1. A safe procedure for HF etching as part of sample preparation for luminescence dating.
- Author
-
Faershtein, Galina and Porat, Naomi
- Subjects
- *
THERMOLUMINESCENCE dating , *HYDROFLUORIC acid , *ETCHING , *QUARTZ , *POISONING - Abstract
This paper presents a protocol for safe quartz etching with hydrofluoric (HF) acid as part of sample preparation for luminescence dating. Concentrated HF is extremely hazardous and can cause severe burns and poisoning, even leading to death. Generally, in order to avoid exposure to light and bleaching, HF etching is performed in a dark laboratory under weak orange-red light in wide-open beakers. Handling HF in open beakers in the dark could result in unfortunate accidents due to unintentional spillage. The presented protocol avoids these two main safety issues - working with open beakers and under poor lighting. The samples are etched inside black opaque bottles with narrow openings so that the procedure can be safely performed in comfortable light levels. To validate the harmlessness of the laboratory environmental light, bleaching experiments of quartz were conducted under the same conditions as the protocol. These showed that no bleaching occurred during this procedure. [ABSTRACT FROM AUTHOR]
- Published
- 2023