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Surface sediments samples were collected at 11 stations around the Pulau Tinggi, Johor in September 2015. A total of 15 PAHs were determined and quantified by gas chromatography coupled with mass spectrometry (GC-MS). The total PAH concentrations of surface sediments from Pulau Tinggi ranged from 39.61 ng/g to 149.2 ng/g and they were classified as being in low to moderate pollution range. Individual PAH analysis showed that two and three rings PAHs were the most frequently detected isomers and accounted for 22 - 46% of the total PAH concentrations. The sources of PAHs were evaluated by employing diagnostic ratiosof specific PAH compounds.PAH ratios analysis showed a prevalence of pyrogenic PAH origin at most of the stations with exception of only a few stations. [ABSTRACT FROM AUTHOR]