102 results on '"Christiane Maierhofer"'
Search Results
2. Ettringite via Mechanochemistry: A Green and Rapid Approach for Industrial Application
- Author
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Julia Stroh, Naveed Z. Ali, Christiane Maierhofer, and Franziska Emmerling
- Subjects
Chemistry ,QD1-999 - Published
- 2019
- Full Text
- View/download PDF
3. On the Registration of Thermographic In Situ Monitoring Data and Computed Tomography Reference Data in the Scope of Defect Prediction in Laser Powder Bed Fusion
- Author
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Simon Oster, Tobias Fritsch, Alexander Ulbricht, Gunther Mohr, Giovanni Bruno, Christiane Maierhofer, and Simon J. Altenburg
- Subjects
selective laser melting (SLM) ,laser powder bed fusion (L-PBF) ,additive manufacturing (AM) ,process monitoring ,infrared thermography ,X-ray micro computed tomography (XCT) ,Mining engineering. Metallurgy ,TN1-997 - Abstract
The detection of internal irregularities is crucial for quality assessment in metal-based additive manufacturing (AM) technologies such as laser powder bed fusion (L-PBF). The utilization of in-process thermography as an in situ monitoring tool in combination with post-process X-ray micro computed tomography (XCT) as a reference technique has shown great potential for this aim. Due to the small irregularity dimensions, a precise registration of the datasets is necessary as a requirement for correlation. In this study, the registration of thermography and XCT reference datasets of a cylindric specimen containing keyhole pores is carried out for the development of a porosity prediction model. The considered datasets show variations in shape, data type and dimensionality, especially due to shrinkage and material elevation effects present in the manufactured part. Since the resulting deformations are challenging for registration, a novel preprocessing methodology is introduced that involves an adaptive volume adjustment algorithm which is based on the porosity distribution in the specimen. Thus, the implementation of a simple three-dimensional image-to-image registration is enabled. The results demonstrate the influence of the part deformation on the resulting porosity location and the importance of registration in terms of irregularity prediction.
- Published
- 2022
- Full Text
- View/download PDF
4. Can Potential Defects in LPBF Be Healed from the Laser Exposure of Subsequent Layers? A Quantitative Study
- Author
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Alexander Ulbricht, Gunther Mohr, Simon J. Altenburg, Simon Oster, Christiane Maierhofer, and Giovanni Bruno
- Subjects
selective laser melting (SLM) ,additive manufacturing (AM) ,process monitoring ,infrared thermography ,optical tomography ,X-ray computed tomography (XCT) ,Mining engineering. Metallurgy ,TN1-997 - Abstract
Additive manufacturing (AM) of metals and in particular laser powder bed fusion (LPBF) enables a degree of freedom in design unparalleled by conventional subtractive methods. To ensure that the designed precision is matched by the produced LPBF parts, a full understanding of the interaction between the laser and the feedstock powder is needed. It has been shown that the laser also melts subjacent layers of material underneath. This effect plays a key role when designing small cavities or overhanging structures, because, in these cases, the material underneath is feed-stock powder. In this study, we quantify the extension of the melt pool during laser illumination of powder layers and the defect spatial distribution in a cylindrical specimen. During the LPBF process, several layers were intentionally not exposed to the laser beam at various locations, while the build process was monitored by thermography and optical tomography. The cylinder was finally scanned by X-ray computed tomography (XCT). To correlate the positions of the unmolten layers in the part, a staircase was manufactured around the cylinder for easier registration. The results show that healing among layers occurs if a scan strategy is applied, where the orientation of the hatches is changed for each subsequent layer. They also show that small pores and surface roughness of solidified material below a thick layer of unmolten material (>200 µm) serve as seeding points for larger voids. The orientation of the first two layers fully exposed after a thick layer of unmolten powder shapes the orientation of these voids, created by a lack of fusion.
- Published
- 2021
- Full Text
- View/download PDF
5. Experimental Determination of the Emissivity of Powder Layers and Bulk Material in Laser Powder Bed Fusion Using Infrared Thermography and Thermocouples
- Author
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Gunther Mohr, Susanna Nowakowski, Simon J. Altenburg, Christiane Maierhofer, and Kai Hilgenberg
- Subjects
laser powder bed fusion (L-PBF) ,selective laser melting (SLM) ,laser beam melting (LBM) ,thermography ,emissivity ,calibration ,Mining engineering. Metallurgy ,TN1-997 - Abstract
Recording the temperature distribution of the layer under construction during laser powder bed fusion (L-PBF) is of utmost interest for a deep process understanding as well as for quality assurance and in situ monitoring means. While having a notable number of thermal monitoring approaches in additive manufacturing (AM), attempts at temperature calibration and emissivity determination are relatively rare. This study aims for the experimental temperature adjustment of an off-axis infrared (IR) thermography setup used for in situ thermal data acquisition in L-PBF processes. The temperature adjustment was conducted by means of the so-called contact method using thermocouples at two different surface conditions and two different materials: AISI 316L L-PBF bulk surface, AISI 316L powder surface, and IN718 powder surface. The apparent emissivity values for the particular setup were determined. For the first time, also corrected, closer to real emissivity values of the bulk or powder surface condition are published. In the temperature region from approximately 150 °C to 580 °C, the corrected emissivity was determined in a range from 0.2 to 0.25 for a 316L L-PBF bulk surface, in a range from 0.37 to 0.45 for 316L powder layer, and in a range from 0.37 to 0.4 for IN718 powder layer.
- Published
- 2020
- Full Text
- View/download PDF
6. In-Situ Defect Detection in Laser Powder Bed Fusion by Using Thermography and Optical Tomography—Comparison to Computed Tomography
- Author
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Gunther Mohr, Simon J. Altenburg, Alexander Ulbricht, Philipp Heinrich, Daniel Baum, Christiane Maierhofer, and Kai Hilgenberg
- Subjects
laser powder bed fusion (l-pbf) ,selective laser melting (slm) ,additive manufacturing (am) ,process monitoring ,infrared thermography ,optical tomography ,computed tomography (ct) ,data fusion ,lack-of-fusion ,Mining engineering. Metallurgy ,TN1-997 - Abstract
Among additive manufacturing (AM) technologies, the laser powder bed fusion (L-PBF) is one of the most important technologies to produce metallic components. The layer-wise build-up of components and the complex process conditions increase the probability of the occurrence of defects. However, due to the iterative nature of its manufacturing process and in contrast to conventional manufacturing technologies such as casting, L-PBF offers unique opportunities for in-situ monitoring. In this study, two cameras were successfully tested simultaneously as a machine manufacturer independent process monitoring setup: a high-frequency infrared camera and a camera for long time exposure, working in the visible and infrared spectrum and equipped with a near infrared filter. An AISI 316L stainless steel specimen with integrated artificial defects has been monitored during the build. The acquired camera data was compared to data obtained by computed tomography. A promising and easy to use examination method for data analysis was developed and correlations between measured signals and defects were identified. Moreover, sources of possible data misinterpretation were specified. Lastly, attempts for automatic data analysis by data integration are presented.
- Published
- 2020
- Full Text
- View/download PDF
7. Detection of Typical Metal Additive Manufacturing Defects by the Application of Thermographic Techniques
- Author
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Ester D’Accardi, Simon Altenburg, Christiane Maierhofer, Davide Palumbo, and Umberto Galietti
- Subjects
Metal Additive Manufacturing ,Laser Powder Bed Fusion (L-PBF) ,Thermography ,General Works - Abstract
One of the most advanced technologies of Metal Additive Manufacturing (AM) is the Laser Powder Bed Fusion process (L-PBF), also known as Selective Laser Melting (SLM). This process involves the deposition and fusion, layer by layer, of very fine metal powders and structure and quality of the final component strongly depends on several processing parameters, for example the laser parameters. Due to the complexity of the process it is necessary to assure the absence of defects in the final component, in order to accept or discard it. Thermography is a very fast non-destructive testing (NDT) technique. Its applicability for defect detection in AM produced parts would significantly reduce costs and time required for NDT, making it versatile and very competitive.
- Published
- 2019
- Full Text
- View/download PDF
8. Vergleich der Messungen der Schmelzbadtemperatur bei der Additiven Fertigung von Metallen mittels IR-Spektroskopie und Thermografie
- Author
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Andrey Gumenyuk, Simon J. Altenburg, Igor B. Gornushkin, Christiane Maierhofer, Anne Straße, Nils Scheuschner, and Giuseppe Pignatelli
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Physics ,Electrical and Electronic Engineering ,Laser metal deposition ,Instrumentation ,Nuclear chemistry - Abstract
Zusammenfassung Im Rahmen des Themenfeldprojektes „Process Monitoring of AM“ (ProMoAM) evaluiert die Bundesanstalt für Materialforschung und -prüfung (BAM) gegenwärtig die Anwendbarkeit verschiedenster ZfP-Verfahren zur in-situ Prozessüberwachung in der additiven Fertigung (AM) von Metallen in Hinblick auf die Qualitätssicherung. Einige der wichtigsten Messgrößen sind hierbei die Temperatur des Schmelzbades und die Abkühlrate, welche starken Einfluss auf das Gefüge und die Eigenspannung haben. Aufgrund der Zugänglichkeit zum Werkstück während des Bauprozesses bieten sich optische Verfahren zu Temperaturbestimmung an. Hierbei stellen jedoch u. a. die hohe Bandbreite der zu messenden Temperaturen, die Bestimmung der Emissivität und ihre Änderung bei Phasenübergängen der verwendeten Legierung große experimentelle Herausforderungen dar. Eine weitere Herausforderung stellt für die IR-Spektroskopie die Absorption durch das Schutzgas und weitere optische Elemente dar. Um diese auch in einem industriellen Umfeld kompensieren zu können, wurde eine Methode entwickelt, die das gemessene Spektrum bei der Verfestigung des Werkstoffes als Referenz nutzt. In diesem Beitrag wird die Anwendung dieser Methode für die IR-Spektrometrie als auch Thermografische Messungen beim Laser-Pulver-Auftragschweißen von 316L gezeigt, wobei beide Methoden weiterhin in Hinblick auf ihre individuellen Vor- und Nachteile miteinander verglichen werden.
- Published
- 2021
9. Can Potential Defects in LPBF Be Healed from the Laser Exposure of Subsequent Layers? A Quantitative Study
- Author
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Christiane Maierhofer, Simon Oster, Alexander Ulbricht, Giovanni Bruno, Gunther Mohr, and Simon J. Altenburg
- Subjects
Materials science ,additive manufacturing (AM) ,02 engineering and technology ,optical tomography ,01 natural sciences ,law.invention ,process monitoring ,law ,0103 physical sciences ,medicine ,Surface roughness ,Cylinder ,General Materials Science ,Composite material ,Optical tomography ,010302 applied physics ,X-ray computed tomography (XCT) ,Fusion ,Mining engineering. Metallurgy ,medicine.diagnostic_test ,in situ monitoring ,Orientation (computer vision) ,Metals and Alloys ,TN1-997 ,021001 nanoscience & nanotechnology ,Laser ,healing ,Thermography ,infrared thermography ,ddc:620 ,0210 nano-technology ,selective laser melting (SLM) ,Layer (electronics) - Abstract
Additive manufacturing (AM) of metals and in particular laser powder bed fusion (LPBF) enables a degree of freedom in design unparalleled by conventional subtractive methods. To ensure that the designed precision is matched by the produced LPBF parts, a full understanding of the interaction between the laser and the feedstock powder is needed. It has been shown that the laser also melts subjacent layers of material underneath. This effect plays a key role when designing small cavities or overhanging structures, because, in these cases, the material underneath is feed-stock powder. In this study, we quantify the extension of the melt pool during laser illumination of powder layers and the defect spatial distribution in a cylindrical specimen. During the LPBF process, several layers were intentionally not exposed to the laser beam at various locations, while the build process was monitored by thermography and optical tomography. The cylinder was finally scanned by X-ray computed tomography (XCT). To correlate the positions of the unmolten layers in the part, a staircase was manufactured around the cylinder for easier registration. The results show that healing among layers occurs if a scan strategy is applied, where the orientation of the hatches is changed for each subsequent layer. They also show that small pores and surface roughness of solidified material below a thick layer of unmolten material (>, 200 µm) serve as seeding points for larger voids. The orientation of the first two layers fully exposed after a thick layer of unmolten powder shapes the orientation of these voids, created by a lack of fusion.
- Published
- 2021
- Full Text
- View/download PDF
10. Active thermography for quality assurance of 3D-printed polymer structures
- Author
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Christiane Maierhofer, Christian Metz, Philipp Franz, Volker Wachtendorf, and Christian Fischer
- Subjects
0209 industrial biotechnology ,3d printed ,Materials science ,02 engineering and technology ,Impulse (physics) ,law.invention ,chemistry.chemical_compound ,020901 industrial engineering & automation ,Ultraviolet visible spectroscopy ,law ,Thermal ,Electrical and Electronic Engineering ,Composite material ,Instrumentation ,chemistry.chemical_classification ,business.industry ,Acrylonitrile butadiene styrene ,Polymer ,021001 nanoscience & nanotechnology ,Selective laser sintering ,chemistry ,Flash (manufacturing) ,Thermography ,Polyamide ,0210 nano-technology ,business ,Quality assurance - Abstract
Additively manufactured test specimens made of polyamide 12 (PA 12) by Laser Sintering (LS) as well as of acrylnitril-butadien-styrol (ABS) by Fused Layer Modeling (FLM), were tested with active thermography. For this, two different excitation methods (flash and impulse excitation) were used and compared, regarding the suitability for the detection of constructed and imprinted defects. To increase the quality of the thermograms, data processing methods like thermal signal reconstruction (TSR) and Fourier-Transformation were applied. Furthermore, the long-term stability of the probes towards environmental stress, like UV-radiation, heat, water contact and frost is being investigated in the presented project with artificial weathering tests.
- Published
- 2019
11. Investigation of the thermal history of L-PBF metal parts by feature extraction from in-situ SWIR thermography
- Author
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Kai Hilgenberg, Simon Oster, Christiane Maierhofer, Alexander Ulbricht, Gunther Mohr, and Simon J. Altenburg
- Subjects
Fusion ,Materials science ,business.industry ,Thermal ,Thermography ,Feature extraction ,Process (computing) ,Mechanical engineering ,Porosity ,business ,Quality assurance ,Near net shape - Abstract
Laser powder bed fusion is used to create near net shape metal parts with a high degree of freedom in geometry design. When it comes to the production of safety critical components, a strict quality assurance is mandatory. An alternative to cost-intensive non-destructive testing of the produced parts is the utilization of in-situ process monitoring techniques. The formation of defects is linked to deviations of the local thermal history of the part from standard conditions. Therefore, one of the most promising monitoring techniques in additive manufacturing is thermography. In this study, features extracted from thermographic data are utilized to investigate the thermal history of cylindrical metal parts. The influence of process parameters, part geometry and scan strategy on the local heat distribution and on the resulting part porosity are presented. The suitability of the extracted features for in-situ process monitoring is discussed.
- Published
- 2021
12. Towards the determination of real process temperatures in the LMD process by multispectral thermography
- Author
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Christiane Maierhofer, Nils Scheuschner, Anne Straße, Simon J. Altenburg, and Andrey Gumenyuk
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Wavelength ,Materials science ,Optics ,business.industry ,Thermal radiation ,Thermal ,Thermography ,Multispectral image ,Emissivity ,Thermodynamic temperature ,business ,Intensity (heat transfer) - Abstract
Additive manufacturing of metals offers the opportunity to build parts with a high degree of complexity without additional costs, opening a new space for design optimization. However, the processes are highly complex and due to the rapid thermal cycles involved, high internal stresses and peculiar microstructures arise, which influence the parts mechanical properties. To systematically examine the formation of internal stresses and the microstructure, in-process spatially resolved measurements of the part temperature are needed. Usually, thermography is used to measure temporally resolved thermal fields. The thermal cameras are calibrated at black body reference radiators (unity emissivity) for the conversion of the measured thermal radiation intensity to temperatures. If the emissivity of the inspected part is known, its thermodynamic temperature can be reconstructed by a suited radiometric model. However, in additive manufacturing of metals, the emissivity of the part surface is strongly inhomogeneous and rapidly changing due to variations of, e.g., the degree of oxidation, the material state and temperature. However, measuring the process thermal radiation at different wavelengths simultaneously enables one to separate temperature and emissivity spatially resolved to obtain further insight into the process. Here, we present results of a study using multispectral thermography to obtain real temperatures and emissivities in the laser metal deposition (LMD) process. For a better understanding of the basic processes, the measurements have been performed first without powder supply and by recording images at different wavelength in subsequent runs.
- Published
- 2021
13. In Situ Real-Time Monitoring Versus Post NDE for Quality Assurance of Additively Manufactured Metal Parts
- Author
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Christiane Maierhofer, Simon J. Altenburg, and Nils Scheuschner
- Subjects
In situ ,Materials science ,business.industry ,business ,Process engineering ,Quality assurance - Published
- 2021
14. Experimental Determination of the Emissivity of Powder Layers and Bulk Material in Laser Powder Bed Fusion Using Infrared Thermography and Thermocouples
- Author
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Kai Hilgenberg, Simon J. Altenburg, Christiane Maierhofer, Gunther Mohr, and Susanna Nowakowski
- Subjects
lcsh:TN1-997 ,0209 industrial biotechnology ,Materials science ,Infrared ,02 engineering and technology ,law.invention ,020901 industrial engineering & automation ,process monitoring ,law ,Thermocouple ,316L ,Thermal ,Calibration ,Emissivity ,laser powder bed fusion (L‑PBF) ,General Materials Science ,Composite material ,laser beam melting (LBM) ,lcsh:Mining engineering. Metallurgy ,Metals and Alloys ,IN718 ,021001 nanoscience & nanotechnology ,Laser ,calibration ,thermography ,thermocouples ,emissivity ,Thermography ,ddc:620 ,0210 nano-technology ,selective laser melting (SLM) ,Layer (electronics) ,ddc:600 - Abstract
Recording the temperature distribution of the layer under construction during laser powder bed fusion (L-PBF) is of utmost interest for a deep process understanding as well as for quality assurance and in situ monitoring means. While having a notable number of thermal monitoring approaches in additive manufacturing (AM), attempts at temperature calibration and emissivity determination are relatively rare. This study aims for the experimental temperature adjustment of an off-axis infrared (IR) thermography setup used for in situ thermal data acquisition in L-PBF processes. The temperature adjustment was conducted by means of the so-called contact method using thermocouples at two different surface conditions and two different materials: AISI 316L L-PBF bulk surface, AISI 316L powder surface, and IN718 powder surface. The apparent emissivity values for the particular setup were determined. For the first time, also corrected, closer to real emissivity values of the bulk or powder surface condition are published. In the temperature region from approximately 150 °, C to 580 °, C, the corrected emissivity was determined in a range from 0.2 to 0.25 for a 316L L-PBF bulk surface, in a range from 0.37 to 0.45 for 316L powder layer, and in a range from 0.37 to 0.4 for IN718 powder layer.
- Published
- 2020
15. Zerstörungsfreie Prüfung von Werkstoffen und Bauteilen
- Author
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Gerd Dobmann and Christiane Maierhofer
- Published
- 2020
16. Quantification of Delaminations in Semitransparent Solids Using Pulsed Thermography and Mathematical 1D Models
- Author
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Simon J. Altenburg, Raphael Bernegger, and Christiane Maierhofer
- Subjects
Thermal contact conductance ,Materials science ,Opacity ,Computer simulation ,Mathematical model ,Delamination ,02 engineering and technology ,021001 nanoscience & nanotechnology ,Condensed Matter Physics ,01 natural sciences ,010309 optics ,0103 physical sciences ,Thermography ,Thermal ,Composite material ,0210 nano-technology ,Material properties - Abstract
Material defects in fiber-reinforced polymers such as delaminations can rapidly degrade the material properties or can lead to the failure of a component. Pulse thermography (PT) has proven to be a valuable tool to identify and quantify such defects in opaque materials. However, quantification of delaminations within semitransparent materials is extremely challenging. We present an approach to quantify delaminations within materials being semitransparent within the wavelength ranges of the optical excitation sources as well as of the infrared (IR) camera. PT experimental data of a glass fiber-reinforced polymer with a real delamination within the material were reconstructed by one-dimensional (1D) mathematical models. These models describe the heat diffusion within the material and consider semitransparency to the excitation source as well to the IR camera, thermal losses at the samples surfaces and a thermal contact resistance between the two layers describing the delamination. By fitting the models to the PT data, we were able to determine the depth of the delamination very accurately. Additionally, we analyzed synthetic PT data from a 2D simulation with our 1D-models to show how the thermal contact resistance is influenced by lateral heat flow within the material.
- Published
- 2020
17. Detecting Delaminations in Semitransparent Glass Fiber Composite by Using Pulsed Infrared Thermography
- Author
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Vladimir P. Vavilov, Raphael Bernegger, Arsenii Chulkov, A.I. Moskovchenko, and Christiane Maierhofer
- Subjects
Materials science ,Opacity ,Laser heating ,business.industry ,Mechanical Engineering ,Glass fiber ,Composite number ,Fibre-reinforced plastic ,Laser ,law.invention ,Mechanics of Materials ,law ,Semi-transparent composite ,Nondestructive testing ,GFRP ,Thermography ,Infrared thermography ,Optical radiation ,Composite material ,Thermal testing ,business - Abstract
Thanks to its good strength/mass ratio, a glass fibre reinforced plastic (GFRP) composite is a common material widely used in aviation, power production, automotive and other industries. In its turn, active infrared (IR) nondestructive testing (NDT) is a common inspection technique for detecting and characterizing structural defects in GFRP. Materials to be tested are typically subjected to optical heating which is supposed to occur on the material surface. However, GFRP composite is semi-transparent for optical radiation of both visual and IR spectral bands. Correspondingly, the inspection process represents a certain combination of both optical and thermal phenomena. Therefore, the known characterization algorithms based on pure heat diffusion cannot be applied to semi-transparent materials. In this study, the phenomenon of GFRP semi-transparency has been investigated numerically and experimentally in application to thermal NDT. Both Xenon flash tubes and a laser have been used for thermal stimulation of opaque and semi-transparent test objects. It has been shown that the penetration of optical heating radiation into composite reduces detectability of shallower defects, and the signal-to-noise ratio can be enhanced by applying the technique of thermographic signal reconstruction (TSR). In the inspection of the semi-transparent GFRP composite, the most efficient has been the laser heating followed by the TSR data processing. The perspectives of defect characterization of semi-transparent materials by using laser heating are discussed. A neural network has been used as a candidate tool for evaluating defect depth in composite materials, but its training should be performed in identical with testing conditions.
- Published
- 2020
18. Thermography in laser powder bed fusion of metals: time over threshold as feasible feature in thermographic data
- Author
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Simon J. Altenburg, Nils Scheuschner, Christiane Maierhofer, Gunther Mohr, and Kai Hilgenberg
- Subjects
Fusion ,Cuboid ,Materials science ,Threshold limit value ,business.industry ,Laser ,law.invention ,Optics ,Feature (computer vision) ,law ,Thermal ,Thermography ,business ,Focus (optics) - Abstract
Thermography is one on the most promising techniques for in-situ monitoring of metal additive manufacturing processes. Especially in laser powder bed fusion processes, the high process dynamics and the strong focus of the laser beam cause a very complex thermal history within the produced specimens, such as multiple heating cycles within single layer expositions. This complicates data interpretation, e.g., in terms of cooling rates. A quantity that is easily calculated is the time a specific area of the specimen is at a temperature above a chosen threshold value (TOT). Here, we discuss variations occurring in time-over-threshold-maps during manufacturing of an almost defect free cuboid specimen.
- Published
- 2020
19. In-situ-Untersuchungen mechanochemischer Eintopfreaktionen
- Author
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Hannes Kulla, Mathias Röllig, Klaus Rademann, Sebastian Haferkamp, Irina Akhmetova, Franziska Emmerling, and Christiane Maierhofer
- Subjects
Materials science ,010405 organic chemistry ,General Medicine ,010402 general chemistry ,01 natural sciences ,0104 chemical sciences - Published
- 2018
20. In Situ Investigations of Mechanochemical One-Pot Syntheses
- Author
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Sebastian Haferkamp, Irina Akhmetova, Klaus Rademann, Mathias Röllig, Hannes Kulla, Christiane Maierhofer, and Franziska Emmerling
- Subjects
Standard enthalpy of reaction ,Reaction mechanism ,Materials science ,010405 organic chemistry ,General Chemistry ,010402 general chemistry ,01 natural sciences ,Cocrystal ,Catalysis ,0104 chemical sciences ,law.invention ,Chemical kinetics ,symbols.namesake ,Chemical engineering ,law ,Mechanochemistry ,symbols ,Knoevenagel condensation ,Crystallization ,Raman spectroscopy - Abstract
We present an in situ triple coupling of synchrotron X-ray diffraction with Raman spectroscopy, and thermography to study milling reactions in real time. This combination of methods allows a correlation of the structural evolution with temperature information. The temperature information is crucial for understanding both the thermodynamics and reaction kinetics. The reaction mechanisms of three prototypical mechanochemical syntheses, a cocrystal formation, a C@C bond formation (Knoevenagel condensation), and the formation of a manganese-phosphonate, were elucidated. Trends in the temperature development during milling are identified. The heat of reaction and latent heat of crystallization of the product contribute to the overall temperature increase. A decrease in temperature occurs via release of, for example, water as a byproduct. Solid and liquid intermediates are detected. The influence of the mechanical impact could be separated from temperature effects caused by the reaction.
- Published
- 2018
21. Einfluss thermischer und optischer Materialeigenschaften auf die Charakterisierung von Fehlstellen in Faserverbundwerkstoffen mit aktiven Thermografieverfahren
- Author
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Alper Aktas, M J Lodeiro, Berndt Gutschwager, G. Baker, Christiane Maierhofer, Christian Monte, Mathias Röllig, Albert Adibekyan, Sreedhar Unnikrishnakurup, Rainer Krankenhagen, Lenka Knazowicka, M. Gower, and Ales Blahut
- Subjects
010309 optics ,Physics ,020401 chemical engineering ,0103 physical sciences ,Analytical chemistry ,02 engineering and technology ,0204 chemical engineering ,Electrical and Electronic Engineering ,01 natural sciences ,Instrumentation - Abstract
Zusammenfassung In diesem Beitrag werden zerstörungsfreie Untersuchungen mittels aktiver Thermografie an Probekörpern aus CFK und GFK mit unterschiedlichen künstlichen Fehlstellen vorgestellt. Dabei wird die zeitliche und örtliche Temperaturverteilung nach der Erwärmung mit Blitzlampen oder mit einem Infrarot-Strahler mit einer Infrarot-Kamera erfasst. Zur späteren Rekonstruktion der Messdaten wurde ein numerisches Modell entwickelt. Dazu war die Bestimmung der thermophysikalischen und optischen Materialeigenschaften erforderlich, was in diesem Beitrag ebenfalls beschrieben wird. Die Ergebnisse der numerischen Modellierung werden mit den experimentellen Untersuchungen der aktiven Thermografie verglichen. Weiterhin werden die experimentellen Untersuchungen hinsichtlich der beiden Materialsysteme CFK und GFK und unter Berücksichtigung der Teiltransparenz des GFK-Materials sowie der unterschiedlichen Anregungsquellen bewertet.
- Published
- 2017
22. Defect characterisation of tensile loaded CFRP and GFRP laminates used in energy applications by means of infrared thermography
- Author
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Alper Aktas, Birgit Rehmer, M J Lodeiro, Rainer Krankenhagen, Christiane Maierhofer, G. Baker, Mathias Röllig, Bernd Gutschwager, Albert Adibekyan, Christian Monte, and M. Gower
- Subjects
Materials science ,Turbine blade ,Infrared ,Delamination ,02 engineering and technology ,Fibre-reinforced plastic ,021001 nanoscience & nanotechnology ,law.invention ,020303 mechanical engineering & transports ,0203 mechanical engineering ,law ,Ultimate tensile strength ,Thermography ,Electrical and Electronic Engineering ,Composite material ,0210 nano-technology ,Instrumentation ,Energy (signal processing) - Abstract
The increased use of fibre reinforced plastic (FRP) composites for improved efficiency and reliability in energy related applications, e.g. wind and marine turbine blades, nacelles, oil and gas fle...
- Published
- 2017
23. Warming up for mechanosynthesis – temperature development in ball mills during synthesis
- Author
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Franziska Emmerling, Christiane Maierhofer, Hannes Kulla, Franziska Fischer, Manuel Wilke, and Mathias Röllig
- Subjects
010405 organic chemistry ,Chemistry ,Mechanical impact ,technology, industry, and agriculture ,Metals and Alloys ,food and beverages ,Thermodynamics ,Nanotechnology ,Hot spot (veterinary medicine) ,General Chemistry ,Plasma ,010402 general chemistry ,01 natural sciences ,Catalysis ,0104 chemical sciences ,Surfaces, Coatings and Films ,Electronic, Optical and Magnetic Materials ,Magma ,Materials Chemistry ,Ceramics and Composites ,Mechanosynthesis ,Soft matter ,Ball mill ,Warming up - Abstract
We present a first direct measurement of the temperature during milling combined with in situ Raman spectroscopy monitoring. The data reveal a low temperature increase due to the mechanical impact and clear temperature increases as a consequence of the reaction heat. Based on the data, temperature rises as postulated in the magma plasma and hot spot theory can be excluded for soft matter milling syntheses.
- Published
- 2017
24. Iterative numerical 2D-modelling for quantification of material defects by pulsed thermography
- Author
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Christiane Maierhofer, Simon J. Altenburg, and Raphael Bernegger
- Subjects
Materials science ,Opacity ,Computer simulation ,law ,Region of interest ,Acoustics ,Thermography ,Thermal ,Impulse (physics) ,Radiation ,Laser ,law.invention - Abstract
This paper presents a method to quantify the geometry of defects such as flat bottom holes (FBH) and notches in opaque materials by a pulse thermography (PT) experiment and a numerical model. The aim was to precisely describe PT experiments in reflection configuration with a simple and fast numerical model in order to use this model and a fit algorithm to quantify defects within the material. The algorithm minimizes the difference between the time sequence of a line shaped region of interest (ROI) on the surface (above the defect) from the PT experiment and the numerical data. Therefore, the experimental data can be reconstructed with the numerical model. In this way, the defect depth of a notch or FBH and its width or diameter was determined simultaneously. A laser was used for heating which was widened to a top hat spatial profile to ensure homogeneous illumination (rectangular impulse profile in time). The numerical simulation considers heating conditions and takes thermal losses due to convection and radiation into account. We quantified the geometry of FBH and notches in steel and polyvinyl chloride plasticized (PVC-U) materials with an accuracy of < 5 %.
- Published
- 2019
25. Probability of detection analysis of round robin test results performed by flash thermography
- Author
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J. Koch, F. Hohlstein, Günter Walle, Matthias Goldammer, Igor Kryukov, Nick Rothbart, M. Sengebusch, Beate Oswald-Tranta, G. Mahler, Bernhard Stotter, Christiane Maierhofer, and Publica
- Subjects
round robin test ,010302 applied physics ,Scope (project management) ,Computer science ,Comparability ,flash excitation ,02 engineering and technology ,multiparameter POD ,021001 nanoscience & nanotechnology ,01 natural sciences ,Statistical power ,active thermography ,Reliability engineering ,Flash (photography) ,Signal-to-noise ratio ,0103 physical sciences ,Thermography ,signal-to-noise ratio ,Round robin test ,Electrical and Electronic Engineering ,0210 nano-technology ,Instrumentation ,Reliability (statistics) - Abstract
Within the scope of a standardisation research project, a flash thermography round robin test that evaluates reliability, comparability and efficiency of different testing situations was performed. Data recorded at metal test specimens with flat bottom holes (FBHs) were analysed by calculating the signal-to-noise ratio (SNR) of the defect signatures in the thermograms as well as in the phase images as a function of defect parameters. A new multi-parameter probability of detection (POD) model was developed, where an a versus a continuous signal analysis was based on the linear relationship between the SNR and a multi-parameter a. This linear relationship was verified by comparison to data obtained from an analytical model that is considering lateral thermal heat diffusion as well as to data obtained by numerical simulation. The resulting POD curves for the thermograms and phase images give an estimation for the detectability of the FBHs with known geometry in steel using different equipment and obtained by different participants. By comparing the SNRs of FBHs with similar geometries, this POD model was transferred to aluminium and copper as well.
- Published
- 2016
26. Comparison of concepts for a point-shaped energy density detector after flash lamp excitation
- Author
-
Christiane Maierhofer and Rainer Krankenhagen
- Subjects
010302 applied physics ,Flash-lamp ,Chemistry ,business.industry ,Mechanical Engineering ,Detector ,Dissipation ,01 natural sciences ,Laser flash analysis ,010309 optics ,Flash (photography) ,Mechanics of Materials ,0103 physical sciences ,Thermal ,Thermography ,Optoelectronics ,General Materials Science ,business ,Energy source - Abstract
The paper describes investigations and research work in order to develop a simple sensor for the quantification of spectral broadband energy dissipation of flash lamps at any point in space. Such flash lamps are often used as energy source during active thermography testing (TT). Here, the temperature transient of the sensor surface has to be recorded by the infrared camera that is already present. During the following data evaluation, the energy input into the investigated specimen can be determined. Two opposite concepts were considered: thermal thick and thermal thin probes. The direct comparison shows advantages for thermal thick probes based on the physics of thermal balance processes.
- Published
- 2016
27. Thermographic inspection of a wind turbine rotor blade segment utilizing natural conditions as excitation source, Part I: Solar excitation for detecting deep structures in GFRP
- Author
-
Henrik Steinfurth, Tamara Worzewski, Manoucher Doroshtnasir, Rainer Krankenhagen, Mathias Röllig, and Christiane Maierhofer
- Subjects
Materials science ,Computer simulation ,Rotor (electric) ,business.industry ,Acoustics ,02 engineering and technology ,Fibre-reinforced plastic ,021001 nanoscience & nanotechnology ,Condensed Matter Physics ,01 natural sciences ,Atomic and Molecular Physics, and Optics ,Electronic, Optical and Magnetic Materials ,Thermographic inspection ,law.invention ,010309 optics ,law ,Nondestructive testing ,0103 physical sciences ,Thermography ,Structural health monitoring ,0210 nano-technology ,business ,Excitation - Abstract
This study evaluates whether subsurface features in rotor blades, mainly made of Glass Fibre Reinforced Plastics (GFRP), can generally be detected with “solar thermography”. First, the suitability of the sun is tested for acting as a heat source for applying active thermography on a 30 mm thick GFRP test specimen. Second, a defective rotor blade segment is inspected outdoors under ideal natural conditions using the sun as excitation source. Additionally, numerical FEM-simulations are performed and the comparability between experiment and simulation is evaluated for outdoor measurements.
- Published
- 2016
28. Parameters in lock-in thermography of CFRP laminates
- Author
-
Philipp Myrach, Christiane Maierhofer, Markus Rahammer, and Marc Kreutzbruck
- Subjects
Carbon fiber reinforced polymers ,Materials science ,business.industry ,Mechanical Engineering ,02 engineering and technology ,021001 nanoscience & nanotechnology ,Ultrasonic excitation ,Power (physics) ,020303 mechanical engineering & transports ,0203 mechanical engineering ,Mechanics of Materials ,Nondestructive testing ,Thermal ,Thermography ,General Materials Science ,Ultrasonic sensor ,Composite material ,0210 nano-technology ,business ,Excitation - Abstract
Active thermography with lock-in excitation is a nondestructive testing method that is also feasible for testing of carbon fiber reinforced polymers (CFRP). For validating the method extensive investigations were done during a research project in order to advance a standardization process. The most important parameters of optical and ultrasonic excitation thermography were investigated. For example, the appropriate selection of spectral sensitivity of the used infrared camera systems is important for recording undisturbed thermal signals. Regarding excitation, influences of excitation power and ultrasonic frequency were studied. Furthermore, material parameters such as CFRP layup are known for strongly affecting the results of measurement.
- Published
- 2016
29. Detection and Characterization of Defects in Isotropic and Anisotropic Structures Using Lockin Thermography
- Author
-
Philipp Myrach, Mathias Röllig, Rainer Krankenhagen, Henrik Steinfurth, and Christiane Maierhofer
- Subjects
lateral resolution ,Materials science ,business.industry ,amplitude images ,Isotropy ,non-destructive testing ,lockin thermography ,Carbon Fiber Reinforced Plastic (CFRP) ,Fibre-reinforced plastic ,Computer Graphics and Computer-Aided Design ,Characterization (materials science) ,Optics ,Amplitude ,Signal-to-Noise Ratio (SNR) ,Nondestructive testing ,Thermography ,Radiology, Nuclear Medicine and imaging ,steel ,Computer Vision and Pattern Recognition ,phase images ,Electrical and Electronic Engineering ,Anisotropy ,business ,Image resolution - Abstract
Lockin thermography is a well-suited method for the characterization of structures made of both metal and fiber reinforced plastic. In most cases, only phase images are analyzed, although the amplitude images might contain useful information as well. Thus, systematic studies of lockin thermography are presented, assessing amplitude and phase images for the detection and quantification of defects in isotropic (steel) and anisotropic (carbon fiber reinforced plastic) materials. Characterized defects are flat bottom holes with different diameters and various remaining wall thicknesses as well as crossed notches at different depths. The excitation frequency was varied while keeping the number of analyzed excitation periods nearly constant for each material. The data analysis was focused on the detectability of the defects both in the amplitude and phase images, including the determination of the signal-to-noise ratio and of the spatial resolution. As a result, the limits of defect detectability and spatial resolution are given for each material.
- Published
- 2015
30. In-Situ Defect Detection in Laser Powder Bed Fusion by Using Thermography and Optical Tomography—Comparison to Computed Tomography
- Author
-
Philipp Heinrich, Simon J. Altenburg, Christiane Maierhofer, Kai Hilgenberg, Daniel Baum, Gunther Mohr, and Alexander Ulbricht
- Subjects
lcsh:TN1-997 ,0209 industrial biotechnology ,Materials science ,Infrared ,ComputingMethodologies_IMAGEPROCESSINGANDCOMPUTERVISION ,additive manufacturing (AM) ,02 engineering and technology ,computed tomography (CT) ,optical tomography ,law.invention ,process monitoring ,020901 industrial engineering & automation ,Optics ,law ,medicine ,General Materials Science ,laser powder bed fusion (L-PBF) ,Optical tomography ,lcsh:Mining engineering. Metallurgy ,lack-of-fusion ,data fusion ,medicine.diagnostic_test ,business.industry ,Near-infrared spectroscopy ,Metals and Alloys ,Filter (signal processing) ,021001 nanoscience & nanotechnology ,Laser ,Sensor fusion ,Casting ,infrared thermography ,Thermography ,ddc:620 ,selective laser melting (SLM) ,0210 nano-technology ,business - Abstract
Among additive manufacturing (AM) technologies, the laser powder bed fusion (L-PBF) is one of the most important technologies to produce metallic components. The layer-wise build-up of components and the complex process conditions increase the probability of the occurrence of defects. However, due to the iterative nature of its manufacturing process and in contrast to conventional manufacturing technologies such as casting, L-PBF offers unique opportunities for in-situ monitoring. In this study, two cameras were successfully tested simultaneously as a machine manufacturer independent process monitoring setup: a high-frequency infrared camera and a camera for long time exposure, working in the visible and infrared spectrum and equipped with a near infrared filter. An AISI 316L stainless steel specimen with integrated artificial defects has been monitored during the build. The acquired camera data was compared to data obtained by computed tomography. A promising and easy to use examination method for data analysis was developed and correlations between measured signals and defects were identified. Moreover, sources of possible data misinterpretation were specified. Lastly, attempts for automatic data analysis by data integration are presented.
- Published
- 2020
31. Evaluation of Different Techniques of Active Thermography for Quantification of Artificial Defects in Fiber-Reinforced Composites Using Thermal and Phase Contrast Data Analysis
- Author
-
Berndt Gutschwager, Michael R.L. Gower, Christiane Maierhofer, Ales Blahut, Lenka Knazowicka, G. Baker, Albert Adibekyan, Christian Monte, Mathias Röllig, and M J Lodeiro
- Subjects
010302 applied physics ,Chassis ,Materials science ,Glass fiber ,02 engineering and technology ,Fiber-reinforced composite ,Epoxy ,Fibre-reinforced plastic ,021001 nanoscience & nanotechnology ,Condensed Matter Physics ,01 natural sciences ,Shearography ,visual_art ,0103 physical sciences ,Thermography ,visual_art.visual_art_medium ,Fiber ,Composite material ,0210 nano-technology - Abstract
For assuring the safety and reliability of components and constructions in energy applications made of fiber-reinforced polymers (e.g., blades of wind turbines and tidal power plants, engine chassis, flexible oil and gas pipelines) innovative non-destructive testing methods are required. Within the European project VITCEA complementary methods (shearography, microwave, ultrasonics and thermography) have been further developed and validated. Together with partners from the industry, test specimens have been constructed and selected on-site containing different artificial and natural defect artefacts. As base materials, carbon and glass fibers in different orientations and layering embedded in different matrix materials (epoxy, polyamide) have been considered. In this contribution, the validation of flash and lock-in thermography to these testing problems is presented. Data analysis is based on thermal contrasts and phase evaluation techniques. Experimental data are compared to analytical and numerical models. Among others, the influence of two different types of artificial defects (flat bottom holes and delaminations) with varying diameters and depths and of two different materials (CFRP and GFRP) with unidirectional and quasi-isotropic fiber alignment is discussed.
- Published
- 2018
32. Applicability of a 1D Analytical Model for Pulse Thermography of Laterally Heterogeneous Semitransparent Materials
- Author
-
Raphael Bernegger, Christiane Maierhofer, Simon J. Altenburg, and Mathias Röllig
- Subjects
Thermal contact conductance ,chemistry.chemical_classification ,Materials science ,02 engineering and technology ,Polymer ,Fibre-reinforced plastic ,021001 nanoscience & nanotechnology ,Condensed Matter Physics ,01 natural sciences ,Characterization (materials science) ,010309 optics ,chemistry ,Attenuation coefficient ,0103 physical sciences ,Thermal ,Heat equation ,Composite material ,0210 nano-technology ,Excitation - Abstract
Pulse thermography (PT) has proven to be a valuable non-destructive testing method to identify and quantify defects in fiber-reinforced polymers. To perform a quantitative defect characterization, the heat diffusion within the material as well as the material parameters must be known. The heterogeneous material structure of glass fiber-reinforced polymers (GFRP) as well as the semitransparency of the material for optical excitation sources of PT is still challenging. For homogeneous semitransparent materials, 1D analytical models describing the temperature distribution are available. Here, we present an analytical approach to model PT for laterally inhomogeneous semitransparent materials. We show the validity of the model by considering different configurations of the optical heating source, the IR camera, and the differently coated GFRP sample. The model considers the lateral inhomogeneity of the semitransparency by an additional absorption coefficient. It includes additional effects such as thermal losses at the samples surfaces, multilayer systems with thermal contact resistance, and a finite duration of the heating pulse. By using a sufficient complexity of the analytical model, similar values of the material parameters were found for all six investigated configurations by numerical fitting.
- Published
- 2018
33. Quantification of impact damages in CFRP and GFRP structures with thermography and ultrasonics
- Author
-
Daniel Brackrock, Christiane Maierhofer, Mathias Röllig, Mate Gaal, Rainer Krankenhagen, and Thomas Heckel
- Subjects
Materials science ,business.industry ,Nondestructive testing ,Composite number ,Thermography ,Impact energy ,Damages ,High temporal resolution ,Fibre-reinforced plastic ,Composite material ,business - Abstract
The extent of damage caused by impacts in fibre reinforced composites depends on the energy of the impacts, on the velocity and the shape of the impacting body, on the material and structure of the composite and on the geometry of the structure. Here, mainly the thickness of the component is essential. The non-destructive evaluation of these damages can be carried out using both ultrasound and active thermography methods. A comparison of the detection sensitivity of these methods for the different damages is carried out in this paper depending on the fibre composite material used (CFRP and GFRP), the thickness of the material and the impact energy. The NDT methods used after the damage are supplemented by thermographic measurements with high temporal resolution, which were already recorded during the impact.
- Published
- 2018
34. Comparison of MWIR thermography and high-speed NIR thermography in a laser metal deposition (LMD) process
- Author
-
Christiane Maierhofer, Andrey Gumenyuk, Simon J. Altenburg, and Anne Straße
- Subjects
Reliability (semiconductor) ,Materials science ,Band-pass filter ,business.industry ,Manufacturing process ,Thermography ,Process (computing) ,Optoelectronics ,Laser metal deposition ,business ,Durability ,Visible spectrum - Abstract
Additive manufacturing (AM) offers a range of novel applications. However, the manufacturing process is complex and the production of defect-free parts with high reliability and durability is still a challenge. Thermography is a valuable tool for process surveillance, especially in metal AM processes. The high process temperatures allow one to use cameras usually operating in the visible spectral range. Here, we compare the results of measurements during the manufacturing process of a commercial laser metal deposition setup using a mid-wavelength-IR camera with those from a visual spectrum high-speed camera with band pass filter in the near-IR range.
- Published
- 2018
35. Systematic errors in the evaluation of uncorrected data from thermographic lock-in measurements
- Author
-
Christiane Maierhofer, Rainer Krankenhagen, and Mathias Ziegler
- Subjects
Harmonic analysis ,Materials science ,Amplitude ,business.industry ,Nondestructive testing ,Thermography ,Fast Fourier transform ,Harmonic ,Phase (waves) ,business ,DC bias ,Computational physics - Abstract
Lock-in thermography (LT) is based on the correct evaluation of phase differences between the temperature oscillations at different surface regions of the object under test during periodic heating. Since the usual heating procedures contain a DC component, the actual heating pattern achieved is not harmonic. This causes systematic deviations when phase differences are determined by means of harmonic analysis, e.g. with FFT analysis. The resulting errors depend clearly on the ratio between DC and AC amplitude, which is demonstrated at simulated and experimentally recorded temperature transients. Further experimental LT data obtained by different oscillating energy inputs showed a variety of possible shapes of transients with different DC components.
- Published
- 2018
36. Untersuchung sicherheitsrelevanter Ablösungen von Fassadenelementen mit aktiver Thermografie
- Author
-
Jeannine Meinhardt, Christiane Maierhofer, Henrik Steinfurth, Mathias Röllig, and Torsten Arnold
- Subjects
Materials science ,Analytical chemistry ,Mechanical engineering ,Building and Construction ,Civil and Structural Engineering - Abstract
Die Bewertung des Zustandes und der Haftung von Putz und Fassadenelementen auf den darunterliegenden Bauwerksstrukturen ist eine haufig auftretende Fragestellung bei der Erhaltung und Instandsetzung von Bauwerken und Baudenkmalern. Hier mussen nicht nur wirtschaftliche und denkmalpflegerische, sondern auch sicherheitsrelevante Aspekte berucksichtigt werden. Fehlstellen und Ablosungen konnen, auch wiederholend, mit hoher Nachweisempfindlichkeit mit aktiven Thermografieverfahren geortet und unter bestimmten Voraussetzungen quantitativ bewertet werden. Dazu wird der zu untersuchende Bereich zunachst kurzzeitig (mehrere Minuten lang) erwarmt und anschliesend die Abkuhlung mit einer Infrarotkamera aufgezeichnet. Systematische Untersuchungen an Probekorpern mit einer Vielzahl unterschiedlicher Fehlstellen unterhalb von Kalkputz, Fliesen und Klinkerriemchen zeigen, dass die Fehlstellen sowohl mittels kunstlicher Erwarmung durch einen Infrarotstrahler als auch mittels naturlicher Erwarmung durch die Sonne detektiert und charakterisiert werden konnen. Inspection of safety relevant delaminations of facade elements using active thermography The evaluation of condition and adhesion of plaster and facade elements to the underlying building structure is a common issue in the maintenance and repair of buildings and monuments. Here not only economic and preservation, but also safety relevant aspects have to be considered. Voids and delaminations can be detected repeatedly with high sensitivity using active thermography methods. Under certain conditions, also a quantitative evaluation is possible. The area under investigation has to be heated up for a short time (up to several minutes). Subsequently, the cooling down is recorded using an infrared camera. Systematic studies on test specimens with a variety of defects below lime plaster, tiles and brick tiles show that the defects can be detected and even characterized both by means of artificial heating using an infrared heater, as well as by natural solar heating.
- Published
- 2015
37. Cooling-down of thermal thick probes after flash excitation – A measure for the real energy density?
- Author
-
Rainer Krankenhagen, Tamara Worzewski, and Christiane Maierhofer
- Subjects
Materials science ,business.industry ,engineering.material ,Condensed Matter Physics ,Laser ,Atomic and Molecular Physics, and Optics ,Laser flash analysis ,Electronic, Optical and Magnetic Materials ,law.invention ,Flash (photography) ,Optics ,Coating ,law ,Thermal ,Thermography ,engineering ,Optoelectronics ,business ,Excitation ,Cooling down - Abstract
Though flash lamps are one of the most applied heat sources in the field of Thermographic Testing (TT) using active thermography, only little is known about the actually achieved energy input into test objects. In this paper, an easy to realize sensor concept is proposed and experimentally evaluated. The concept is based on the measurement of the surface temperature of a thermal thick probe after flash excitation. After considering the sensor concept with FEM simulations the experimental investigation of four materials (two polymer and two building materials) is described. It will be shown that a suited coating is essential for the realization of the sensor concept. The experimental results prove the suitability of black rigid PVC as the most promising material. Using a coated PVC sample the energy density of short laser pulses, similar to flashes of flash lamps, could be determined exactly with an estimated relative uncertainty of only a few percent.
- Published
- 2015
38. Determining the material parameters for the reconstruction of defects in carbon fiber reinforced polymers from data measured by flash thermography
- Author
-
Jan P. Müller, Christiane Maierhofer, Martin Weiser, and Sebastian Götschel
- Subjects
Carbon fiber reinforced polymer ,Absorption (acoustics) ,Materials science ,Flash (manufacturing) ,Thermography ,Forensic engineering ,Experimental data ,Transient (oscillation) ,Composite material ,Thermal diffusivity ,Excitation - Abstract
Flash thermography is a fast and reliable non-destructive testing method for the investigation of defects in carbon fiber reinforced polymer (CFRP) materials. In this paper numerical simulations of transient thermography data are presented, calculated for a quasi-isotropic flat bottom hole sample. They are compared to experimental data. These simulations are one important step towards the quantitative reconstruction of a flaw by assessing thermographic data. The applied numerical model is based on the finite-element method, extended by a semi-analytical treatment of the boundary of the sample, which is heated by the flash light. A crucial part for a reliable numerical model is the prior determination of the material parameters of the specimen as well as of the experimental parameters of the set-up. The material parameters in plane and in depth diffusivity are measured using laser line excitation. In addition, the absorption and heat transfer process of the first layers is investigated using an IR microsco...
- Published
- 2017
39. Measurement of the radiative energy output of flash lamps by means of thermal thin probes
- Author
-
Rainer Krankenhagen and Christiane Maierhofer
- Subjects
Flash-lamp ,Range (particle radiation) ,Materials science ,business.industry ,Energy conversion efficiency ,Radiant energy ,Condensed Matter Physics ,Atomic and Molecular Physics, and Optics ,Laser flash analysis ,Electronic, Optical and Magnetic Materials ,Flash (photography) ,Optics ,Thermography ,Black-body radiation ,business - Abstract
Flash lamps are widely used excitation sources in the field of non-destructive testing with active thermography. Though the realized energy density in front of the investigated object is a significant factor with regard to detection sensitivity, only few data concerning this issue have been published so far. It is shown here that local energy densities can be estimated by means of a simple metal plate, which exhibits a certain temperature increase after flash excitation. After discussing the underlying calorimetric principle the sensor concept is reviewed using constant blackbody radiation and short laser pulses, since both kinds of sources generate known energy densities. The relative uncertainty of measurements of the energy density is found to be in the range of 10%. The last part of the present paper describes an application for characterizing the radiation of a usual 6 kJ flash lamp. The energy conversion efficiency was found to be only about 11%.
- Published
- 2014
40. Validation of flash thermography using computed tomography for characterizing inhomogeneities and defects in CFRP structures
- Author
-
Christiane Maierhofer, Mathias Röllig, Gilbert Céspedes-Gonzales, Dietmar Meinel, and Karsten Ehrig
- Subjects
Materials science ,medicine.diagnostic_test ,Mechanical Engineering ,Computed tomography ,Fibre-reinforced plastic ,Industrial and Manufacturing Engineering ,Mechanics of Materials ,Flash (manufacturing) ,Thermography ,Ceramics and Composites ,Reflection (physics) ,High spatial resolution ,medicine ,Fiber ,Composite material ,GLUE - Abstract
Active thermography is an efficient non-destructive testing method for investigating the internal structure of larger carbon fiber reinforced plastic (CFRP) components as well as smaller CFRP components in mass customization. The method can be applied contactless and automated. This study contains systematic investigations of CFRP structures with typical defects and inhomogeneities occurring during production by means of flash thermography in reflection and transmission configuration and by computed tomography (CT). The latter one was used as a reference method, since also very small defects at larger depth can be visualized with high spatial resolution. The CFRP structures consist of plates which contain metallic and non-metallic inclusions, contaminations with glue or wax rests, areas with inhomogeneous re-injection of dry parts, fiber misalignments, and fiber damages. Further on, two specimens have been glued together with different artificial inhomogeneities of the four glue beads. The results of the applied methods are compared and the advantages and disadvantages of each configuration are discussed based on the detectability of the inhomogeneities. It is shown that although CT has led to best contrasts and spatial resolutions in displaying the inhomogeneities and inclusions, flash thermography is very well suited to detect most of these structures. Considering that flash thermography can be applied on-site and has a high potential for automation and for a fast and efficient testing, it can be highly recommended for quality assurance during and after production of CFRP structures.
- Published
- 2014
41. Characterizing damage in CFRP structures using flash thermography in reflection and transmission configurations
- Author
-
Mercedes Reischel, Matthias Kunert, Henrik Steinfurth, Christiane Maierhofer, Mathias Röllig, and Philipp Myrach
- Subjects
Carbon fiber reinforced polymer ,Accuracy and precision ,Materials science ,business.industry ,Mechanical Engineering ,Structural engineering ,Industrial and Manufacturing Engineering ,Characterization (materials science) ,Cross section (physics) ,Flash (photography) ,Optics ,Transmission (telecommunications) ,Mechanics of Materials ,Thermography ,Ceramics and Composites ,Reflection (physics) ,Composite material ,business - Abstract
Carbon fiber reinforced polymer (CFRP) specimens with artificial delaminations and with impact damage have been characterized using active thermography with flash excitation. Systematic investigations have been performed in four different experimental configurations of flash lamps and infrared (IR) camera in transmission as well as in reflection alignment. It is shown here that the diffusivities determined for the sound and for the damaged areas give a good measure for damage characterization. Although reflection measurements also give information about defect depth, reflection measurements from only one side are not sufficient for assessing the whole cross section of the specimens. Thus, depending on sample thickness the lateral size of damage could only be determined from reflections measurements from both sides or from transmission measurements. In this paper, measurement accuracy and limits of flash thermography for the investigation of CFRP specimens are presented in detail together with quantitative data concerning the defects.
- Published
- 2014
42. Application of thermographic testing for the characterization of impact damage during and after impact load
- Author
-
Mathias Röllig, Rainer Krankenhagen, and Christiane Maierhofer
- Subjects
Materials science ,Mechanical Engineering ,02 engineering and technology ,Fibre-reinforced plastic ,010402 general chemistry ,021001 nanoscience & nanotechnology ,01 natural sciences ,Industrial and Manufacturing Engineering ,0104 chemical sciences ,Characterization (materials science) ,Mechanics of Materials ,Thermal ,Ceramics and Composites ,Impact energy ,Composite material ,0210 nano-technology - Abstract
Low-velocity impact damages were monitored in-situ using an infrared camera before, during and after impact load. Thermal images were recorded as a function of time at the front side (impact) as well as at the rear side of the plates using a high frame rate. In CFRP and GFRP specimens with different thicknesses and made of various types of fibers and matrix materials, different kind of damages were observed. The sizes of the heated areas being related to the damages and the amount of energy dissipated into heat was determined quantitatively as a function of impact energy and are a measure of the resistance of the different materials against impact load.
- Published
- 2019
43. Pulse phase thermography for characterising large historical building façades after solar heating and shadow cast – a case study
- Author
-
Rainer Krankenhagen and Christiane Maierhofer
- Subjects
Sequence reconstruction ,Image quality ,Shadow ,Thermography ,Phase (waves) ,Facade ,Electrical and Electronic Engineering ,Instrumentation ,Geology ,Phase image ,Remote sensing ,Pulse (physics) - Abstract
For assessing building facades using active thermography, in case of direct solar exposure the sun itself can be used as heat source. It is shown that active thermography can be applied to large areas successfully, if a shadow cast occurs. After performing a sequence reconstruction in order to correct the temporal behaviour of shadow movement, the data could be analysed by pulse phase thermography (PPT). Compared to raw thermograms, the obtained phase images display an improved image quality with a lot of details. The frequency of the phase images is related to the probing depth. The presented case study describes the thermographic investigation of an historical building facade, where an area of 17 m × 13 m has been investigated.
- Published
- 2013
44. Numerical method of active thermography for the reconstruction of back wall geometry
- Author
-
Marc Kreutzbruck, Regina Richter, and Christiane Maierhofer
- Subjects
Optics ,Materials science ,business.industry ,Mechanical Engineering ,Numerical analysis ,Thermography ,General Materials Science ,Geometry ,Inverse problem ,Condensed Matter Physics ,Wall thickness ,business ,Pulse thermography - Abstract
The paper presents a numerical method to detect and characterise defects and inhomogeneities by means of active thermography. The objective was to determine the wall thickness of structure elements with an inaccessible back wall, e.g., elements of pipes or containers. As test specimens we used PVC samples with the thickness of about 2 cm that had spatial variations in the back wall geometry. Flash lamps provided the heating. To measure the thickness of the wall, we employed the Levenberg–Marquardt method, which we applied here to experimental thermographic data for non-destructive testing. We started the inversion procedure by making a rough first estimation of the back wall geometry following the echo defect shape method, and then we calculated the thickness of the back wall. We found reasonable reconstruction results which differed from the real value significantly below 1 mm at the defect centre, whereas the error wais increased at the edge of the defect, depending on its shape and depth.
- Published
- 2013
45. Characterization of pores in high pressure die cast aluminum using active thermography and computed tomography
- Author
-
Bernhard Illerhaus, Mathias Röllig, Dietmar Meinel, Florian Jonietz, Ronald Miksche, Philipp Myrach, Christiane Maierhofer, and Uwe Richter
- Subjects
business.product_category ,Materials science ,Computer simulation ,business.industry ,chemistry.chemical_element ,Structural engineering ,Casting ,Raising (metalworking) ,Characterization (materials science) ,chemistry ,Aluminium ,Thermography ,Die (manufacturing) ,Composite material ,business ,Porosity - Abstract
Larger high pressure die castings (HPDC) and decreasing wall thicknesses are raising the issue of casting defects like pores in aluminum structures. Properties of components are often strongly influenced by inner porosity. As these products are being established more and more in lightweight construction (e.g. automotive and other transport areas), non-destructive testing methods, which can be applied fast and on-site, are required for quality assurance. In this contribution, the application of active thermography for the direct detection of larger pores is demonstrated. The analysis of limits and accuracy of the method are completed by numerical simulation and the method is validated using computed tomography.
- Published
- 2016
46. A round robin test of flash thermography – detectability and quantification of artificial and natural defects in CFRP and metal structures
- Author
-
Igor Kryukov, Christiane Maierhofer, Nick Rothbart, Beate Oswald-Tranta, M. Sengebusch, J. Koch, B. Stotter, F. Hohlstein, G. Mahler, Günter Walle, and Matthias Goldammer
- Subjects
010302 applied physics ,Flash (photography) ,Computer science ,0103 physical sciences ,Thermography ,Evaluation methods ,02 engineering and technology ,Round robin test ,021001 nanoscience & nanotechnology ,0210 nano-technology ,01 natural sciences ,Reliability (statistics) ,Reliability engineering - Abstract
Within the scope of a DIN INS project, a flash thermography round robin test that evaluates reliability, comparability, and efficiency of different testing situations was organized. The results give information about the detectability of defects, e.g. depending on their size and depth, the evaluation methods and the materials used. Besides, the influences of equipment and parameters used by the participants on the results were analysed. All of the quantitative results as well as the feedback given by the participants will be presented in a DIN committee in order to contribute to a flash thermography standard.
- Published
- 2016
47. Non-destructive testing of Cu solder connections using active thermography
- Author
-
Mathias Röllig, Christiane Maierhofer, Henrik Steinfurth, Marc Kreutzbruck, Mathias Ziegler, S. Heck, and Christian Scheuerlein
- Subjects
Materials science ,Busbar ,Infrared ,business.industry ,Mechanical Engineering ,Detector ,Microbolometer ,Impulse (physics) ,Condensed Matter Physics ,Optics ,Soldering ,Nondestructive testing ,Thermography ,Electronic engineering ,General Materials Science ,business - Abstract
Impulse and lock-in thermography have been applied to detect delaminations of prototype solder joints, similar to those to be produced between Cu shunts and Cu busbar stabilisers at the Large Hadron Collider (LHC) at CERN. Two infrared cameras with different detector materials and with different spectral ranges and two excitation techniques have been tested and compared for their ability to detect delaminations behind 2 and 3 mm thick Cu shunts. We have analyzed the signal to noise ratio (SNR) for each detected defect and are able to detect defects down to a nominal edge length of 4 mm behind 2 mm thick Cu shunts by using fast impulse thermography and a camera with a microbolometer array. For the 3 mm thick Cu shunt, on the other hand, the nominal 4 mm defect is only visible in the lock-in thermography phase images and the highest SNR has been achieved with a cooled InSb-based camera. In addition, numerical simulations show the influence of the minimum detectable defect size on the shunt thickness and that the developed on-site testing technique is sufficient to find all defects that are detectable theoretically.
- Published
- 2012
48. Methoden der Dauerüberwachung von Gebäuden des kulturellen Erbes im Rahmen der Denkmalkonservierung
- Author
-
Florian Antretter, Jeannine Meinhardt, Paul Bellendorf, Markus Krüger, Christiane Maierhofer, and Johanna Leissner
- Subjects
Engineering ,business.industry ,business - Published
- 2012
49. Efficient data evaluation for thermographic crack detection
- Author
-
Mathias Ziegler, Joachim Schlichting, Christiane Maierhofer, Marc Kreutzbruck, and Anika Dey
- Subjects
Data set ,Sequence ,Laser scanning ,Pixel ,Computer science ,Acoustics ,Frame (networking) ,Thermography ,Derivative ,Magnetic particle inspection ,Electrical and Electronic Engineering ,Instrumentation - Abstract
We present an all-purpose crack detection algorithm for flying spot thermography which is directly applicable to a thermogram sequence without the need of any additional information about the experimental setup. A single image containing distinct crack signatures is derived in two steps. Firstly, the spatial derivative is calculated for each frame of the sequence and, secondly, the resulting data set is sorted pixel wise along the time axis. The feasibility of the proposed procedure is proven by testing a piece of rail that comprises roll contact fatigue cracks and by comparing the results with magnetic particle testing.
- Published
- 2011
50. Integration of active thermography into the assessment of cultural heritage buildings
- Author
-
Rainer Krankenhagen, Christiane Maierhofer, and Mathias Röllig
- Subjects
Cultural heritage ,Historical structure ,Engineering ,Active infrared ,business.industry ,Thermography ,Heat losses ,Masonry ,Mortar ,business ,Civil engineering ,Atomic and Molecular Physics, and Optics - Abstract
Applications of infrared thermography in civil engineering are not limited to the identification of heat losses in building envelopes. Active infrared thermography methods enable structural investigations of building elements with one-sided access up to a depth of about 10 cm. Masonry and especially historical masonry has a very heterogeneous structure containing several different materials (brick, stone, mortar, plaster, wood, metal, etc.) with various thermal properties. As many classes of damage originate from defects that are close to the surface, active thermography is in general very well suited to assessing different test problems in cultural heritage buildings. In this paper, the physical background, equipment, environmental influences and material properties are discussed. Several application results are presented. It is shown how active thermography can be integrated into a holistic approach for the assessment of historical structures.
- Published
- 2010
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