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The control of solidification microstructure is critical to successful laser processing of single-crystal (SX) nickel-base superalloys and a practical tool for the microstructural control is processing–microstructure maps. However, the maps presented in literature do not consider the effects of powder feeding during laser additive manufacturing (LAM) of SX superalloys. This paper therefore presents a simple and feasible strategy to deal with the effects of powder feeding and to extend the combined numerical model used to calculate processing–microstructure maps. A characteristic ratio of epitaxial SX growth was defined to quantitatively compare the final solidification microstructure. Resulting processing–microstructure maps can estimate the influence of most processing variables, especially powder feeding rate, on the extent of epitaxial SX growth and the position of columnar-to-equiaxed transition. Using the processing parameters selected according to these processing–microstructure maps, a multi-layer SX deposit with fine dendrites was successfully fabricated by LAM. This successful SX LAM indicates that these new processing–microstructure maps involving powder feeding are reliable and useful because they can determine proper processing windows for LAM of SX superalloys and further advance the understanding of the processing–microstructure relationship in powder-feeding LAM process. [ABSTRACT FROM AUTHOR]

Experimental process optimization is essential to obtain reliable processing conditions prior to performing actual laser additive manufacturing (LAM) of single-crystal (SX) nickel-base superalloys. The influence of processing parameters on deposited productivity and epitaxial SX growth in powder-feeding LAM process was systematically investigated by the orthogonal experiment (OE) method, a statistical experiment design method. This method can rapidly and economically estimate the effect of each processing parameter by a small number of experiments. Resulting relationship between the processing variables and each of deposited productivity and microstructure formation contributes to the selection of detailed processing conditions to balance the factors crucial to successful SX LAM, which means that appropriate adjustment of the processing parameters during actual SX LAM is easy to be performed. On the basis of the analyses of the OE results, a combination of relatively high power, low scanning velocity and moderate powder feeding rate is beneficial to both deposited productivity and epitaxial SX growth during powder-feeding LAM, and allows the preparation of good multilayer SX deposits with fine dendrites. [ABSTRACT FROM AUTHOR]

The solidification path of single-crystal nickel-base superalloys containing minor carbon was investigated under various laser rapid directional solidification (LRDS) conditions. By controlling the solidification rate, LRDS processing can provide the evidence whether some diffusion-controlled phase transformations occur because such transformations will be suppressed under high cooling rates. Results show that the solidification path and final solidification microstructure depend upon the cooling rate; the microstructure without γ-γ′ eutectic can be obtained as long as the cooling rate is high enough. A peritectic transformation in carbon-containing single-crystal superalloys was first experimentally verified by controlling the cooling rate during LRDS processing. [ABSTRACT FROM AUTHOR]

Primary dendritic arm spacing (PDAS) is an important microstructure feature in the nickel-base single-crystal (SX) superalloys by laser rapid directional solidification (LRDS). A combined numerical model was developed in this paper to investigate the influence of laser processing parameters on the PDAS. This model consists of (1) the theoretical PDAS models which relate PDAS to the solidification conditions and (2) the heat-flux calculations of laser processing which provide the solidification conditions as a function of the processing parameters. It is therefore able to immediately relate the PDAS to the processing parameters and obtain corresponding processing–microstructure maps. To verify the predicted accuracy, the PDAS values calculated by different theoretical models were compared with those produced under different processing conditions. Results show that the PDAS firstly decreases and then increases at a lower laser power whereas it decreases with increasing scanning velocity at a higher laser power, leading to nose-shape contour lines. The predicted accuracy depends on appropriate selections of material thermo-physical properties. These processing–microstructure maps can accurately capture the trends of the PDAS variation with the processing parameters and contribute to the control and optimization of dendritic microstructure while determining relevant processing windows for controlled SX laser processing. [ABSTRACT FROM AUTHOR]

The stray-grain formation and epitaxy loss at the substrate during laser surface remelting of single-crystal nickel-base superalloys, which immediately lead to the break of the single-crystal growth, were investigated by means of modeling and experiments. Results indicate that the stray-grain formation and epitaxy loss at the substrate are attributed to the increased trend of the formation of equiaxed grains resulting from the composition segregation at the substrate interdendritic region. Accordingly, a solution treatment for the substrates prior to laser processing can effectively avoid the SG formation and epitaxy loss, which reveals a basic precondition, homogenized solution treatment of substrates, for successful single-crystal laser processing. [ABSTRACT FROM AUTHOR]