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In this work, an ingredient containing non-starch polysaccharides (NSP), obtained from overripe bananas, was characterized using differential scanning calorimetry (DSC) and vapor sorption isotherms. Soluble sugars from overripe bananas were extracted using ethanol, resulting in a solid NSP-rich fraction. The physical properties of this new ingredient and its response to temperature and water interactions are needed for its application as a fiber flour aggregate in food preparations. Results from thermal analyses, including gelatinization, glass transition and fusion, allowed building state diagrams, then compared to vapor sorption isotherms which resulted similar to a Brunauer-Emmet-Teller (BET) type III isotherm at 25 °C, for NSP and standards samples as arabinoxylan and polygalacturonic acid. A good fit was obtained for the glass transition curves using the Kwei model. This approach enabled us to explore the stability of the material, regarding safety limits for microbial deterioration and structural changes due to glass transition., (Copyright © 2021 Elsevier Ltd. All rights reserved.)

Banana has non-starch polysaccharides (NSP) in its cell wall similar to dietary fiber from cereals like oats. These NSP could be used as potential functional ingredient due to their prebiotic action and potential food immuno-modulators. However, NSP purification is limited due to high quantities of soluble sugars accumulate during banana ripening. The aim of this study was to extract soluble sugars from ripe banana (Musa cavendishii var. Nanicão) to obtain a purified NSP matrix. Two different extraction methodologies (solid-liquid extraction SLE and ultrasound-assisted extraction UAE) were tested using ethanol (99.5 mL/100 mL) as solvent. Soluble sugars were quantified by high-performance liquid chromatography (HPLC). SLE and UAE showed to be effective in extraction process of soluble sugars. Best results were obtained with SLE at sample/solvent ratio of 1:5, 65 °C and 30 min of extraction time. A solid residue with NSP was obtained, that could be used as a functional ingredient., (Copyright © 2019 Elsevier Ltd. All rights reserved.)