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Milk of lime (MOL) suspension is widely utilized in many industries; however, in some of the applications, such as the production of precipitated calcium carbonate (PCC), the suspension must be of high purity and quality. In other words, the amounts of iron and magnesium should be so little so that the final PCC product would be of high quality. The effects of initial temperature, quicklime particle size, amount of initial solid present, agitation rate, and time on the recovery of hydrated lime and iron/magnesium reduction efficiency were investigated through a central composite design (CCD) of experiments. The iron reduction efficiency and the weight recovery of hydrated lime were obtained as 91% and 98.5%, respectively. The reduction of magnesium was not significant in this stage. Moreover, approximately the whole existing SiO2 was eliminated. [ABSTRACT FROM AUTHOR]