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Usually for non-destructive testing at high temperatures, ultrasonic transducers made of PZT and silver electrodes are used, but this could lead to damage to or malfunction of the ultrasonic transducer due to poor adhesion between PZT and silver. Soldering is one of the most common types of bonding used for individual parts of ultrasonic transducers (protector, backing, matching layer, etc.), but silver should be protected using additional metal layers (copper) due to its solubility in solder. A mathematical modelling could help to predict if an ultrasonic transducer was manufactured well and if it could operate up to 225 °C. The observed von Mises stresses were very high and concentrated in metal layers (silver and copper), which could lead to disbonding under long-term cyclic temperature loads. This paper presents a multilayer ultrasonic transducer (PZT, silver electrodes, copper layers, backing), which was heated evenly from room temperature to 225 °C and then cooled down. In the B-scan, it was observed that the amplitude of the reflected signal from the bottom of the sample decreased with an increase in temperature. However, after six heating–cooling cycles, the results repeated themselves and no signs of fatigue were noticed. This ultrasonic transducer was well manufactured and could be used for non-destructive testing when the environment temperature changes in cycles up to 225 °C.

An ultrasonic technique, invariant to temperature changes, for a density measurement of different liquids under in situ extreme conditions is presented. The influence of geometry and material parameters of the measurement system (transducer, waveguide, matching layer) on measurement accuracy and reliability is analyzed theoretically along with experimental results. The proposed method is based on measurement of the amplitude of the ultrasonic wave, reflected from the interface of the solid/liquid medium under investigation. In order to enhance sensitivity, the use of a quarter wavelength acoustic matching layer is proposed. Therefore, the sensitivity of the measurement system increases significantly. Density measurements quite often must be performed in extreme conditions at high temperature (up to 220 °C) and high pressure. In this case, metal waveguides between piezoelectric transducer and the measured liquid are used in order to protect the conventional transducer from the influence of high temperature and to avoid depolarization. The presented ultrasonic density measurement technique is suitable for density measurement in different materials, including liquids and polymer melts in extreme conditions. A new calibration algorithm was proposed. The metrological evaluation of the measurement method was performed. The expanded measurement uncertainty Uρ = 7.4 × 10−3 g/cm3 (1%).

Ultrasonic non-destructive testing techniques (NDT) based on the application of guided waves are already used for inspection of plate-type structures made of various materials, including composite materials. Air-coupled ultrasonic techniques are used to test such structures by means of guided waves. The objective of this research was development and investigation of air-coupled excitation of a slow A0 Lamb wave mode in thin plastic films by a PMN-32%PT ultrasonic array. It is known that when the velocity of the A0 mode in the film is less than the ultrasound velocity in air no leaky wave is observed in a surrounding air. It opens new possibilities for NDT of composite structures. The influence of the airborne wave may be eliminated by 3D filtering in a wavenumbers-frequency domain. A special filter and corresponding signals processing technique were developed in order to obtain directivity patterns and velocity maps of the waves propagating in all directions. The measured ultrasound velocity values prove that, with the proposed method, it is possible to excite a slow A0 Lamb wave mode and to separate it from other parasitic waves propagating in air. Measurements of the parameters of the slow A0 mode, such as the propagation velocity in the plastic film, may be applied for the material characterization.

For improvement of the efficiency of air-coupled ultrasonic transducers PMN-32%PT piezoelectric crystals which possess very high piezoelectric properties may be used. The electromechanical coupling factor of such crystals for all main vibration modes such as the thickness extension and transverse extension modes is more than 0.9. Operation of ultrasonic transducers with such piezoelectric elements in transmitting and receiving modes is rather different. Therefore, for transmission and reception of ultrasonic signals, separate piezoelectric elements with different dimensions must be used. The objective of this research was development of novel air-coupled ultrasonic receivers with PMN-32%PT strip-like piezoelectric elements vibrating in a transverse-extension mode with electromechanically controlled operation and suitable for applications in ultrasonic arrays. Performance of piezoelectric receivers made of the PMN-32%PT strip-like elements vibrating in this mode may be efficiently controlled by selecting geometry of the electrodes covering side surfaces of the piezoelectric element. It is equivalent to introduction of electromechanical damping which does not require any additional backing element. For this purpose; we have proposed the continuous electrodes to divide into two pairs of electrodes. The one pair is used to pick up the electric signal; another one is exploited for electromechanical damping. Two types of electrodes may be used—rectangular or non-rectangular—with a gap between them directed at some angle, usually 45°. The frequency bandwidth is wider (up to 9 kHz) in the case of non-rectangular electrodes. The strip-like acoustic matching element bonded to the tip of the PMN-32%PT crystal may significantly enhance the performance of the ultrasonic receiver. It was proposed to use for this purpose AIREX T10.110 rigid polymer foam, the acoustic impedance of which is close to the optimal value necessary for matching with air. It was found that in order to get a wide bandwidth the length of the matching strip should be selected not a quarter wavelength λ/4 at the antiresonance frequency but at lower frequency. It allowed achieving the frequency bandwidth (14–18)% with respect to the central frequency at −3 dB level.

Air-coupled ultrasonic techniques are being increasingly used for material characterization, non-destructive evaluation of composite materials using guided waves as well as for distance measurements. Application of those techniques is mainly limited by the big losses of ultrasonic signals due to attenuation and mismatch of the acoustic impedances of ultrasonic transducers and air. One of the ways to solve this problem is by application of novel more efficient piezoelectric materials like lead magnesium niobate-lead titanate (PMN-PT) type crystals. The objective of this research was the development and investigation of low frequency (