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1. Synthesis of novel tetrahydro-1H-pyrazolo[4,3-c]pyridines via intramolecular nitrilimine cycloaddition

Author

Albert William, Garofalo, Jacek Jerzy, Jagodzinski, Andrei William, Konradi, Raymond Anthony, Ng, Christopher Michael, Semko, Hing Leung, Sham, Minghua, Sun, and Xiaocong Michael, Ye

Subjects
Models, Molecular, Magnetic Resonance Spectroscopy, Cyclization, Pyridines, Nitriles, Imines, Mass Spectrometry
Abstract

The preparation of novel tetrahydro-1H-pyrazolo[4,3-c]pyridines is reported. Pivotal to the synthesis of these compounds was the development of mild reaction conditions to generate a highly functionalized nitrilimine capable of undergoing an intramolecular cycloaddition with a tethered alkyne. The desired cycloadduct was formed as an equal mixture of diastereomers.

Published
2012

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