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Two small exposures of quartz-porphyritic rocks occur on the farm Zoutpekel 98 in the Marydale Terrane between the Doornberg Fault and Brakbos Shear Zone, apparently overlying Kaapvaal basement granite but lacking clear field relationships due to sand and Dwyka tillite cover. They are lavas and tuffs, metamorphosed in lower amphibolite facies. They contain quartz phenocrysts with a distinctive blue colour, due to metamorphic exsolution of rutile. Microbeam U-Pb zircon dating gives a combined 207Pb/206Pb age of 2 722 ± 3 Ma (seven determinations on four samples), interpreted as the age of extrusion. Three of these samples give the same discordia upper intercept age, but one sample gives discordia intercepts of 2 688 ± 15 and 1 223 ± 120 Ma, thought to reflect metamorphic lead loss related to the ~1 210 Ma Namaqua terrane assembly collisions. The Zoutpekel exposures are coeval with the 2 720 ± 2 Ma Makwassie Formation of the Platberg Group, Ventersdorp Supergroup. They also correspond geochemically to the Makwassie Formation and no other unit of the supergroup. A sample from the T'kuip Formation of the nearest Ventersdorp Supergroup inlier on the Kaapvaal Craton (east of the Doornberg Fault), gives an age of 2 716 ± 8 Ma, also confirming its lithostratigraphic and geochemical correlation with the Makwassie Formation. The Zoutpekel exposures show that not only the Kaapvaal basement granites, but also the supracrustal cover rocks of the Ventersdorp Supergroup, extend southwards across the Doornberg Fault, The Marydale Terrane is thus not an exotic terrane, but probably represents a passive continental margin developed at the beginning of the 1 300 to 1 000 Ma Namaqua-Natal Wilson cycle. The age range of the Ventersdorp Supergroup and the age and stratigraphic correlation of the Marydale Group thrust complex, which straddles the Zoutpekel exposures, will be investigated in two companion papers. [ABSTRACT FROM AUTHOR]

The Koras Group is a bimodal volcanosedimentary group located in post-tectonic grabens in a foreland thrust complex in the Kaaien Terrane of the Mesoproterozoic Namaqua-Natal Province of southern Africa. It contains two sequences of mafic and felsic volcanic rocks with an unconformity between them, only the lower sequence being slightly folded. The Koras Group was long regarded as having formed at the end of the 1 210 to 1 000 Ma Namaqua Orogeny, because it lacks the severe deformation and metamorphism of the underlying rocks, with igneous minerals preserved in many samples. Following years of unsuccessful attempts to precisely date the volcanic rocks, the first two ion probe U-Pb zircon studies both reported ages of ~1 172 Ma for the Swartkopsleegte Formation felsic lava in the slightly folded lower sequence (based on relatively few dated zircons) and ~1 100 Ma for the Leeuwdraai Formation rhyolite in the undeformed upper sequence. Thus a major 70 m.y. hiatus seemed apparent between the lower and upper sequences despite their similar geochemistry and rift-related setting. This gave rise to models which envisaged the Kaaien Terrane being unaffected by the syn- to late-tectonic deformation, migmatisation and granite intrusions, documented between 1 200 and 1 150 Ma in the adjoining Namaqua-Natal terranes to the west. A high-pressure (10 kbar) metamorphic event, recognised in the Kaaien Terrane basement just south of hardlydeformed Koras Group exposures and dated at 1 150 Ma, is inconsistent with such models. A re-investigation and microbeam dating campaign on the Koras Group confirms the 1 101 ± 2 Ma (n = 6) age for felsic volcanic rocks of the upper sequence, but establishes a new reliable age of 1 114 ± 4 Ma for the lower one (n = 2). The 1 170 ages obtained in the earlier two studies were revisited and are now considered to reflect the age of zircon xenocrysts from the source rocks, which dominate the zircon population of some Swartkopsleegte Formation samples. Several criteria to distinguish autocrystic (magmatic) from antecrystic (age-overlappping xenocrystic) data points were investigated. One sample had high Th levels in only the younger zircons, but histograms of sufficiently precise 207Pb/206Pb ages provided the main criterion. Calculations of zircon crystallisation temperature intervals were not useful in predicting the abundance or proportions of magmatic and antecryst zircons. A multi-episode model of magmatic generation and crystallisation events is probably appropriate. In cases when felsic volcanic samples yield few zircons, care must be taken to avoid the problem exposed in this study. The Koras Group sediments have similar detrital zircon U/Pb age distributions to those of the Rehoboth Basement Inlier. This supports the concept that the Kaaien Terrane originated as the southern part of the Rehoboth Province. [ABSTRACT FROM AUTHOR]

• Ventersdorp Contact Reef (VCR) second youngest gold ore horizon after Black Reef. • Major erosional unconformity between Witwatersrand and VCR. • Most detrital zircons derived from Witwatersrand Supergroup. • Youngest detrital zircons 2799 ± 9 Ma, probably not from Witwatersrand Supergroup. • Ventersdorp Supergroup constrained between 2799 and 2642 Ma. The Ventersdorp Contact Reef (VCR) at the base of the >4.5 km-thick volcanosedimentary Ventersdorp Supergroup unconformably overlies the Witwatersrand Supergroup and is the second youngest mineable reef in the Witwatersrand Goldfields. The volcanic rocks of the Ventersdorp Supergroup are predominantly mafic, affected by low-grade thermal metamorphism and difficult to date. Only the Makwassie Formation in the upper Platberg Group of the main Ventersdorp repository has been reliably dated on four felsic volcanic samples at 2720 ± 2 Ma. The actual timing of Ventersdorp volcanism and the duration of the three recognised lithostratigraphic groups remains enigmatic, despite much research and heroic attempts to synthesize the available data. In this work detrital zircon grains from VCR conglomerates were U-Pb dated in order to improve the time constraints on the Klipriviersberg Group at the base of the Ventersdorp Supergroup. The six youngest grains in VCR samples were reliably dated at 2799 ± 9 Ma. The Klipriviersberg Group and the Ventersdorp Supergroup is thus younger than 2808 Ma and the supergroup is older than the 2642 Ma Vryburg Formation at the base of the Transvaal Supergroup. Comparisons of detrital grain dates confirm that the VCR was largely derived from erosion products of the underlying Witwatersrand Supergroup, however the youngest VCR grains are ~20 Ma younger and may have been derived directly from magmatic rocks in the provenance or a felsic facet of the synchronous komatiitic Klipriviersberg volcanism. Multi-grain analyses of discordant grains show that recent lead loss is predominant. However about 5% of the data show the effect of complex Mesoproterozoic lead loss, which can yield ages as much as 150 Ma too young in 10% discordant data. This was found in grains with high Th-induced radiation damage, providing a criterion for data rejection. The proposed large igneous provinces dated between 2791 and 2683 Ma, based mainly on dated mafic dykes, which are not in contact with supracrustal Ventersdorp rocks, do fit the established time constraints and might provide a key to Ventersdorp chronostratigraphy. However only the proposed 2754–2709 Ma Platberg volcanic province is based on reliably dated Platberg Group volcanic rocks. [ABSTRACT FROM AUTHOR]