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The Simons Observatory (SO) is a cosmic microwave background instrumentation suite in the Atacama Desert of Chile. More than 65,000 polarization-sensitive transition-edge sensor (TES) bolometers will be fielded in the frequency range spanning 27 to 280 GHz, with three separate dichroic designs. The mid-frequency 90/150 GHz and ultra-high-frequency 220/280 GHz detector arrays, fabricated at NIST, account for 39 of 49 total detector modules and implement the feedhorn-fed orthomode transducer-coupled TES bolometer architecture. A robust production-level fabrication framework for these detector arrays and the monolithic DC/RF routing wafers has been developed, which includes single device prototyping, process monitoring techniques, in-process metrology, and cryogenic measurements of critical film properties. Application of this framework has resulted in timely delivery of nearly 100 total superconducting focal plane components to SO with 88 % of detector wafers meeting nominal criteria for integration into a detector module: a channel yield > 95 % and T c in the targeted range. [ABSTRACT FROM AUTHOR]

The Simons Observatory is a cosmic microwave background experiment stationed atop Cerro Toco, at an elevation of 5200 ms in Chile's Atacama Desert. The receivers of the Observatory will contain more than 60,000 transition edge sensor bolometers. In order to read out this large detector count in a scalable manner, we utilize a microwave superconducting quantum interference device (SQUID) multiplexing scheme where each detector is inductively coupled to an rf SQUID, which in turn is inductively coupled to a GHz resonator. More than 2000 SQUIDs and resonators are fabricated on a single 76.2-mm-diameter silicon wafer. To qualify wafers before integration, we cryogenically screen ∼ 10% of the devices on each wafer by use of a standard set of measurements. From these data, we report parameter value trends in 47 wafers that were fabricated in the past two years. We show good control in key parameters such as frequency placement, internal quality factor, and response to applied flux. We demonstrate a wafer acceptance yield of 86%. [ABSTRACT FROM AUTHOR]

The Simons Observatory (SO) experiment is a cosmic microwave background (CMB) experiment located in the Atacama Desert, Chile. The SO's small aperture telescopes (SATs) consist of three telescopes designed for precise CMB polarimetry at large angular scales. Each SAT uses a cryogenic rotating half-wave plate (HWP) as a polarization modulator to mitigate atmospheric 1/f noise and other systematics. To realize efficient polarization modulation over the observation bands, we fabricated an achromatic HWP (AHWP) consisting of three sapphire plates with anti-reflection coatings. The AHWP is designed to have broadband modulation efficiency and transmittance. This paper reports on the design and the preliminary characterization of the AHWPs for SATs. [ABSTRACT FROM AUTHOR]

The Simons Observatory (SO) is a cosmic microwave background instrumentation suite being deployed in the Atacama Desert in northern Chile. The telescopes within SO use three types of dichroic transition-edge sensor (TES) detector arrays, with the 90 and 150 GHz Mid-Frequency (MF) arrays containing 65% of the approximately 68,000 detectors in the first phase of SO. All of the 26 required MF detector arrays have now been fabricated, packaged into detector modules, and tested in laboratory cryostats. Across all modules, we find an average operable detector yield of 84% and median saturation powers of (2.8, 8.0) pW with interquartile ranges of (1, 2) pW at (90, 150) GHz, respectively, falling within their targeted ranges. We measure TES normal resistances and superconducting transition temperatures on each detector wafer to be uniform within 3%, with overall central values of 7.5 m Ω and 165 mK, respectively. Results on time constants, optical efficiency, and noise performance are also presented and are consistent with achieving instrument sensitivity forecasts. [ABSTRACT FROM AUTHOR]

For cosmic microwave background (CMB) polarization observations, calibration of detector polarization angles is essential. We have developed a fully remote controlled calibration system with a sparse wire grid that reflects linearly polarized light along the wire direction. The new feature is a remote-controlled system for regular calibration, which has not been possible in sparse wire grid calibrators in past experiments. The remote control can be achieved by two electric linear actuators that load or unload the sparse wire grid into a position centered on the optical axis of a telescope between the calibration time and CMB observation. Furthermore, the sparse wire grid can be rotated by using a motor. A rotary encoder and a gravity sensor are installed on the sparse wire grid to monitor the wire direction. They allow us to achieve detector polarization angle calibration with an expected systematic error of 0.08°. The calibration system will be installed in small-aperture telescopes at Simons Observatory. [ABSTRACT FROM AUTHOR]

The microwave SQUID multiplexer (μ MUX) is a high channel-count multiplexer that, when coupled to low-temperature detectors such as Transition Edge Sensor (TES) Bolometers, has applications across astronomy and physics. Our primary application is for the Simons Observatory, an array of CMB polarimeters utilizing over 70,000 μ MUX readout channels, located in the Atacama Desert. To facilitate the delivery of high-quality multiplexers to the project, we have developed a high-throughput microwave SQUID screening measurement system, capable of measuring microwave devices operating over the frequency range of 4–8 GHz. Here, we present the hardware design comprised of a cryogen-free 100 mK 2-stage Adiabatic Demagnetization Refrigerator (ADR) cryostat, microwave packages which hold μ MUX chips, and the microwave readout chain necessary to do these measurements. In addition, we describe the screening protocols and show example results. [ABSTRACT FROM AUTHOR]

The Simons Observatory is a ground-based cosmic microwave background instrument to be sited in the Atacama Desert in Chile. SO will deploy 60,000 transition-edge sensors (TES) bolometers in 49 separate focal-plane modules across a suite of four telescopes covering three dichroic bands termed low frequency (LF), mid-frequency and ultra-high frequency. Each MF and UHF focal-plane module packages 1720 feedhorn-coupled detectors with cryogenic components for highly multiplexed readout using microwave SQUID multiplexing. In this paper, we describe the testing program we have developed for high-throughput validation of modules after they are assembled. The validation requires measurements of the yield, saturation powers, time constants, noise properties and optical efficiencies. Additional measurements will be performed for further characterization as needed. We describe the methods developed and demonstrate preliminary results from the initial testing of a prototype module. [ABSTRACT FROM AUTHOR]

The Simons Observatory (SO) will detect and map the temperature and polarization of the millimeter-wavelength sky from Cerro Toco, Chile, across a range of angular scales, providing rich data sets for cosmological and astrophysical analysis. The SO focal planes will be tiled with compact hexagonal packages, called universal focal-plane modules (UFMs), in which the transition-edge sensor (TES) detectors are coupled to 100 mK microwave-multiplexing electronics. Three different types of dichroic TES detector arrays with bands centered at 30/40, 90/150, and 220/280 GHz will be implemented across the 49 planned UFMs. The 90/150 GHz and 220/280 GHz arrays each contain 1764 TESes, which are read out with two 910x multiplexer circuits. The modules contain a series of routed silicon chips, which are packaged together in a controlled electromagnetic environment and operated at 100 mK. Following an overview of the module design, we report on early results from the first 220/280 GHz UFM, including detector yield, as well as readout and detector noise levels. [ABSTRACT FROM AUTHOR]

The Simons Observatory (SO) includes four telescopes that will measure the temperature and polarization of the cosmic microwave background using over 60,000 highly sensitive transition-edge bolometers (TES). These multichroic TES bolometers are read out by a microwave RF SQUID multiplexing system with a multiplexing factor of 910. Given that both TESes and SQUIDs are susceptible to magnetic field pickup and that it is hard to predict how they will respond to such fields, it is important to characterize the magnetic response of these systems empirically. This information can then be used to limit spurious signals by informing magnetic shielding designs for the detectors and readout. This paper focuses on measurements of magnetic pickup with different magnetic shielding configurations for the SO universal multiplexing module (UMM), which contains the SQUIDs, associated resonators, and TES bias circuit. The magnetic pickup of a prototype UMM was tested under three shielding configurations: no shielding (copper packaging), aluminum packaging for the UMM, and a tin/lead-plated shield surrounding the entire dilution refrigerator 100 mK cold stage. We also present measurements of the pickup in the UMM when aluminum feedhorns are installed. The measurements show that the aluminum packaging outperforms the copper packaging by a shielding factor of 8-10, and adding the tin/lead-plated 1K shield further increases the relative shielding factor in the aluminum configuration by 1-2 orders of magnitude. The addition of feedhorns provides a factor of 30 improvement when the tin/lead shield is not installed and a factor of 5 improvement when it is. [ABSTRACT FROM AUTHOR]

We present the design and measured performance of a new carbon fiber strut design that is used in a cryogenically cooled truss for the Simons Observatory small aperture telescope. The truss consists of two aluminum 6061 rings separated by 24 struts. Each strut consists of a central carbon fiber tube fitted with two aluminum end caps. We tested the performance of the strut and truss by (i) cryogenically cycling and destructively pull-testing strut samples, (ii) non-destructively pull-testing the final truss, and (iii) measuring the thermal conductivity of the carbon fiber tubes. We found that the strut strength is limited by the mounting fasteners and the strut end caps, not the epoxy adhesive or the carbon fiber tube. This result is consistent with our numerical predictions. Our thermal measurements suggest that the conductive heat load through the struts (from 4 to 1 K) will be less than 1 mW. This strut design may be a promising candidate for use in other cryogenic support structures. [ABSTRACT FROM AUTHOR]

A cadmium germanium arsenide compound, Cd3Ge2As4, was synthesized using a double-containment fused quartz ampoule method within a rocking furnace and a melt-quench technique. The crystal structure was determined from single-crystal X-ray diffraction (SC-XRD), scanning and transmission electron microscopies (i.e. SEM, STEM, and TEM), and selected area diffraction (SAD) and confirmed with electron backscatter diffraction (EBSD). The chemistry was verified with electron energy loss spectroscopy (EELS). [ABSTRACT FROM AUTHOR]

Hysteretic behavior was studied in a series of Fe thin films, grown by molecular beam epitaxy, having different grain sizes and grown on different substrates. Major and minor loops and first order reversal curves (FORCs) were collected to investigate magnetization mechanisms and domain behavior under different magnetic histories. The minor loop coefficient and major loop coercivity increase with decreasing grain size due to higher defect concentration resisting domain wall movement. First order reversal curves allowed estimation of the contribution of irreversible and reversible susceptibilities and switching field distribution. The differences in shape of the major loops and first order reversal curves are described using a classical Preisach model with distributions of hysterons of different switching fields, providing a powerful visualization tool to help understand the magnetization switching behavior of Fe films as manifested in various experimental magnetization measurements. [ABSTRACT FROM AUTHOR]

Abstract: Cement-based waste forms have long been considered economical technologies for disposal of various types of waste. A solidified cementitious waste form, Cast Stone, has been identified to immobilize the radioactive secondary waste from vitrification processes. In this work, Cast Stone was considered for a Na-based caustic liquid waste, and its physical properties were analyzed as a function of liquid waste loading up to 2M Na. Differences in crystallinity (phase composition), microstructure, mesostructure (pore size distribution and surface area), and macrostructure (density and compressive strength) were investigated using various analytical techniques, in order to assess the suitability of Cast Stone as a chemically durable waste. It was found that the concentration of secondary waste simulant (caustic waste) had little effect on the relevant engineering properties of Cast Stone, showing that Cast Stone could be an effective and tolerant waste form for a wide range of concentrations of high sodium waste. [Copyright &y& Elsevier]

Abstract: Thin film samples of CeCl3, CeBr3, and combinatorial compositions along the CeCl3–CeBr3 join were produced using thermal evaporation, which is being evaluated as a method for rapid screening of scintillator materials. The combinatorial thin films were shown to be compositionally reproducible from run-to-run within reasonable limitations. Analytical results suggest a continuous variation in the combinatorial samples in terms of their compositions, crystal structures, and luminescence characteristics. [Copyright &y& Elsevier]

Both granular activated carbon (GAC) and silver mordenite (AgM) are utilized for the removal of contaminants and radionuclides (e.g., radioiodine) from off-gas streams in nuclear fuel reprocessing and high temperature immobilization of nuclear waste. Following their service lifetimes, the GAC and AgM contain an inventory of contaminants and radionuclides and require stabilization in a matrix for disposal. GAC and AgM are referred to as solid secondary waste (SSW) materials. Cementitious waste forms can be used as the stabilization matrix for SSW, however, for successful stabilization, the inclusion of GAC and AgM should not negatively impact the physical behavior of the cementitious waste form or increase release of the contaminants/radionuclides compared to the baseline case without stabilization. The present work focuses on evaluation of cement formulations, with and without slag, for the stabilization of iodine-loaded GAC or AgM. The results showed that both a slag-containing and slag-free formulations were able to stabilize GAC and AgM, up to 30 vol%, without deleterious impacts on the bulk physical properties of the encapsulating matrix. When monolithic samples of the GAC or AgM containing cement formulations were subjected to leach tests, it was observed that iodide leached from the SSW) had limited sorption to either of the cement matrices. Nonetheless, the iodine can interact with the SSW materials themselves. Specifically, iodine retention within monolithic samples containing the iodine-loaded GAC or AgM was improved for AgM containing waste forms while no improvement was observed for the GAC containing waste forms. The improvement for the AgM containing waste forms was likely due to an enrichment of Ag at the interface between the AgM particles and the cement matrix that can impede iodine migration out from the waste form. The results are significant in highlighting the potential for long-term retention of iodine in specific cementitious waste forms. • Cementitious formulations can be used to stabilize solid secondary waste (SSW). • SSW includes granular activated carbon (GAC) and silver mordenite (AgM). • SSW inclusion up to 30 vol% had minimal impact on bulk properties. • At AgM-matrix interface, an Ag layer was observed that could serve as an I barrier. • Substantial improvement in I retention was observed for AgM based on diffusivity. [ABSTRACT FROM AUTHOR]

Single crystal Fe thin films (∼250 nm) were grown on MgO substrates and irradiated with 2.0 MeV Fe+ ions at 10 and 50 dpa, and the defect evolution was studied using high resolution Transmission Electron Microscopy (HR-TEM) and Doppler Broadening Positron Annihilation Spectroscopy (PAS). It was shown that irradiation induced or exacerbated a thin oxide layer at the outer interface and produced substantial Fe/Mg mixing at the film/substrate interface, particularly for the higher dose. Modeling of the PAS data allowed interpretation of the defect types at different distances from the Fe surface, and included several types of MgO substrate damage and annihilation condition changes, indicative of damage due to ballistic effects of the Fe atoms as well as chemical changes due to implantation and subsequent diffusion. This detailed PAS study compared with TEM and energy dispersive spectroscopy (EDS) provides significant insight into depth-dependent defect creation. These results will be useful for predicting defect creation in Fe-based materials under irradiation conditions, for extension to neutron irradiated structural materials. [ABSTRACT FROM AUTHOR]

We developed a broadband two-layer anti-reflection (AR) coating for use on a sapphire half-wave plate (HWP) and an alumina infrared (IR) filter for the cosmic microwave background (CMB) polarimetry. Measuring the faint CMB B-mode signals requires maximizing the number of photons reaching the detectors and minimizing spurious polarization due to reflection with an off-axis incident angle. Sapphire and alumina have high refractive indices of 3.1 and are highly reflective without an AR coating. This paper presents the design, fabrication, quality control, and measured performance of an AR coating using thermally sprayed mullite and Duroid 5880LZ. This technology enables large optical elements with diameters of 600 mm. We also present a thermography-based nondestructive quality control technique, which is key to assuring good adhesion and preventing delamination when thermal cycling. We demonstrate the average reflectance of about 2.6% (0.9%) for two observing bands centered at 90/150 (220/280) GHz. At room temperature, the average transmittance of a 105 mm square test sample at 220/280 GHz is 83%, and it will increase to 90% at 100 K, attributed to reduced absorption losses. Therefore, our developed layering technique has proved effective for 220/280 GHz applications, particularly in addressing dielectric loss concerns. This AR coating technology has been deployed in the cryogenic HWP and IR filters of the Simons Array and the Simons observatory experiments and applies to future experiments such as CMB-S4.

We present near-field radio holography measurements of the Simons Observatory Large Aperture Telescope Receiver optics. These measurements demonstrate that radio holography of complex millimeter-wave optical systems comprising cryogenic lenses, filters, and feed horns can provide detailed characterization of wave propagation before deployment. We used the measured amplitude and phase, at 4 K, of the receiver near-field beam pattern to predict two key performance parameters: 1) the amount of scattered light that will spill past the telescope to 300 K and 2) the beam pattern expected from the receiver when fielded on the telescope. These cryogenic measurements informed the removal of a filter, which led to improved optical efficiency and reduced sidelobes at the exit of the receiver. Holography measurements of this system suggest that the spilled power past the telescope mirrors will be less than 1%, and the main beam with its near sidelobes are consistent with the nominal telescope design. This is the first time such parameters have been confirmed in the lab prior to deployment of a new receiver. This approach is broadly applicable to millimeter and submillimeter instruments.