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1. Hybrid Molecular Sieve-Based Interfacial Layer with Physical Confinement and Desolvation Effect for Dendrite-free Zinc Metal Anodes.

Author

Xu, J, Han, P, Jin, Y, Lu, H, Sun, B, Gao, B, He, T, Xu, X, Pinna, N, Wang, G, Xu, J, Han, P, Jin, Y, Lu, H, Sun, B, Gao, B, He, T, Xu, X, Pinna, N, and Wang, G

Abstract

The side reactions and dendrite growth at the interface of Zn anodes greatly limit their practical applications in Zn metal batteries. Herein, we propose a hybrid molecular sieve-based interfacial layer (denoted as Z7M3) with a hierarchical porous structure for Zn metal anodes, which contains 70 vol % microporous ZSM-5 molecular sieves and 30 vol % mesoporous MCM-41 molecular sieves. Through comprehensive molecular dynamics simulations, we demonstrate that the mesopores (∼2.5 nm) of MCM-41 can limit the disordered diffusion of free water molecules and increase the wettability of the interfacial layer toward aqueous electrolytes. In addition, the micropores (∼0.56 nm) of ZSM-5 can optimize the Zn2+ solvation structures by reducing the bonded water molecules, which simultaneously decrease the constraint force of solvated water molecules to Zn2+ ions, thus promoting the penetrability and diffusion kinetics of Zn2+ ions in Z7M3. The synergetic effects from the hybrid molecular sieves maintain a constant Zn2+ concentration on the surface of the Zn electrode during Zn deposition, contributing to dendrite-free Zn anodes. Consequently, Z7M3-coated Zn electrodes achieved excellent cycling stability in both half and full cells.

Published
2024

2. Ultrasensitive Non-enzymatic Electrochemical Glucose Sensor Based on NiO/CNT Composite

Author

Movlaee, K., Raza, H., Pinna, N., Leonardi, S. G., Neri, G., Angrisani, Leopoldo, Series Editor, Arteaga, Marco, Series Editor, Panigrahi, Bijaya Ketan, Series Editor, Chakraborty, Samarjit, Series Editor, Chen, Jiming, Series Editor, Chen, Shanben, Series Editor, Chen, Tan Kay, Series Editor, Dillmann, Ruediger, Series Editor, Duan, Haibin, Series Editor, Ferrari, Gianluigi, Series Editor, Ferre, Manuel, Series Editor, Hirche, Sandra, Series Editor, Jabbari, Faryar, Series Editor, Jia, Limin, Series Editor, Kacprzyk, Janusz, Series Editor, Khamis, Alaa, Series Editor, Kroeger, Torsten, Series Editor, Liang, Qilian, Series Editor, Ming, Tan Cher, Series Editor, Minker, Wolfgang, Series Editor, Misra, Pradeep, Series Editor, Möller, Sebastian, Series Editor, Mukhopadhyay, Subhas, Series Editor, Ning, Cun-Zheng, Series Editor, Nishida, Toyoaki, Series Editor, Pascucci, Federica, Series Editor, Qin, Yong, Series Editor, Seng, Gan Woon, Series Editor, Veiga, Germano, Series Editor, Wu, Haitao, Series Editor, Zhang, Junjie James, Series Editor, Andò, Bruno, editor, Baldini, Francesco, editor, Di Natale, Corrado, editor, Ferrari, Vittorio, editor, Marletta, Vincenzo, editor, Marrazza, Giovanna, editor, Militello, Valeria, editor, Miolo, Giorgia, editor, Rossi, Marco, editor, Scalise, Lorenzo, editor, and Siciliano, Pietro, editor

Published
2019
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3. Verwey transition in single magnetite nanoparticles

Author

Yu, Q., Mottaghizadeh, A., Wang, H., Ulysse, C., Zimmers, A., Rebuttini, V., Pinna, N., and Aubin, H.

Subjects
Condensed Matter - Mesoscale and Nanoscale Physics, Condensed Matter - Strongly Correlated Electrons
Abstract

We present a tunnel spectroscopy study of the electronic spectrum of single magnetite \chemform{Fe_3O_4} nanoparticles trapped between nanometer-spaced electrodes. The Verwey transition is clearly identified in the current voltage-characteristics where we find that the transition temperature is electric field dependent. The data show the presence of localized states at high energy, $\varepsilon \sim 0.6eV$, which can be attributed to polaron states. At low energy, the density of states (DOS) is suppressed at the approach of the Verwey transition. Below the Verwey transition, a gap, $\Delta \sim 300meV$, is observed in the spectrum. In contrast, no gap is observed in the high temperature phase, implying that electronic transport in this phase is possibly due to polaron hopping with activated mobility., Comment: 5 pages, 5 figures. Higher resolution images in published paper

Published
2014
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5. Understanding the factors affecting contact resistance in nanowire field effect transistors (NWFETs) to improve nanoscale contacts for future scaling.

Author

Ramesh, S., Ivanov, Ts., Sibaja-Hernandez, A., Alian, A., Camerotto, E., Milenin, A., Pinna, N., El Kazzi, S., Lin, D., Lagrain, P., Favia, P., Bender, H., Collaert, N., and De Meyer, K.

Subjects
FIELD-effect transistors, NANOWIRES, PLASMA etching, SURFACE states, LOW temperatures, OHMIC contacts
Abstract

In this paper, dry etched vertical nanowires (VNWs) are used in transmission line/transfer length analysis to study the contacts of gate-all-around devices for future technology nodes. VNW resistors with Mo and Pd based metal stack contacts to p-InGaAs show Schottky behavior, unlike the planar counterpart. The resistance for Mo contact is higher than Pd, however, Pd was found to form an alloy with InGaAs at temperatures as low as 190 °C, and the length of Pd diffusion into the InGaAs increased at smaller NW dimensions, hindering future scalability. The minimum extracted specific contact resistivity (ρC) values are 1.6 × 10−5 Ω cm2 (Mo) and 4.2 × 10−6 Ω cm2 (Pd) for a doping level of 1 × 1019 cm−3. An apparent dependence of ρC on the NW diameter was also observed. This has been attributed to the surface states under the un-gated region of NW devices and found to dominate at smaller diameters. An analytical model to account for such geometrical effects has also been developed and validated with technology computer-aided design simulations. The analysis presented in this paper effectively captures the 3D aspects of an NW contact at nanoscale dimensions and can be applied irrespective of the semiconductor and contact metal used. [ABSTRACT FROM AUTHOR]

Published
2022
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7. A randomized trial of intensive versus minimal surveillance of patients with resected Dukes B2-C colorectal carcinoma

Author

Rosati, G., Ambrosini, G., Barni, S., Andreoni, B., Corradini, G., Luchena, G., Daniele, B., Gaion, F., Oliverio, G., Duro, M., Martignoni, G., Pinna, N., Sozzi, P., Pancera, G., Solina, G., Pavia, G., Pignata, S., Johnson, F., Labianca, R., Apolone, G., Zaniboni, A., Monteforte, M., Negri, E., Torri, V., Mosconi, P., and Fossati, R.

Published
2016
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8. Sensing Behavior of SnO2-Graphene Nanocomposites

Author

Neri, G., Latino, M., Donato, N., Baek, S., Pinna, N., Baldini, Francesco, editor, D’Amico, Arnaldo, editor, Di Natale, Corrado, editor, Siciliano, Pietro, editor, Seeber, Renato, editor, De Stefano, Luca, editor, Bizzarri, Ranieri, editor, and Andò, Bruno, editor

Published
2014
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17. Fetal alcohol spectrum disorders awareness in health professionals: implications for psychiatry

Author

Messina, M. P., D'Angelo, A., Battagliese, G., Coriale, G., Tarani, L., Pichini, S., Rasio, D., Parlapiano, G., Fiore, M., Petrella, C., Vitali, M., Ferraguti, G., Ceccanti, M., Bertoli, D., Canepa, M., Cappadona, R., D'Alessio, A., Danza, M., Morese, A., Paolino, A., Pileri, F., Pinna, N., Neri, I., Razzano, R., Ricchi, A., and Rizzi, M.

Subjects
Male, Psychiatry, Analysis of Variance, Health Knowledge, Attitudes, Practice, Students, Health Occupations, Alcohol Drinking, Alcohol, FASD, Health professionals, Pregnancy, Health Personnel, Facies, Midwifery, Europe, Italy, Fetal Alcohol Spectrum Disorders, Health Care Surveys, Physicians, Humans, Female
Abstract

Fetal Alcohol Spectrum Disorders (FASD) are a plethora of malformative conditions leading to mental retardation that affect newborns and children who have been exposed to alcohol during pregnancy or breastfeeding. FASD is a relevant topic for public health in Europe: European area is first in ranking for alcohol use during pregnancy with a prevalence of 25.2%. Italy ranked third among European countries with higher prevalence of FASD (45.0 per 1000 population). Furthermore, FASD could still be underestimated because of numerous undiagnosed and misdiagnosed cases. Aims of the study were to briefly summarize existing evidences about FASD and its psychiatric aspects to assess knowledge, attitudes and practice towards alcohol drinking during pregnancy in an Italian sample of health care professionals in order to provide information about FASD prevention. An anonymous online questionnaire containing the AUDIT-C, T-ACE model and the Drinking Motive Questionnaire was sent to 400 Italian healthcare professionals and students. The survey included socio-demographic information, questions about drinking habits and about knowledge, attitude and practice towards alcohol assumption during pregnancy. Among 320 respondents, 96.3% were women. AUDIT-C revealed that 52.4% were low risk drinkers but 27.6% were hazardous drinkers. The 90.6% of participants denied to ever attended a course about the fetus damage induced by alcohol consumption during pregnancy but 91.3% were willing to participate to professional update initiatives on the topic. Only 19.1% of participants talk regularly about the deleterious effects for the fetus of prenatal alcohol drinking to women and only 51.1% advise the 'zero alcohol' policy. Around 41% of participants tolerates the assumption of low-alcohol beverages. No differences were found between no drinkers and low and hazardous drinkers. In conclusion, data show that only specific and continuing updating for health care professionals about drinking habits may have impactful actions to prevent gestational alcohol intake in order to prevent the main cause of mental retardation in western countries.

Published
2020

20. Fetal alcohol spectrum disorders awareness in health professionals: Implications for psychiatry|La conoscenza della sindrome alcolica fetale negli operatori sanitari: Implicazioni per la psichiatria

Author

Messina, M. P., D'Angelo, A., Battagliese, G., Coriale, G., Tarani, L., Pichini, S., Rasio, D., Parlapiano, G., Fiore, M., Petrella, C., Vitali, M., Ferraguti, G., Ceccanti, M., Bertoli, D., Canepa, M., Cappadona, R., D'Alessio, A., Danza, M., Morese, A., Paolino, A., Pileri, F., Pinna, N., Neri, I., Razzano, R., Ricchi, A., and Rizzi, M.

Subjects
alcohol, Fetal Alcohol Spectrum Disorders, health professionals, Health Care Surveys, gravidanza, education, FASD, pregnancy, alcohol, health professionals, Fetal Alcohol Spectrum Disorders, Health Care Surveys, FASD, FASD, gravidanza, alcol, operatori sanitari, operatori sanitari, pregnancy, alcol, NO
Abstract

Fetal Alcohol Spectrum Disorders (FASD) are a plethora of malformative conditions leading to mental retardation that affect newborns and children who have been exposed to alcohol during pregnancy or breastfeeding. FASD is a relevant topic for public health in Europe: European area is first in ranking for alcohol use during pregnancy with a prevalence of 25.2%. Italy ranked third among European countries with higher prevalence of FASD (45.0 per 1000 population). Furthermore, FASD could still be underestimated because of numerous undiagnosed and misdiagnosed cases. Aims of the study were to briefly summarize existing evidences about FASD and its psychiatric aspects to assess knowledge, attitudes and practice towards alcohol drinking during pregnancy in an Italian sample of health care professionals in order to provide information about FASD prevention. An anonymous online questionnaire containing the AUDIT-C, T-ACE model and the Drinking Motive Questionnaire was sent to 400 Italian healthcare professionals and students. The survey included socio-demographic information, questions about drinking habits and about knowledge, attitude and practice towards alcohol assumption during pregnancy. Among 320 respondents, 96.3% were women. AUDIT-C revealed that 52.4% were low risk drinkers but 27.6% were hazardous drinkers. The 90.6% of participants denied to ever attended a course about the fetus damage induced by alcohol consumption during pregnancy but 91.3% were willing to participate to professional update initiatives on the topic. Only 19.1% of participants talk regularly about the deleterious effects for the fetus of prenatal alcohol drinking to women and only 51.1% advise the 'zero alcohol' policy. Around 41% of participants tolerates the assumption of low-alcohol beverages. No differences were found between no drinkers and low and hazardous drinkers. In conclusion, data show that only specific and continuing updating for health care professionals about drinking habits may have impactful actions to prevent gestational alcohol intake in order to prevent the main cause of mental retardation in western countries.

Published
2020
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28. A cross-species and model comparison of the acute toxicity of nanoparticles used in the pigment and ink industries

Author

Brown, D.M., Johnston, H.J., Gaiser, B., Pinna, N., Caputo, G., Çulha, Mustafa, Fernandes, T.F., Brown, D.M., Johnston, H.J., Gaiser, B., Pinna, N., Caputo, G., Çulha, Mustafa, Fernandes, T.F., and Yeditepe Üniversitesi

Subjects
In vitro, technology, industry, and agriculture, Cross-species models, Toxicity testing, Nanoparticles
Abstract

A major user of nanoparticles (NPs) is the pigment and ink industry, where NPs are incorporated into numerous products (e.g. paints, food, plastics, printers, personal care products, and construction materials). Assessment of NP toxicity requires potential impacts on human health and the environment to be evaluated. In this study, we examined the toxicity of a range of NPs, of varied physico-chemical properties, used in the pigment and ink industries including silver (Ag), iron oxide (Fe2O3), titanium dioxide (TiO2), aluminium oxide (Al2O3), zinc oxide (ZnO), cobalt aluminium oxide (CoAl2O4) and cadmium selenide/zinc sulphide (CdSe/ZnS) quantum dots (QDs). Acute toxicity exerted by this NP panel to mammalian cells in vitro (macrophages, hepatocytes and alveolar epithelial cells) and aquatic environmental organisms (Raphidocelis subcapitata Daphnia magna, Lumbriculus variegatus) was investigated. For mammalian cells, cytotoxicity was assessed 24 h post exposure, at concentrations ranging from 1 to 125 µg/ml using the LDH and WST-1 assays. The aquatic toxicity of the NP panel was assessed according to OECD protocols (201, 202, 315), up to 96 h post exposure. Rats were exposed to selected NPs via intratracheal instillation (62 µg) and the pulmonary inflammatory response quantified 24 h post exposure. This cross-species comparison revealed that Ag, QDs and ZnO NPs were consistently more toxic than the other NPs tested. By looking across mammalian and aquatic ecotoxicological models we obtained a better understanding of the sensitivity of each model, and thus which models should be prioritised for selection in the future when assessing the mammalian and ecotoxicity of NPs, and in particular when screening the toxicity of a panel of NPs. We recommend that macrophage and daphnia models are prioritised when assessing the mammalian toxicity and ecotoxicity of NPs, respectively, due to their increased sensitivity, compared to the other models tested. Of interest is that the in vitro and invertebrate models used were able to predict the toxic potency of the NPs in rodents, and thus our approach has the potential to enhance the implementation of the 3Rs principles in nanotoxicology and reduce reliance on rodent testing when assessing NP safety. By identifying hazardous NPs the data obtained from this study can feed into the selection of (low toxicity) NPs to use in products and will also contribute to the safe design of future generations of NPs used by the pigment and ink industries. © 2018 NMP4-SL-2012-280713 This work was supported by the European Commission within the Seventh Framework Programme (2007–2013), policy acronym Nanomicex, grant agreement NMP4-SL-2012-280713 .

Published
2018

30. Single and solid solutions metal carboxyphosphonates as precursors for phosphorous-containing electrocatalysts

Author

López-Vergara, Adrián, El-Refaei, S.M., Russo, P.A., Vilchez, A, Losilla, Enrique R., Porras-Vázquez, José Manuel, Olivera-Pastor, Pascual, Pinna, N, and Cabeza-Diaz, Aurelio

Subjects
Metal phosphonates, Metal phosphides, Elelctrocatalysis, Water splitting, Química inorgánica
Abstract

Co1-xFex-HPAA metal phosphonates were prepared and pyrolyzed under N2 and H2/Ar flows. The result-ing powders were structural and electrochemically characterised by XRD and CV, respectively. The ob-tained materials possess different structures depending on the temperature and pyrolysis atmosphere. Samples pyrolized in N2 at 1000 ºC are monophasic diphosphates, while phosphides form in H2/Ar at 850 ºC. Cyclic voltammetry studies indicate that the Co0.5Fe0.5HPAA sample, pyrolized in H2/Ar, exhibits the best behaviour, but further studies are needed to fully understand the role of graphene oxide and pyrazine. Universidad de Málaga. Campus de Excelencia Internacional Andalucía Tech

Published
2019

31. Anomalous C-V response correlated to relaxation processes in TiO2 thin film based-metal-insulator-metal capacitor: Effect of titanium and oxygen defects.

Author

Kahouli, A., Marichy, C., Sylvestre, A., and Pinna, N.

Subjects
CAPACITANCE-voltage characteristics, TITANIUM dioxide films, METAL-insulator-semiconductor capacitors, TITANIUM, OXYGEN, METAL ions, TEMPERATURE
Abstract

Capacitance-voltage (C-V) and capacitance-frequency (C-f) measurements are performed on atomic layer deposited TiO2 thin films with top and bottom Au and Pt electrodes, respectively, over a large temperature and frequency range. A sharp capacitance peak/discontinuity (C-V anomalous) is observed in the C-V characteristics at various temperatures and voltages. It is demonstrated that this phenomenon is directly associated with oxygen vacancies. The C-V peak irreversibility and dissymmetry at the reversal dc voltage are attributed to difference between the Schottky contacts at the metal/TiO2 interfaces. Dielectric analyses reveal two relaxation processes with degeneration of the activation energy. The low trap level of 0.60-0.65 eV is associated with the first ionized oxygen vacancy at low temperature, while the deep trap level of 1.05 eV is associated to the second ionized oxygen vacancy at high temperature. The DC conductivity of the films exhibits a transition temperature at 200 °C, suggesting a transition from a conduction regime governed by ionized oxygen vacancies to one governed by interstitial Ti3+ ions. Both the C-V anomalous and relaxation processes in TiO2 arise from oxygen vacancies, while the conduction mechanism at high temperature is governed by interstitial titanium ions. [ABSTRACT FROM AUTHOR]

Published
2015
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32. Occurrence of intestinal parasites among asylum seekers in Italy: A cross-sectional study

Author

Fontanelli Sulekova, Lucia, primary, Ceccarelli, Giancarlo, additional, Pombi, Marco, additional, Esvan, Rozenn, additional, Lopalco, Maurizio, additional, Vita, Serena, additional, Mattiucci, Simonetta, additional, Gabrielli, Simona, additional, Bellanca, G., additional, Cavallari, E.G., additional, Gangarossa, G., additional, Kehbuma Dinga, C., additional, Spaziante, M., additional, Amato, E., additional, Bujor, M., additional, Dimitrova, E., additional, Durante, D., additional, Pereda Figueroa, G., additional, Pinna, N., additional, Velez, L., additional, and Walter, I., additional

Published
2019
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35. Record performance Top-down In0.53Ga0.47As vertical nanowire FETs and vertical nanosheets

Author

Ramesh, S., primary, Ivanov, Ts., additional, Putcha, V., additional, Alian, A., additional, Sibaja-Hernandez, A., additional, Rooyackers, R., additional, Camerotto, E., additional, Milenin, A., additional, Pinna, N., additional, Kazzi, S. El, additional, Veloso, A., additional, Lin, D., additional, Lagrain, P., additional, Favia, P., additional, Collaert, N., additional, and De Meyer, K., additional

Published
2017
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38. Stabilization of Titanium Dioxide Nanoparticles at the Surface of Carbon Nanomaterials Promoted by Microwave Heating

Author

Zhang, R, Santangelo, S, Fazio, E, Neri, F, D'Arienzo, M, Morazzoni, F, Zhang, Y, Pinna, N, Russo, P, Russo, P., D'ARIENZO, MASSIMILIANO, MORAZZONI, FRANCA, Zhang, R, Santangelo, S, Fazio, E, Neri, F, D'Arienzo, M, Morazzoni, F, Zhang, Y, Pinna, N, Russo, P, Russo, P., D'ARIENZO, MASSIMILIANO, and MORAZZONI, FRANCA

Abstract

TiO2 is frequently combined with carbon materials, such as reduced graphene oxide (RGO), to produce composites with improved properties, for example for photocatalytic applications. It is shown that heating conditions significantly affect the interface and photocatalytic properties of TiO2@C, and that microwave irradiation can be advantageous for the synthesis of carbon-based materials. Composites of TiO2 with RGO or amorphous carbon were prepared from reaction of titanium isopropoxide with benzyl alcohol. During the synthesis of the TiO2 nanoparticles, the carbon is involved in reactions that lead to the covalent attachment of the oxide, the extent of which depends on the carbon characteristics, heating rate, and mechanism. TiO2 is more efficiently stabilized at the surface of RGO than amorphous carbon. Rapid heating of the reaction mixture results in a stronger coupling between the nanoparticles and carbon, more uniform coatings, and smaller particles with narrower size distributions. The more efficient attachment of the oxide leads to better photocatalytic performance. Microwave heating promotes the covalent attachment of titanium dioxide particles to carbon nanomaterials. This method is more effective than conventional methods. The structures with the stabilized oxide show improved photocatalytic properties.

Published
2015

44. Carboxylic Acids as Oxygen Supplying Agents for Atomic Layer Deposition of Oxide Thin Films

Author

Rauwel, E., Ducroquet, F., Rauwel, P., Willinger, M.-G., Matko, I., Pinna, N., Laboratoire des matériaux et du génie physique (LMGP ), Institut polytechnique de Grenoble - Grenoble Institute of Technology (Grenoble INP )-Institut National Polytechnique de Grenoble (INPG)-Institut de Chimie du CNRS (INC)-Centre National de la Recherche Scientifique (CNRS), Institut de Microélectronique, Electromagnétisme et Photonique - Laboratoire d'Hyperfréquences et Caractérisation (IMEP-LAHC), Université Joseph Fourier - Grenoble 1 (UJF)-Institut polytechnique de Grenoble - Grenoble Institute of Technology (Grenoble INP )-Institut National Polytechnique de Grenoble (INPG)-Université Savoie Mont Blanc (USMB [Université de Savoie] [Université de Chambéry])-Centre National de la Recherche Scientifique (CNRS), Commissariat à l'énergie atomique et aux énergies alternatives - Laboratoire d'Electronique et de Technologie de l'Information (CEA-LETI), Direction de Recherche Technologique (CEA) (DRT (CEA)), Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-Commissariat à l'énergie atomique et aux énergies alternatives (CEA), Institut National Polytechnique de Grenoble (INPG)-Institut polytechnique de Grenoble - Grenoble Institute of Technology (Grenoble INP )-Institut de Chimie du CNRS (INC)-Centre National de la Recherche Scientifique (CNRS), and Université Joseph Fourier - Grenoble 1 (UJF)-Institut polytechnique de Grenoble - Grenoble Institute of Technology (Grenoble INP )-Université Savoie Mont Blanc (USMB [Université de Savoie] [Université de Chambéry])-Institut National Polytechnique de Grenoble (INPG)-Centre National de la Recherche Scientifique (CNRS)

Subjects
[PHYS.COND.CM-GEN]Physics [physics]/Condensed Matter [cond-mat]/Other [cond-mat.other], ComputingMilieux_MISCELLANEOUS
Abstract

International audience

Published
2010

50. Carboxylic acids as oxygen supplying agents for ALD of high k thin films

Author

Rauwel, E., Ducroquet, F., Rauwel, P., Willinger, M.-G., Matko, I., Pinna, N., Institut de Microélectronique, Electromagnétisme et Photonique - Laboratoire d'Hyperfréquences et Caractérisation (IMEP-LAHC), Université Joseph Fourier - Grenoble 1 (UJF)-Institut polytechnique de Grenoble - Grenoble Institute of Technology (Grenoble INP )-Université Savoie Mont Blanc (USMB [Université de Savoie] [Université de Chambéry])-Institut National Polytechnique de Grenoble (INPG)-Centre National de la Recherche Scientifique (CNRS), and Domenget, Chahla

Subjects
[SPI.NANO] Engineering Sciences [physics]/Micro and nanotechnologies/Microelectronics, [SPI.NANO]Engineering Sciences [physics]/Micro and nanotechnologies/Microelectronics, ComputingMilieux_MISCELLANEOUS
Abstract

International audience

Published
2008

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