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In this study we test the potential of the elevated temperature infrared stimulated luminescence (IRSL) signals for dating Romanian loess. The recently developed post-IR IRSL protocol is applied to Romanian loess using polymineral fine grains extracted from the loess-palaeosol sequence at Mircea Vodă (SE Romania). This approach is aimed at obtaining an additional age control to examine the age discrepancy obtained from previous optically stimulated luminescence (OSL) studies using different grain-sizes of quartz (4–11 μm and 63–90 μm). Two preheat post-IR IR stimulation temperature combinations were used, 250–225 °C and 325–300 °C, respectively. The signals obtained are documented in terms of dose response curve, laboratory tests and fading. Although both post-IR IRSL signals exhibit small fading rates, dose response characteristics indicate that these rates may be laboratory artefacts. The post-IR IRSL signal stimulated at 300 °C is observed to suffer from dose dependent initial sensitivity changes as both natural and regenerated signals are observed to lie above the saturation level of the dose response curve. Uncorrected age results obtained using both post-IR IRSL signals are in general agreement with previously reported silt-sized quartz OSL ages for samples collected from the uppermost loess unit L1. For older material, the post-IR IRSL signal stimulated at 225 °C is considered to provide reliable age results, in agreement with independent age control available for this sequence. [ABSTRACT FROM AUTHOR]

Abstract: Romanian loess -palaeosol sequences are amongst the thickest and most complete available in Europe. These deposits represent an extended continental record of environmental and climatic change during at least five glacial/interglacial cycles. Their chronology, however, is mainly based on relative methods. In this paper, we investigate whether SAR–OSL dating of fine-grained quartz can be used to establish a reliable chronology for Romanian loess. The samples were collected from the loess–palaeosol sequence near Mircea Vodă (Dobrogea, SE Romania). The luminescence characteristics of the fine-grained quartz extracts are investigated to some extent, and indicate that the applied laboratory measurement procedure (SAR) is reliable. An internally consistent set of optical ages is obtained for the loess deposited up to ∼70ka, and evidence is presented for a varying loess accumulation rate during the Last Glacial. Comparison with independent age control (pedostratigraphy and a newly-developed palaeomagnetic time–depth model) indicates that the optical dating procedure underestimates the true burial age from the penultimate glacial period onwards (i.e. for samples below the last interglacial S1 palaeosol). These results indicate that an apparently reliable laboratory measurement procedure not necessarily yields accurate sedimentation ages. We suggest that quartz-based SAR–OSL ages obtained using the high dose linear region of the growth curve are interpreted with caution. [Copyright &y& Elsevier]