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The aging characteristics of Al/UHSS resistance rivet welding (RRW) joints are investigated for the first time in this paper. Microstructure studies have shown that the aging treatment does not change the phase composition of the Al/steel mixed nugget still remaining the ferrite structure, while the precipitation, growth and dissolution occur for the microstructure of Al alloy varying with the distance from the rivet. Mechanical tests revealed that for interfacial fracture (IF) and button pullout fracture (BPF) joints, the maximum peak load increased by 13% and 26% with the prolonged aging time, respectively. The improvement in the joint strength after aging can be attributed to the relaxation of the residual stress for IF joint and the age hardening of Al sheet for BPF joint. In addition, interestingly, the accelerated artificial aging is discovered firstly in Al/steel RRW joint. The phenomenon can be attributed to the higher solid solubility of Mg and Si in softening zone of Al sheet, resulting in faster and more precipitation during the aging treatment. The precipitation kinetics indicated that the average Avrami exponent was 1.25, proving the one-dimensional linear growth of fresh nuclei of the hardening phase β''. The block shear model analysis suggested that the Canadian Standards Association, giving the calculating/test values ratio ranged from 0.88 to 1.08, could provide a more reasonable calculation, which showed that the shear failure was mainly determined by the yield of the gross shear plane, and the tension plane failed because of tensile rupture during the lap-shear test.

The purpose of this study was to evaluate the effect of finishing/polishing systems on the translucency parameter (TP) of resin composites after accelerated artificial aging (AAA). Four composite resins (Filtek Z250, Admira, IPS Empress Direct, Clearfil Majesty Esthetic) were evaluated. Thirty samples were prepared with each resin composite and divided into three subgroups: control (Mylar strip), disc (Optidisc), and rubber (Dimanto) (n=10). The spectrophotometer was used to determine color measurements. TP was calculated the using the CIEDE 2000 formula. Data were analyzed using Generalized Lineer Model (p<0.05). The three factors (composite resin, finishing/polishing, and AAA) had no statistically significant influence on the TP. However, composite and finishing/polishing influenced the TP. Filtek Z250 showed the lowest TP values and the IPS Empress Direct showed the highest TP values before and after AAA. Polished groups showed higher TP values than control groups before and after AAA. IPS Empress Direct with Dimanto had higher TP values than other groups (except for IPS Empress Direct with Optidisc); Filtek Z250 with finishing/polishing groups showed lower TP values than other groups. Composite type and finishing/polishing systems influenced TP values. Unfinished groups exhibited lower TP values than finished groups. There was no difference in TP values between finishing/polishing systems (Dimanto and OptiDisc). [ABSTRACT FROM AUTHOR]

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Aim In the present study, we evaluated the influence of surface sealing on color stability and surface roughness of a composite resin after accelerated artificial aging. Methods Thirty-two specimens of a composite were prepared. After 24 h, the specimens were polished and divided into four groups ( n = 8), according to the surface sealant used, including the control, which had no sealant application. Baseline color was measured according to the CIELab system using a reflection spectrophotometer. Surface roughness was determined using a profilometer with a cut-off of 0.25 mm. After these tests, specimens were aged for 252 h in an ultraviolet ( UV)-accelerated aging chamber. Color stability was determined by difference between coordinates obtained before and after the aging procedure. Data of color change and roughness were evaluated by anova and Fisher's exact test ( α = 0.05). Results The results showed that the unsealed group had the highest color change compared to other groups ( P = 0.0289), and there was no significant difference between groups sealed with surface sealant ( P > 0.05). The artificial aging caused an increase in roughness values independent of the experimental group studied ( P = 0.0015). Conclusion The sealed composites showed lower color change after UV aging, but all groups showed clinically-acceptable color change, and only liquid polish decreased roughness. [ABSTRACT FROM AUTHOR]

Tests simulating exposure to severe weather conditions have been relevant in seeking new applications for particleboard. This study aimed to produce particleboards with residues of CCB (chromium-copper-boron oxides) impregnated Pinus sp. and castor oil-based polyurethane resin, and to evaluate their performance before and after artificial accelerated aging. Panels were produced with different particle mass, resin content and pressing time, resulting eight treatments. Particles moisture and size distribution were determined, beyond panel physical and mechanical properties, according to NBR14810-3: 2006. After characterization, treatments B and G (small adhesive consumption and better mechanical performance, respectively) were chosen to artificial aging tests. Statistical results analysis showed best performances were achieved for waterproof aged samples, of both B and G treatments. As example, in treatment B, MOR and MOE values were 23 MPa and 2,297 MPa, samples before exposure; 26 MPa and 3,185 MPa, 32 MPa and 3,982 MPa for samples after exposure (non-sealed and sealed), respectively.

This study evaluated the effect of artificially accelerated aging (AAA) on the surface hardness of eight composite resins: Filtek Z250, Filtek Supreme, 4 Seasons, Herculite, P60, Tetric Ceram, Charisma, and Filtek Z100. Sixteen specimens were made from the test piece of each material, using an 8.0 × 2.0 mm teflon matrix. After 24 hours, eight specimens from each material were submitted to three surface hardness readings using a Shimadzu Microhardness Tester for 5 seconds at a load of 50 gf. The other eight specimens remained in the artificially accelerated aging machine for 382 hours and were submitted to the same surface hardness analysis. The means of each test specimen were submitted to the Kolmogorov-Smirnov test (p > 0.05), ANOVA and Tukey test (p < 0.05). With regard to hardness (F = 86.74, p < 0.0001) the analysis showed significant differences among the resin composite brands. But aging did not influence the hardness of any of the resin composites (F = 0.39, p = 0.53). In this study, there was interaction between the resin composite brand and the aging factors (F = 4.51, p < 0.0002). It was concluded that notwithstanding the type of resin, AAA did not influence surface hardness. However, with regard to hardness there was a significant difference among the resin brands.

Purpose: The objective of the in vitro study was to assess the effect accelerated artificial aging, bleaching agents and coffee staining on the color, gloss, roughness and microhardness of a nanocomposite. Materials and methods: 120 (7 x 2 mm) were prepared and randomly divided into 2 groups (n = 60) depending on the aging. Each group was further subdivided into 6 subgroups (n = 10) according to the bleaching and staining as follows: 10% carbamide peroxide (10% CP), 10% CP + staining, 35% hydrogen peroxide (35% HP), 35% HP + staining, without bleaching treatment (WB) and WB + staining. Scanning electron microscopy was performed for qualitative analysis of the resin surface. Data were submitted to 3-way analysis of variance (ANOVA) and Tukey's test for multiple comparisons. As for ΔE, multiple comparisons were performed by using Tukey's and Dunnett's tests (α = 0.05). Results: The bleaching reduced significantly the microhardness of the nanocomposite in without aging groups. All physical properties were found to be negatively changed after the aging process, with bleaching treatment with 10% CP increasing significantly the roughness and loss of gloss compared to the 35% HP. Staining reduced microhardness of both with and without aging nanocomposite as well as the color of the former (E>25), a significantly different result compared to controls. Conclusions: The bleaching reduced the microhardness of the nanocomposite, whereas the aging process changed all the properties studied. The bleaching favored extrinsic staining of the with aging nanocomposite. [ABSTRACT FROM AUTHOR]

The aim of this study was to compare the compressive strength of a silorane-based composite resin (Filtek P90) to that of conventional composite resins (Charisma, Filtek Z250, Fill Magic, and NT Premium) before and after accelerated artificial aging (AAA). For each composite resin, 16 cylindrical specimens were prepared and divided into 2 groups. One group underwent analysis of compressive strength in a universal testing machine 24 hours after preparation, and the other was subjected first to 192 hours of AAA and then the compressive strength test. Data were analyzed by analysis of variance, followed by the Tukey HSD post hoc test (α = 0.05). Some statistically significant differences in compressive strength were found among the commercial brands (P < 0.001). The conventional composite resin Fill Magic presented the best performance before (P < 0.05) and after AAA (P < 0.05). Values for compressive strength of the silorane-based composite were among the lowest obtained, both before and after aging. Comparison of each material before and after AAA revealed that the aging process did not influence the compressive strength of the tested resins (P = 0.785). [ABSTRACT FROM AUTHOR]

Objective: Investigation of the shade stability of polymer-infiltrated and resin nano ceramic crowns before and after artificial aging., Method: 40 identical crowns of each of the materials VITA Enamic (VE) and Lava Ultimate (LU) were manufactured. Half of the crowns went through a dynamic chewing simulation (CS) with thermocycling. Material subgroups: 1. VE, 2. VE/CS, 3. LU, 4. LU/CS (each n=20). These were divided into 4 groups (n=5) and distributed in usual stain solutions. The shade of each crown was measured occlusally and vestibularly before and after insertion using a spectrophotometer (n=5). The data were analyzed using ANOVA and Tukey's test (p≤0.05)., Results: Sum scores (SSC) of the occlusal ΔE values: LU/CS: 7.99, VE: 5.75 VE/CS: 5.44, LU: 5.17. The total sum of the SSC yielded, for the materials: SSCtotal(VE): 20.0 and SSCtotal(LU): 24.0., Significance: Occlusally, there were significant shade differences for VE/CS (p=0.025) and LU/CS (p=0.014) between red wine and distilled water. LU/CS is significantly more clearly stained occlusally by coffee in comparison to the other three material subgroups (VE: p=0.007, LU: p=0.026, VE/CS: p=0.013)., Conclusions: The shade stability of VITA Enamic crowns is superior to that of Lava Ultimate crowns. Only Lava Ultimate is affected by chewing simulation., (Copyright© 2018 Dennis Barber Ltd.)

Aim: The aim of this in vitro study was to evaluate the effect of accelerated artificial aging (AAA) and fatigue on the biaxial flexural strength (BFS) of three types of monolithic high-translucency zirconia restorations compared with conventional low-translucency zirconia restorations., Materials and Methods: Four groups of 20 disc-shaped specimens (10 × 1.2 mm) were made from the following computer-aided design and computer-aided manufacturing (CAD/CAM) zirconia blocks: Low-translucency zirconia (Ceramill ZI-LT) as a control, and three brands of high-translucent zirconia (Lava Plus, Ceramill Zolid White, and Copran Monolithic HT). Ten discs from each group were subjected to the BFS test using the universal testing machine. The other 10 discs from each group were subjected to AAA (thermocycling, 3,500 cycles) and fatigue (250,000 cycles) before the fracture test. The definitive fracture load was recorded, and the BFS was calculated in accordance with International Organization for Standardization (ISO) 6872. The data were analyzed with one-way analysis of variance (ANOVA), Scheffe post hoc, and Mann-Whitney U test. Data analyses were evaluated at a significance level of p < 0.05., Results: Significant differences were detected in the BFS among the four groups before AAA and fatigue. The mean BFS was highest with Ceramill ZI (935.3 ± 47.1 MPa), and least in Ceramill Zolid White (685.7 ± 32.6 MPa). After AAA and fatigue, significant differences were reported where the mean of BFS was highest with Copran Zr-i Monolithic HT (777.5 ± 21.2 MPa), and least in Ceramill Zolid White (576.0 ± 36.3 MPa). Furthermore, Mann-Whitney U test showed that AAA and fatigue significantly affect the BFS of each material individually., Conclusion: The AAA and fatigue significantly affected the BFS of the monolithic high-translucency zirconia restorations., Clinical Significance: Although monolithic high-translucency zirconia had significantly lower BFS than conventional zirconia tested in this study, they still have sufficient strength for clinical use.

Objectives: This study assessed the color stability of two composites associated with two pulp protectors submitted to accelerated artificial aging (AAA)., Methods: 60 test specimens were made with 0.5 mm of protection material (calcium hydroxide - CH or glass ionomer cement - GIC) and 2.5 mm of restoration material (Concept or QuixFil) and divided into 3 groups (n=10) according to the type of protection material/composite, and the control group (no protection). After polishing, color readings were obtained with a spectrophotometer (PCB 6807 Byk Gardner) before and after AAA for 384 hours, and L*, a*, and b* coordinates and total color variation (DeltaE) were analyzed (2-way ANOVA, Bonferroni, alpha=05)., Results: Composites placed on CH presented lower L* levels than those on GIC, which presented higher L* values than the control group and lower b* values than those of the CH group. The Concept composite presented higher DeltaE levels for all groups, differing statistically from QuixFil, except when placed on GIC., Conclusions: It was concluded that the protection material could affect the color stability and AAA is a factor that enhances this effect, depending on the type of composite used.