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3. Ir(III)-catalyzed decarbonylative annulation of salicylaldehydes with cyclohexane-1,3-diones.

Author

Jiang, Qiao-Juan, Min, Yu-Tao, Liu, Yan-Ping, Li, Hua, Peng, Jun-Ao, and Liu, Cong-Jun

Subjects
*ANNULATION, *YLIDES, *FUNCTIONAL groups, *BENZOFURAN
Abstract

An efficient Ir(III)-catalyzed decarbonylative annulation of salicylaldehydes with cyclohexane-1,3-diones has been achieved via the in situ generated iodonium ylides. The reaction proceeds smoothly under mild and operationally simple conditions, affording a variety of benzofuran derivatives in moderate to high yields with good functional group tolerance. Moreover, the large-scale synthesis and further modification of the products highlight the utility of this protocol. [ABSTRACT FROM AUTHOR]

Published
2023
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