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Mamuju is an area of high natural radiation in Indonesia with high natural radiation levels (average 613 nSv h−1). Mamuju is anomalous due to its high average 238U and 232Th concentrations of 22,882 and 33,549 Bq kg−1, respectively, in laterite and rock. High natural radionuclide concentrations of 238U, 232Th, and 40K have also been reported in soil samples from several locations in Mamuju, including Botteng, Northern Botteng, Takandeang, Ahu, and Taan. High radiation levels are related to radioactive mineral occurrences in the Adang volcanic complex, comprised of phonolitoid and foiditoid lithologies. According to the International Atomic Energy Agency (IAEA), uranium deposits can be classified into several types, among them a volcanic-related deposits, which include three sub-types: stratabound, structure-bound, and volcano-sedimentary deposits. This study aims to characterize volcanic rock deposit sub-types in the Mamuju area based on uranium radioisotope measurements. The uranium isotopes were measured using a tandem quadrupole inductively coupled plasma mass spectrometer combined with chemical separation by extraction chromatography using UTEVA resin. The analytical results for the 234U/238U ratios are used to determine the formation characteristics of minerals in each deposit sub-type based on mineral formation age, post-formation processes, and disturbances that affected the formation processes. Based on geochronological calculations using 234U/238U mineralization age, the deposits in the Mamuju area are 0.914–1.11 million years old and are classified as recent mineralization. These data have important implications for tracing uranium source rocks in the Mamuju area and may explain the anomalously high radiation levels in the Mamuju area.

Radiometric mapping could play a prominent role in locating the host rock or alteration that leads to gold mineralization. Nevertheless, in low-sulfidation epithermal gold deposits, the radiometric signatures have to be priorly characterized due to their geometry. It is comprised of a small ore vein system within the large alteration zones. The Pongkor gold mine is a low-sulfidation epithermal deposit and was selected for this purpose. The method started with the surface identification of radiometric signatures on altered and unaltered rocks near Pongkor using portable spectrometers. They are followed by the characterization of the underground mining front, which is comprised of different types of veins and host rocks. The results show that the altered rocks were characterized by a high K% and a low eTh/K ratio. Vice versa, the mineralized veins show low radioelement concentrations. Following the characterization of the geometry of alteration zones and mineralized veins, a study of the relationship between radioelements detected by radiometric mapping and gold pathfinder elements was conducted. Gold pathfinders of Mn, Fe, Zn, As, and Pb were selected for correlation studies with the radioelement. The pathfinders and radioelements were more significantly correlated in veins compared to the host rock. Based on this study, radiometric mapping has the potential and benefit of being applied in the exploration of low-sulfidation epithermal gold deposits. An alteration zone could be delineated by K or eTh/K as an anomaly indicator, and the vein bodies could also be delineated using low K or eTh as an anomaly indicator.