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13. Bonding strength and thermal shock resistance of a novel bilayer (c‐AlPO4‐SiCw‐mullite)/SiC coated carbon fiber reinforced CMCs.

Author

Chen, Pengju, Xiao, Peng, Li, Zhuan, Pan, Ling, Li, Jinwei, Liu, Zeyan, Pu, Dongmei, and Li, Yang

Subjects
THERMAL shock, THERMAL resistance, BOND strengths, CARBON fibers, ALUMINUM phosphate, SOL-gel materials, CRYSTAL whiskers
Abstract

Mullite coating, SiC whiskers toughened mullite coating (SiCw‐mullite), and cristobalite aluminum phosphate (c‐AlPO4) particle modified SiCw‐mullite coating (c‐AlPO4‐SiCw‐mullite) were prepared on SiC coated C/SiC composites using a novel sol‐gel method combined with air spraying. Results show that molten SiO2 formed by the oxidation of SiC whiskers and molten c‐AlPO4 improved the bonding strength between mullite outer coating and SiC–C/SiC composites due to their high‐temperature bonding properties. The bonding strength between mullite, SiCw‐mullite, c‐AlPO4‐SiCw‐mullite outer coatings and SiC–C/SiC composites were 2.41, 4.31, and 7.38 MPa, respectively. After 48 thermal cycles between 1773 K and room temperature, the weight loss of mullite/SiC coating coated C/SiC composites was up to 11.61%, while the weight losses of SiCw‐mullite/SiC and c‐AlPO4‐SiCw‐mullite/SiC coatings coated C/SiC composites were reduced to 7.40% and 5.12%, respectively. The addition of appropriate SiC whiskers can considerably improve the thermal shock resistance of mullite coating owing to their excellent mechanical properties at high temperature. In addition, c‐AlPO4 particles can further improve the thermal shock resistance of SiCw‐mullite coating due to their high‐temperature bonding and sealing properties. No obvious micro‐pores and cracks were observed on the surface of c‐AlPO4‐SiCw‐mullite coating after 48 thermal cycles due to timely healing effect by formation of secondary mullite. [ABSTRACT FROM AUTHOR]

Published
2020
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17. Effect of Ti particles on microstructure and mechanical properties of TiP/AZ91 composites

Author

Pu, Dongmei, Wu, Shifen, Yang, Hong, Chen, Xianhua, Li, Jianbo, Feng, Xiaowei, Zheng, Kaihong, and Pan, Fusheng

Abstract

Ti particles (5 wt.%) reinforced AZ91 Mg matrix composites (TiP/AZ91 composites) were prepared by powder metallurgy. As a result, the strength and ductility of TiP/AZ91 composites were improved compared with AZ91 alloy. The ultimate tensile stress (UTS) increased significantly from 163 MPa to 221 MPa, and the elongation increased from 3.5% to 10.9%. The YS and hardness decreased due to the slightly coarser grain size. The microstructural results showed that Ti particles were uniformly dispersed in the Mg matrix and the content of Mg17Al12was reduced, indicating that Ti particles can inhibit the precipitation of the second phase. The interface between Ti particle and Mg matrix showed that the Al3Ti layer was formed at the edge of the Ti particles. EBSD was used to analyze the twins and dislocations at different tensile strains. During the tensile deformation at room temperature, many tensile twins and dislocations formed in the TiP/AZ91 composites. The tensile twins and dislocations could coordinate plastic deformation, thus improving the elongation of the TiP/AZ91 composites.

Published
2022
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