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Interleaving thermoplastic veils has proved to enhance the interlaminar fracture toughness of carbon fibre/epoxy composites under static loading conditions. However, the fatigue delamination behaviour has yet to be investigated. Herein, meltable Polyamide-12 (PA) veils and non-meltable Polyphenylene-sulphide (PPS) veils were used for interlay toughening of unidirectional (UD) and non-crimp fabric (NCF) laminates that were manufactured using a prepreg process and resin transfer moulding process, respectively. The results of Mode-I fatigue delamination tests demonstrated a significant improvement in the fatigue life of the laminates due to interleaving. Additionally, the fatigue resistance energy has been maximumly increased by 143% and 190% for the UD and NCF laminates, respectively. The microscopy analysis revealed that the toughening mechanisms of thermoplastic veils were affected by the form of the thermoplastic veils in the laminates (melted or non-melted), the fracture mechanisms of the reference laminates and the adhesion/miscibility between the thermoplastic veils and the epoxy., Green Open Access added to TU Delft Institutional Repository ‘You share, we take care!’ – Taverne project https://www.openaccess.nl/en/you-share-we-take-care Otherwise as indicated in the copyright section: the publisher is the copyright holder of this work and the author uses the Dutch legislation to make this work public., Structural Integrity & Composites

This work studied the effects of adding short basalt fibers (BFs) and multi-walled carbon nanotubes (MWCNTs), both separately and in combination, on the mechanical properties, fracture toughness, and electrical conductivity of an epoxy polymer. The surfaces of the short BFs were either treated using a silane coupling agent or further functionalized by atmospheric plasma to enhance the adhesion between the BFs and the epoxy. The results of a single fiber fragmentation test demonstrated a significantly improved BF/epoxy adhesion upon applying the plasma treatment to the BFs. This resulted in better mechanical properties and fracture toughness of the composites containing the plasma-activated BFs. The improved BF/epoxy adhesion also affected the hybrid toughening performance of the BFs and MWCNTs. In particular, synergistic toughening effects were observed when the plasma-activated BFs/MWCNTs hybrid modifiers were used, while only additive toughening effects occurred for the silane-sized BFs/MWCNTs hybrid modifiers. This work demonstrated a potential to develop strong, tough, and electrically conductive epoxy composites by adding hybrid BF/MWCNT modifiers., Structural Integrity & Composites

The present work is concerned with adhesive bonding of thermoplastic composites used in general aerospace applications, including polyphenylene sulfide (PPS), polyetherimide (PEI) and polyetheretherketone (PEEK) carbon fibre composites. Three different surface treatments have been applied to the PEEK, PPS and PEI-based composites in order to enhance the adhesion: atmospheric plasma, ultraviolet radiation (UV) and isopropanol wiping as a control. Water contact angles and free surface energies were measured following the standard experimental procedure based on the employment of three different liquid droplets. Infrared spectroscopy and X-ray photoelectron spectroscopy (XPS) were subsequently performed to characterize the surface chemistry of the samples after treatment. The single lap joints were manufactured and bonded by an Aerospace grade epoxy-based film adhesive originally developed for use on metals but with the ability to bond treated thermoplastics to good strength (supplied by Henkel Ireland). Quasi-static (QS) tests were conducted. The lap shear strength was evaluated, and the failure mechanisms of the different joints were examined for the range of surface treatments considered. It was found that the performances of the PEEK and PPS joints were considerably improved by the plasma and UV treatments resulting in cohesive and delamination failures, while PEI was unaffected by the plasma and UV treatments and performed very well throughout., Structural Integrity & Composites

Interlaying thermoplastic veils into carbon fibre/epoxy composites has proved to significantly increase the interlaminar fracture toughness. The main toughening mechanism is thermoplastic fibre bridging for the non-meltable veils and matrix toughening for the meltable veils. Herein, to take advantage of different toughening mechanisms, hybrid meltable/non-meltable thermoplastic veils were used to interlay two types of aerospace-grade composites produced from unidirectional (UD) prepregs and resin transfer moulding of non-crimp carbon fibre fabrics (NCF). The mode-I and mode-II fracture behaviour of the interleaved laminates were investigated. The experimental results demonstrated outstanding toughening performance of the hybrid veils for the mode-I fracture behaviour of the UD laminates and for both of the mode-I and mode-II fracture behaviour of the NCF laminates, resulting from the combination of different toughening mechanisms. For example, the maximum increases in the mode-I and mode-II fracture energies of the NCF laminates were observed to be 273% and 206%, respectively., Structural Integrity & Composites, Aerospace Manufacturing Technologies

Carbon fibre reinforced poly-etherether-ketone (PEEK) and poly-phenylene-sulfide (PPS) composites were rapidly surface-treated by high-power UV light, and then adhesively bonded to aluminium 2024-T3 and carbon fibre/epoxy composites. The results of a single lap-shear joint test demonstrated that a UV-treatment lasting for 5 s was sufficient to prevent joint failure occurring at the composite/adhesive interfaces in all cases, e.g. it increased the failure strength of the PPS composite/aluminium joints from 11.1 MPa to 37.5 MPa. Moreover, the composite/adhesive interfaces performed well upon an exposure of the joints to an environment of high humidity and temperature for 8 weeks. Additionally, an investigation lasting for 6 months showed no degradation of the surface functionalisation from UV-irradiation. Overall, this work highlights high-power UV-irradiation a very promising method for surface preparation of thermoplastic composites (TPCs) for adhesive joining, i.e. TPC adhesive joints with excellent structural integrity can be obtained by using this rapid, eco-friendly and low-cost surface-treatment method., Structural Integrity & Composites