnesium from [Mg2(μ-Cl)3·6(OC4H8)]+ has been monitored in situ with X-ray absorption spectroscopy. The viability of the cell design was confirmed by a reversible shift in the X-ray absorption near-edge spectroscopy (XANES) of the Mg K-edge. In situ electrochemical XANES revealed the presence of an interfacial Mg intermediate below the equilibrium Mg/Mg2+ potential. A new method has been established to directly observe the complex electrochemical reduction process from Mg electrolytes. [Copyright &y& Elsevier]

Published
2012
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