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Cameroon harvests a considerable volume of round wood each year, only a small part of which is used for manufactured products. In recent decades, various charcoal-making initiatives have emerged around industrial timber-processing units, particularly in the eastern region, in order to develop a market for residual biomass. However, the undifferentiated use of these residues obtained from different species often results in products with varying energy potential that are not always appreciated by consumers. Moreover, the physical and chemical characteristics of the charcoal produced are unknown, as are the factors that influence its quality. The aim of this study was to assess the variability of the physical and chemical properties of charcoal produced from industrial sawmill residues in the eastern region of Cameroon using different carbonisation techniques. Three wood species, Ayous, Frake and Movingui, and three types of kilns (traditional, improved traditional and Casamance system) were used. For each species, three bundles of five pieces of wood each were prepared, with an initial moisture content ranging from 28% to 36%. The physical and chemical properties determined were moisture content, apparent density, volatile matter content, fixed carbon content, ash content and Higher Heating Value (HHV). Our results showed that the charcoal properties varied depending on the wood species and types of kilns used. Movingui, with the highest density (0.73 g/cm3), produced charcoal with the lowest moisture content (4.03%) and the highest apparent density (0.42 g/cm3). The lowest volatile matter content (20.32%), the lowest ash content (1.27%) and the highest fixed carbon content (74.95%) were also obtained with this species. All these values were obtained with Movingui charcoal produced with the Casamance system. However, the highest HHV (32.51 MJ/kg) was obtained with charcoal from Ayous, also produced with the Casamance system. On comparing the three charcoaling systems used, the Casamance model yielded the best physical and chemical charcoal properties. All the charcoals studied complied with FAO standards for cooking fuel. The highest HHV obtained with charcoal from Ayous hardwood shows its ability to release large amounts of thermal energy during combustion. Keywords: Charcoal, carbonization technologies, eastern Cameroon, physicochemical properties, industrial sawmills wastes.