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14 results on '"Kanakal, Mahibub"'

3. Gas Chromatography-Mass Spectrometry (GC-MS) Analysis of Scaphium Affine Seed Extract and Assessment of its Anti-Hemorrhoidal Efficacy

Author

Abbas, Syed Atif, primary, Khan, Abdullah, additional, Fatima, Mehraj, additional, Kalusalingam, Anandarajagopal, additional, Kanakal, Mahibub Mahamadsa, additional, Inamdar, Shiva kumar, additional, Kotra, Vijay, additional, Ming, Long Chiau, additional, Dastapur, Ashok Kumar M., additional, and B, Tazneem, additional

Published
2024
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5. The Effect of Aflatoxin B1 on Tumor-Related Genes and Phenotypic Characters of MCF7 and MCF10A Cells

Author

Adam, Mowaffaq Adam Ahmed, primary, Kamal, Laina Zarisa Muhd, additional, Kanakal, Mahibub, additional, Babu, Dinesh, additional, Dahham, Saad Sabbar, additional, Tabana, Yasser, additional, Lok, Bronwyn, additional, Bermoy, Brittany M., additional, Yunus, Muhammad Amir, additional, Than, Leslie Thian Lung, additional, Barakat, Khaled, additional, and Sandai, Doblin, additional

Published
2022
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6. Cancer protective effects of plums: A systematic review

Author

Bahrin, Abdul Alim, primary, Moshawih, Said, additional, Dhaliwal, Jagjit Singh, additional, Kanakal, Mahibub Mahahamadsa, additional, Khan, Abdullah, additional, Lee, Kah Seng, additional, Goh, Bey Hing, additional, Goh, Hui Poh, additional, Kifli, Nurolaini, additional, and Ming, Long Chiau, additional

Published
2022
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7. A Mini-review on Ultra Performance Liquid Chromatography

Author

Basharat, Rabia, primary, Kotra, Vijay, additional, Loong, Lean Yen, additional, Mathews, Allan, additional, Kanakal, Mahibub Mahamadsa, additional, Dev, CH B Praveena, additional, Nyamathulla, Shaik, additional, Varala, Ravi, additional, Ming, Long Chiau, additional, Rao, KRS Sambasiva, additional, Babu, B. Hari, additional, and Alam, M. Mujahid, additional

Published
2021
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8. Ultra Performance Liquid Chromatography (Mini-Review).

Author

BASHARAT, RABIA, KOTRA, VIJAY, LEAN YEN LOONG, MATHEWS, ALLAN, KANAKAL, MAHIBUB MAHAMADSA, DEVI, CH B. PRAVEENA, NYAMATHULLA, SHAIK, VARALA, RAVI, MING, LONG CHIAU, RAO, KRS SAMBASIVA, BABU, B. HARI, and ALAM, M. MUJAHID

Subjects
LIQUID chromatography, HIGH performance liquid chromatography, LITERARY criticism, CHROMATOGRAMS, SEPARATION (Technology)
Abstract

Chromatography is a widely used analytical tool for separating a mixture of compounds into individual component. High performance liquid chromatography (HPLC) is one of the most important methods used for the separation, identification and quantification of a compounds present in a mixture. It meets many criteria of analysis but its main drawbacks are it is relatively time consuming to run a chromatogram and consumes high amount of solvent compared to other analytical methods. There is a need to develop a method which can overcome these drawbacks of HPLC. Ultra performance liquid chromatography (UPLC) is the new approach which opens novel direction in the field of liquid chromatography. It works on similar principle but shows better performance than conventional HPLC. UPLC is a technique of liquid chromatography with improved runtime and sensitivity with less than 2 μm particle size. The UPLC separation process is carried out under very high pressure (up to100 MPa). Additionally, it reduces the cost of reagent with shorter run time as compared to conventional HPLC. This article updated until 2020, provides a general review on the principle, instrumentation and application of UPLC in different fields of science. [ABSTRACT FROM AUTHOR]

Published
2021
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14. Buffer-Free High Performance Liquid Chromatography Method for the Determination of Theophylline in Pharmaceutical Dosage Forms.

Author

Kanakal, Mahibub M., Abdul Majid, Aman Shah, Sattar, Munavvar Zubaid A., Ajmi, Noor Shahida, and Abdul Majid, Amin Malik Shah

Subjects
*DOSAGE forms of drugs, *HIGH performance liquid chromatography, *THEOPHYLLINE, *MOBILE phase (Chromatography), *PHYSIOLOGICAL effects of caffeine, *ACETONITRILE, *THERAPEUTICS
Abstract

Purpose: To develop and validate a simple, economical and reproducible high performance liquid chromatographic (HPLC) method for the determination of theophylline in pharmaceutical dosage forms. Method: Caffeine was used as the internal standard and reversed phase C-18 column was used to elute the drug and standard. The mobile phase was prepared by mixing water:acetonitrile:methanol at the ratio of 90:03:07 and the pH set at 4.6. Flow rate and ultraviolet (UV) detector were set at 1.0 mLmin-1 and 271 nm, respectively. The method was validated for linearity, recovery, accuracy, precision, specificity, and also for inter-day stability under laboratory conditions. Results: Retention time was 5.5 min. The limits of detection and quantification were 12.5 ngmL-1 and 100 ngmL-1, respectively. Recovery accuracy (%) for different concentrations ranged from 100.05 to 102.43; regression coefficient (R2) of 0.994; precision RSD < 2.0, and negligible interference from common excipients. Conclusion: The method is simple, rapid, highly specific and suitable for the determination of theophylline. Absence of buffer and use of small quantity of organic solvents increase the life span of the column and reduce the cost of routine analysis of theophylline in industry. [ABSTRACT FROM AUTHOR]

Published
2014
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