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With the downscaling of devices, due to device geometry shrinkage, the total number of cleaning steps has increased dramatically. As a result, the number of drying cycles after cleaning has increased as well. As the device shrinks with the integration density increase, it is noteworthy that a perfect drying efficiency is mandatory to obtain a high performance device [. Basically, the mechanism of wafer drying in semiconductor industry can be explained as: first reducing the amount of liquid on the wafer surface by mechanical forces. There are some approaches for removing the liquid such as spinning, high pressure gas blowing by nozzle or air-jet, vertical withdrawal from the liquid bath, using surface gradient tension and so on [2]. Second: if the mechanical forces in the liquid removal part are not sufficient for drying and some droplets or a thin liquid layer remain on the wafer surface, complete drying will be achieved by evaporation of the remaining layer on the wafer. After this evaporation step, known as state transformation, the wafers will be completely dried. Evaporation of the remaining liquid layer is the main mechanism for generating drying defects (watermarks, residues, particles, and etc.)[3]. In this study, we propose a new methodology for semiconductor wafer drying based on a high-pressure gas flow. In comparison to conventional drying tools, the new drying set up combines high speed drying (wafer drying time down to 2 sec at 150mm.s-1) and a low number of added drying defects.

Cleaning of nano-particles is becoming a major challenge in semiconductor manufacturing as efficient particle removal must be achieved without substrate loss and without damage to fragile structures. In this work cleaning performance and structural damage by a mixed fluid-jet technique were evaluated and directly compared to the performance of several megasonic systems. The test vehicles were hydrophilic Si wafers contaminated with 78-nm SiO2 particles and 70-nm poly-gatestack line patterned wafers. The results showed a broader process window for particle removal without damaging for the mixed fluid-jet technique compared to the megasonic systems.

In this paper, a single wafer linear IPA vapour based vertical drying technique is presented. Using salt residue tests the performance of this technique is evaluated and compared to spin drying. The equivalent film thickness of evaporating liquid is below 0.05µm for blanket wafers, which is two orders of magnitude less than with spin drying. It is also shown that the presence of surface topography (200nm high TEOS features on Si covered with a chemical oxide) does not significantly influence the drying performance. A study of the process window shows that for the setup evaluated in this work best performance is achieved when the IPA/N2 flow rate is above 20 liters per minute and the drying speed is below 8 mm/s. With a manual prototype already very good particle performance is demonstrated.

Publisher Summary In this chapter, the performance of several drying techniques commonly used in the semiconductor manufacturing industry is evaluated. This is done by measuring the residues on a wafer onto which a solution containing metal salts acting as tracer elements has been dispensed and dried. To correctly interpret the experimental data, the results are compared with predictions from a theoretical model. This model assumes two distinct mechanisms for deposition: adsorption and evaporative deposition. The first mechanism is a result of attractive interactions between the contaminant and the wafer surface, while the second mechanism is due to liquid evaporation during drying. For the latter case, the evaporated film thickness is introduced as a figure of merit for the drying process under study. In the tests, tests, spin drying was compared with two types of Marangoni based drying: on a vertically moving wafer and on a horizontally rotating wafer. The results show that for spin drying two consecutive phases occur: during the first seconds of spinning convective removal of liquid is the dominant mechanism, followed by a phase where evaporation takes over. This behavior is confirmed by models reported in the literature describing photo-resist coating. The amount of liquid evaporating during spin drying is inversely proportional to the square root of the rotation speed. This suggests that entrainment of liquid by the gas flow over the wafer surface is the dominant mechanism for evaporation. This finding is in agreement with fluid dynamics models describing the flow of gas entrained with a rotating substrate.

A novel fast drying method for single wafer wet cleaning is proposed. The water-mark free drying method is based on an efficient interaction between Marangoni forces and rotational forces. The method is shown to yield excellent particle performance.

To ensure high device yields, wafer surface contamination and defects must be monitored and controlled during the entire process of semiconductor manufacturing. Particle surface concentrations on the wafers, mostly related to chemical mechanical polishing (CMP) processes, must be kept at the lowest possible levels. Brush scrubber cleaning has the potential to achieve this goal. However, the particle removal mechanisms are still under discussion especially the removal of nano-sized particles. This paper investigates the interactions between the particle, the brush and the wafer surface and explores the potential and limitations of the brush scrubbing technique. Furthermore the effect of the various brush/wafer parameters on the particle removal efficiency (PRE) is studied. From a mechanistic viewpoint it is shown that brush scrubbing acts in a mixed lubrication regime. From an extensive analysis of the relevant forces and moments it can be concluded that in the hydrodynamic lubrication regime, particles ar...

Brush scrubbers are among the most commonly used instruments for wafer-cleaning applications nowadays. However, the removal mechanisms of nanosized particles are far from clear, especially because no direct experimental data are available to backup theoretical models in the literature. This study combines a theoretical approach based on a force analysis with an experimental study of the removal of nanosized slurry particles. In the theoretical part, all forces affecting the adhesion and the removal of particles are evaluated to determine which are dominant in two extreme removal mechanisms: lifting and rolling. In the experimental part, the removal efficiency of 34nm SiO2 particles is investigated by using the haze approach. Based on a study of the aging of contaminated wafers, conditions are selected where no chemical bonds are formed between a particle and a substrate. Force analysis and experimental observations both show that nanosized particles cannot be lifted directly by a brush. Instead, rolling s...