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Wireless sensor networks (WSNs) are distributed networks comprising small sensing devices equipped with a processor, memory, power source, and often with the capability for short range wireless communication. These networks are used in various applications, and have created interest in WSN research and commercial uses, including industrial, scientific, household, military, medical and environmental domains. These initiatives have also been stimulated by the finalisation of the IEEE 802.15.4 standard, which defines the medium access control (MAC) and physical layer (PHY) for low-rate wireless personal area networks (LR-WPAN). Future applications may require large WSNs consisting of huge numbers of inexpensive wireless sensor nodes with limited resources (energy, bandwidth), operating in harsh environmental conditions. WSNs must perform reliably despite novel resource constraints including limited bandwidth, channel errors, and nodes that have limited operating energy. Improving resource utilisation and quality-of-service (QoS), in terms of reliable connectivity and energy efficiency, are major challenges in WSNs. Hence, the development of new WSN applications with severe resource constraints will require innovative solutions to overcome the above issues as well as improving the robustness of network components, and developing sustainable and cost effective implementation models. The main purpose of this research is to investigate methods for improving the performance of WSNs to maintain reliable network connectivity, scalability and energy efficiency. The study focuses on the IEEE 802.15.4 MAC/PHY layers and the carrier sense multiple access with collision avoidance (CSMA/CA) based networks. First, transmission power control (TPC) is investigated in multi and single-hop WSNs using typical hardware platform parameters via simulation and numerical analysis. A novel approach to testing TPC at the physical layer is developed, and results show that contrary to what has be