51. Fabrication and characterization of cadmium sulfide nanoparticles using chemical precipitation method.
- Author
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Turki, Zainab T., Hindawi, Aula M. Al, and Shiltagh, Nagham M.
- Subjects
- *
PRECIPITATION (Chemistry) , *CADMIUM sulfide , *NANOPARTICLES , *X-ray diffraction , *SHAPE measurement - Abstract
CdS nanoparticles were prepared successfully using chemical precipitation technique. CdCl2 and Na2S were utilized as precursors for Cd ions and sulfide ions in aqueous media, respectively. The effect of reaction temperature, reaction time and PH values on the growth process of CdS particles were investigated realizing that 30 oC. 6 hours and PH of 11 are the best conditions for producing CdS nanoparticles. Structural features showed that CdS particles have a nearly spherical shape and the XDR measurement confirmed the presence of both cadmium and sulfur atoms in as-prepared particles. The bandgap energy was calculated from the Uv-Visible spectrum ∼2.66 eV, which is high compared to 2.42 eV (Eg of bulk CdS). XRD pattern showed that the zinc blend phase is dominated and the particle size was estimated at around 3.2 nm using the Scherrer formula. [ABSTRACT FROM AUTHOR]
- Published
- 2023
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