1. Effect of incorporation of calcium polyphosphate sub-microparticles in low-concentration bleaching gels on physical properties of dental enamel.
- Author
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Dos Anjos HA, Ortiz MIG, Aguiar FHB, Dos Santos JJ, Rodrigues UP, Rischka K, and Lima DANL
- Subjects
- Cattle, Animals, Hardness, Surface Properties, Spectrometry, X-Ray Emission, In Vitro Techniques, Color, Peroxides pharmacology, Urea analogs & derivatives, Urea pharmacology, Urea chemistry, Hydrogen-Ion Concentration, Particle Size, Dental Enamel drug effects, Gels, Hydrogen Peroxide chemistry, Tooth Bleaching Agents pharmacology, Tooth Bleaching Agents chemistry, Microscopy, Electron, Scanning, Polyphosphates pharmacology, Polyphosphates chemistry, Tooth Bleaching methods, Carbamide Peroxide pharmacology
- Abstract
Aim: To evaluate the bleaching efficacy and effects on enamel properties of experimental gels with carbamide peroxide (CP; 10%) or hydrogen peroxide (HP; 6%) containing calcium polyphosphate sub-microparticles (CaPPs)., Methods: A total of 216 bovine tooth specimens were divided for microhardness and color analyses (n = 108) and block randomized into nine groups (n = 12): (G1) commercial CP (Whiteness Perfect, FGM; Brazil); (G2) experimental CP; (G3) CP-0.5%CaPPs; (G4) CP-1.5%CaPPs; (G5) commercial HP (Potenza Bianco, PHS; Brazil); (G6) experimental HP; (G7) HP-0.5%CaPPs; (G8) HP-1.5%CaPPs; (G9) artificial saliva. The gels' pH values were determined with a bench pH meter. Color (ΔE, ΔE
00 , ΔWID ) and microhardness variation were evaluated before and after the therapy. Part of the specimens used for microhardness was submitted to the scanning electron microscopy (SEM) (n = 3) and energy-dispersive X-ray spectroscopy EDX (n = 3) analyses. Statistical analyses were performed in the R statistical software (α = 0.05). Linear mixed models for repeated measures in time were used to analyze microhardness and L* values. Generalized linear models were used to analyze the a*, b*, ΔE, ΔE00 , and ΔWID, considering a group effect. The EDX data were analyzed using a one-way ANOVA with Tukey's test., Results: The gels' pH remained over 6,0. All gels effectively bleached the specimens and did not differ significantly. When compared to the control group, the hardness was significantly lower in the G1, G2, G6, and G7 groups. The G3, G4, G5, and G8 groups did not differ significantly (p > 0.05)., Conclusion: The incorporation of CaPPs in low-concentration whitening gels reduces its negative effects on microhardness without interfering with their bleaching efficacy., (© 2023. The Author(s), under exclusive licence to The Society of The Nippon Dental University.)- Published
- 2024
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