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InconelTM 718 is widely used for commercial application in aerospace industry and additive manufacturing process allows for versatile design and manufacturing opportunities. In the present research, the results of a wide experimental campaign run on additive manufactured InconelTM 718 specimens obtained with different processing parameters are presented. In particular, the influence of process parameters (for both vertical and horizontal planes with respect to the building direction) on the hardness properties are investigated. A further investigation is performed on the optimal hardness testing procedure for additive manufacturing. The research is extended to as-built and heat-treated specimens. The new insight gained is that the orientation of the printing direction with respect to indentation direction can be responsible for scattering in hardness measurements and indentation size effect. As-built specimens show a strong anisotropy for in-plane and growth directions and an increment of hardness with respect to increasing energy density. The difference between hardness value with respect to the energy density and the measurements scattering are reduced by the heat treatment. A careful handling of hardness data is required when dealing with additive manufactured materials.

A customized Al-Cu-Mg-Si alloy is successfully processed by selective laser melting. AlSi10Mg powder, used as a master alloy, has been mixed with pure Cu powder through a fluidized bed and the obtained powder mix was used as feedstock material for the printing process. To investigate the feasibility of the process and to discuss the effect of the process parameters, a two-step experimental campaign has been carried out: in the first batch of experiments the energy density has been varied to frame the processing window while in the second batch the energy density has been kept constant and the main process parameters have been varied to highlight their influence on the process. Density, porosity, and microhardness have been chosen as output to evaluate the success of the process. The microstructure and composition phase were studied through scanning electron microscopy and X-ray elemental mapping, respectively. A maximum relative density of 97% has been obtained while a predominant role of the laser beam power has been observed.

The in-situ contour strategy during Laser-Powder Bed Fusion (L-PBF) process remains one of the most promising solutions to improve the poor surface quality of the parts. On the other hand, it is well established that contour step affects the formation of sub-surface defects. The aim of this work is to assess the entity of sub-surface defects during the Laser-Powder Bed Fusion of Inconel 718 samples for which different contour processing conditions are considered. Cubic samples with 10 mm side were produced through L-PBF using a Concept Laser Cusing M2 L-PBF machine. The samples were printed with fixed bulk laser parameters, adopting a layer thickness of 30 μm and a chessboard laser scanning strategy. The in-situ contour conditions were changed in terms of laser scanning speed and hatch zone border. Afterwards, the samples were analyzed in terms of surface roughness (Sa) and sub-surface density through confocal microscopy. The results revealed that the surface roughness was the most affected output as a function of the varied process parameters, including the sample position on the building platform, with values ranging from 13 to 32 μm. On the other hand, the sub-surface density was always higher than 99%.

In this research activity, the manufacturing of metallic coatings on polymer-based panels through the low pressure cold spray technique was studied. Aluminium particles were sprayed for the metallization and carbon fibre composite materials with thermoplastic matrix (PP, PA66) were used as substrates. Different deposition parameter combinations have been set to investigate the feasibility of the process; SEM analyses were carried out to study the coating surface morphology and the interface interaction between particle and substrate. The results showed that the CS process is an effective technique to create aluminium coatings on polymeric matrix composite materials: compact coatings can be obtained if the process parameters are properly set.

The deposition of steel powders on glass fiber reinforced polymer (GFRP) with the Cold Spray technique is investigated. Metallization of composite materials is still challenging when high-strength and dense powders, such as steel, are used due to excessive erosion of the polymer or disruption of the fibers during the deposition. To overcome these issues, low-pressure cold spray equipment has been used for the experimental campaign shown in this paper. Different coatings were obtained by using nitrogen as the carrier gas and different sets of pressure and standoff distance. Optimization of the process parameters, including the stratification of the laminate, has been carried out. Results of an initial study of the feasibility of the process and the influence of the different chosen spray conditions are exposed. In particular, the bonding mechanisms of steel powders and their morphology are discussed.

Cold spray deposition of aluminum powders on polyethylene reinforced with glass fibers has been studied. Different processing conditions, including different stratifications of the fiber-reinforced polymer used as a substrate, have been investigated to better understand the deposition mechanism. The experimental campaign has been conceived and tailored to highlight the influence of several process parameters on the deposition of the first layer of particles. The results obtained allowed to highlight and clarify the influence of standoff distance and gas pressure and also gave some insights concerning the effect of the substrate stratification. Guidelines regarding the design of the manufacturing process have been also released.

In this work, the mechanical behaviour of natural composite fibre sandwich panels is experimentally investigated. The composite sandwich panels are composed of a natural core made of Posidonia dried leaves reinforced with aluminium skins. The introduced material system is characterized by good structural behaviour (due to the aluminium skins) combined with the good thermal and acoustical insulation provided by the Posidonia core. Flexural and impact tests, characterized by different impact energies, have been performed on specimens with and without the aluminium skins, to preliminary assess the influence of the Posidonia core densities on the natural fibre sandwich mechanical behaviour.

In this activity, customized panels for the CS deposition have been produced and aluminium has been deposited using air as a carrier gas. The custom-made panels were made with different matrix thicknesses on the surface in order to point out the influence of the fibres in the deposition and to study the feasibility and the growth of the coating. The polymer chosen for the matrix is polypropylene, widely used in the automotive sector, while for the reinforcements glass fibres have been used. Different process parameters have been examined in order to point out the influence of temperature, stand-off distance and pressure chosen, on the compaction and densification of the coating produced. In addition, morphological investigations were performed to further characterize the coatings deposited. It has been noticed that aluminium powders can be effectively deposited on polypropylene panels, leading to significantly better results when the thickness of the matrix is ​​sufficient to prevent the powders bouncing elastically on the fibres, while benefiting from the stiffening effect of the latter.

Cemented carbides present some characteristics that ensure high performances for cutting and wear-resistant tools. The aim of the work is to evaluate the influence of Chromium Carbide and Nickel on the properties (wear and friction) of a cemented carbide constituted by a hard phase of tungsten carbide and a binder phase of cobalt. Different tests were carried out by varying the percentage of Cr3C2 and, for one only case, also Nickel was added. The tests were carried out by a pin-on-disk apparatus and diamond abrasive sheet. The experimental campaign provided tests for different values of load and relative velocity. Friction coefficient was directly evaluated by the apparatus and data on the wear were obtained by measuring the loss of weight of the samples (parallelepipeds with hemispherical head). The tests allowed to determine the percentage of Cr3C2 that ensure an improvement of the aforementioned properties and to highlight the irrelevance of Nickel.

Cold roll forming is a process for plastic deformation, which allows realizing profiles, with a defined section and established length, from the plastic deformation of a metal sheet. The sheet is induced to cross several stands of rolls, arranged along the same axis of advancing. The rolls induce plastic deformation in the sheet and then lead it to the desired geometric configuration. In order to control the geometric parameters of the plate during the profiling, it was created a FEM model to simulate the final stage of the technological process, developed by an industrial production line of a company located in Naples (Italy), that sells tubes with several cross sections. In this phase, the semi-finished product, having a circular cross section, is forced to cross through four stands of rolls. In this way, it changes the geometric condition of the cross section from circular to square. The model was carried out using a non-linear calculation code, which allows analyzing the parameters of interest in the different process steps. The results, obtained numerically, were compared with the experimental ones through the measurement of five specimens, obtained directly from technological process. The values of percentage deviation, regarding the external dimension and the thickness, for each step of advancement, do not exceed the 3% of error. Then, the analysis results denote the capability to simulate the cold roll forming process using finite element method.