1. In situ X-ray imaging and numerical modeling of damage accumulation in C/SiC composites at temperatures up to 1200 °C.
- Author
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Qian, Weijian, Zhang, Wanen, Wu, Shengchuan, Hu, Yue, Zhang, Xiangyu, Hu, Qiaodan, Dong, Shaoming, and Tu, Shantung
- Subjects
X-ray imaging ,STRESS concentration ,THERMAL stresses ,INFRARED radiation ,RESIDUAL stresses ,SYNCHROTRON radiation ,CARBON fiber-reinforced ceramics ,CERAMIC-matrix composites - Abstract
• An in situ extreme thermal-force coupled X-ray tomography testing system is described. • Temperature-induced failure mode transition is revealed by time-lapse X-ray tomography. • The role of thermal residual stresses and voids is analyzed via high-fidelity simulations. Carbon fiber reinforced silicon carbide matrix composites (C/SiC) have emerged as key materials for thermal protection systems owing to their high strength-to-weight ratio, high-temperature durability, resistance to oxidation, and outstanding reliability. However, manufacturing defects deteriorate the mechanical response of these composites under extreme thermal-force coupling conditions, prompting significant research attention. This study demonstrates a customized in situ loading device compatible with synchrotron radiation facilities, enabling high spatial and temporal resolution recording of internal material damage evolution and failure behavior under thermal-force coupling conditions. Infrared thermal radiation units in a confocal configuration were used to create ultra-high-temperature environments, offering advantages of compactness, rapid heating, and versatility. In situ tensile tests were conducted on C/SiC samples in a nitrogen atmosphere at both room temperature and 1200 °C. The high-resolution image data demonstrate various failure phenomena, such as matrix cracking and pore linkage. Image-based finite element simulations indicate that the temperature-dependent variation of the failure mechanism is attributable to thermal residual stresses and defect-induced stress concentrations. This work seamlessly integrates extreme mechanical testing methods with in situ observation techniques, providing a comprehensive solution for accurately quantifying crack initiation, pore connection, and failure behavior of C/SiC composites. [Display omitted] [ABSTRACT FROM AUTHOR]
- Published
- 2024
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