201. Microstructural and thermochemical properties of Al/AlN/CuAl2 composite prepared by a combination of combustion synthesis and spark plasma sintering
- Author
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Jong-Hyeon Lee, Tae-Hyuk Lee, Hayk H. Nersisyan, Kap-Ho Lee, Ha-Guk Jung, and Ju-Hyeon Sun
- Subjects
Mechanical pressure ,Materials science ,Fabrication ,Thermal conductivity ,Mechanics of Materials ,Nanofiber ,Composite number ,Ceramics and Composites ,Nitrogen atmosphere ,Spark plasma sintering ,Composite material ,Combustion - Abstract
A combination of combustion synthesis (CS) and spark plasma sintering (SPS) technology was employed in the fabrication of Al/AlN/CuAl 2 dense composites. Al/AlN/CuAl 2 composite powders in which a portion of the AlN was present in macro- and nanofiber forms were prepared by combustion of Al–Cu–5 wt.% (C 2 F 4 ) n , under a nitrogen atmosphere. The resulting composite powders were then subjected to consolidation by SPS at a dwell temperature level of 1500 °C, mechanical pressure of 60 MPa, and a non-isothermal heating time of 10 min. It is found that the actual thermal conductivity of Al/AlN/CuAl 2 composites fabricated with 5 wt.% (C 2 F 4 ) n is much higher than that of materials prepared in the absence (C 2 F 4 ) n . Maximum thermal conductivity (320 W/m K) was recorded for the samples prepared from an 0.8Al–0.2Cu–5 wt.% (C 2 F 4 ) n mixture. The influence of (C 2 F 4 ) n on the growth mechanism of AlN fibers and thermal conductivity of composite samples is discussed in light of the experimental data.
- Published
- 2012
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