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1. Development of a method to measure trace level of uranium and thorium in scintillation films

Author

Ichimura, K., Chiba, K., Gando, Y., Ikeda, H., Kishimoto, Y., Kurasawa, M., Nemoto, K., Sakaguchi, A., Takaku, Y., and Sakakieda, Y.

Subjects
Physics - Instrumentation and Detectors
Abstract

We have established a method to measure picograms-per-gram (pg g$^{-1}$) levels of $^{238}$U and $^{232}$Th in scintillation films by combining the dry ashing method and inductively coupled plasma mass spectrometry. Trace amounts of $^{238}$U and $^{232}$Th were measured in up to 2~g of the scintillation film with almost 100% collection efficiency. This paper details the experimental procedure, including the pretreatment of the samples and labware, detection limit of the method, collection efficiencies of $^{238}$U and $^{232}$Th, and measurement of $^{238}$U and $^{232}$Th in a polyethylene naphthalate film. This method is also applicable to $^{238}$U and $^{232}$Th measurements in other low-background organic materials for rare event search experiments.

Published
2024
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2. Second gadolinium loading to Super-Kamiokande

Author

Abe, K., Bronner, C., Hayato, Y., Hiraide, K., Hosokawa, K., Ieki, K., Ikeda, M., Kameda, J., Kanemura, Y., Kaneshima, R., Kashiwagi, Y., Kataoka, Y., Miki, S., Mine, S., Miura, M., Moriyama, S., Nakano, Y., Nakahata, M., Nakayama, S., Noguchi, Y., Sato, K., Sekiya, H., Shiba, H., Shimizu, K., Shiozawa, M., Sonoda, Y., Suzuki, Y., Takeda, A., Takemoto, Y., Tanaka, H., Yano, T., Han, S., Kajita, T., Okumura, K., Tashiro, T., Tomiya, T., Wang, X., Yoshida, S., Fernandez, P., Labarga, L., Ospina, N., Zaldivar, B., Pointon, B. W., Kearns, E., Raaf, J. L., Wan, L., Wester, T., Bian, J., Griskevich, N. J., Smy, M. B., Sobel, H. W., Takhistov, V., Yankelevich, A., Hill, J., Jang, M. C., Lee, S. H., Moon, D. H., Park, R. G., Bodur, B., Scholberg, K., Walter, C. W., Beauchene, A., Drapier, O., Giampaolo, A., Mueller, Th. A., Santos, A. D., Paganini, P., Quilain, B., Rogly, R., Nakamura, T., Jang, J. S., Machado, L. N., Learned, J. G., Choi, K., Iovine, N., Cao, S., Anthony, L. H. V., Martin, D., Prouse, N. W., Scott, M., Uchida, Y., Berardi, V., Calabria, N. F., Catanesi, M. G., Radicioni, E., Langella, A., De Rosa, G., Collazuol, G., Iacob, F., Mattiazzi, M., Ludovici, L., Gonin, M., Perisse, L., Pronost, G., Fujisawa, C., Maekawa, Y., Nishimura, Y., Okazaki, R., Akutsu, R., Friend, M., Hasegawa, T., Ishida, T., Kobayashi, T., Jakkapu, M., Matsubara, T., Nakadaira, T., Nakamura, K., Oyama, Y., Sakashita, K., Sekiguchi, T., Tsukamoto, T., Bhuiyan, N., Burton, G. T., Di Lodovico, F., Gao, J., Goldsack, A., Katori, T., Migenda, J., Ramsden, R. M., Xie, Z., Zsoldos, S., Suzuki, A. T., Takagi, Y., Takeuchi, Y., Zhong, H., Feng, J., Feng, L., Hu, J. R., Hu, Z., Kawaue, M., Kikawa, T., Mori, M., Nakaya, T., Wendell, R. A., Yasutome, K., Jenkins, S. J., McCauley, N., Mehta, P., Tarant, A., Wilking, M. J., Fukuda, Y., Itow, Y., Menjo, H., Ninomiya, K., Yoshioka, Y., Lagoda, J., Mandal, M., Mijakowski, P., Prabhu, Y. S., Zalipska, J., Jia, M., Jiang, J., Shi, W., Yanagisawa, C., Harada, M., Hino, Y., Ishino, H., Koshio, Y., Nakanishi, F., Sakai, S., Tada, T., Tano, T., Ishizuka, T., Barr, G., Barrow, D., Cook, L., Samani, S., Wark, D., Holin, A., Nova, F., Jung, S., Yang, B. S., Yang, J. Y., Yoo, J., Fannon, J. E. P., Kneale, L., Malek, M., McElwee, J. M., Thiesse, M. D., Thompson, L. F., Wilson, S. T., Okazawa, H., Lakshmi, S. M., Kim, S. B., Kwon, E., Seo, J. W., Yu, I., Ichikawa, A. K., Tairafune, S., Nishijima, K., Eguchi, A., Nakagiri, K., Nakajima, Y., Shima, S., Taniuchi, N., Watanabe, E., Yokoyama, M., de Perio, P., Fujita, S., Jesus-Valls, C., Martens, K., Tsui, K. M., Vagins, M. R., Xia, J., Izumiyama, S., Kuze, M., Matsumoto, R., Terada, K., Ishitsuka, M., Ito, H., Ommura, Y., Shigeta, N., Shinoki, M., Yamauchi, K., Yoshida, T., Gaur, R., Gousy-Leblanc, V., Hartz, M., Konaka, A., Li, X., Chen, S., Xu, B. D., Zhang, B., Posiadala-Zezula, M., Boyd, S. B., Edwards, R., Hadley, D., Nicholson, M., O'Flaherty, M., Richards, B., Ali, A., Jamieson, B., Amanai, S., Marti, Ll., Minamino, A., Suzuki, S., Scovell, P. R., Meehan, E., Bandac, I., Pena-Garay, C., Perez, J., Gileva, O., Lee, E. K., Leonard, D. S., Sakakieda, Y., Sakaguchi, A., Sueki, K., Takaku, Y., and Yamasaki, S.

Subjects
Physics - Instrumentation and Detectors, Astrophysics - High Energy Astrophysical Phenomena
Abstract

The first loading of gadolinium (Gd) into Super-Kamiokande in 2020 was successful, and the neutron capture efficiency on Gd reached 50\%. To further increase the Gd neutron capture efficiency to 75\%, 26.1 tons of $\rm Gd_2(\rm SO_4)_3\cdot \rm 8H_2O$ was additionally loaded into Super-Kamiokande (SK) from May 31 to July 4, 2022. As the amount of loaded $\rm Gd_2(\rm SO_4)_3\cdot \rm 8H_2O$ was doubled compared to the first loading, the capacity of the powder dissolving system was doubled. We also developed new batches of gadolinium sulfate with even further reduced radioactive impurities. In addition, a more efficient screening method was devised and implemented to evaluate these new batches of $\rm Gd_2(\rm SO_4)_3\cdot \rm 8H_2O$. Following the second loading, the Gd concentration in SK was measured to be $333.5\pm2.5$ ppm via an Atomic Absorption Spectrometer (AAS). From the mean neutron capture time constant of neutrons from an Am/Be calibration source, the Gd concentration was independently measured to be 332.7 $\pm$ 6.8(sys.) $\pm$ 1.1(stat.) ppm, consistent with the AAS result. Furthermore, during the loading the Gd concentration was monitored continually using the capture time constant of each spallation neutron produced by cosmic-ray muons,and the final neutron capture efficiency was shown to become 1.5 times higher than that of the first loaded phase, as expected., Comment: 34 pages, 13 figures, submitted to Nuclear Inst. and Methods in Physics Research, A

Published
2024
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3. Rapid Analysis of $\mathrm{^{226}Ra}$ in Ultrapure Gadolinium Sulfate Octahydrate

Author

Sakakieda, Y., Hosokawa, K., Nakanishi, F., Hino, Y., Inome, Y., Sakaguchi, A., Takaku, Y., Ikeda, M., and Sekiya, H.

Subjects
Physics - Instrumentation and Detectors
Abstract

Numerous particle physics experiments utilize gadolinium (Gd), a rare earth element with the most significant neutron capture cross-section among all elements, to detect anti-neutrinos via inverse beta-decays or to remove neutron-induced background events. For example, to load Gd into water Cherenkov detectors, $\mathrm{{Gd_{2}(SO_{4})_{3}\cdot 8H_{2}O}}$ is dissolved and rare event search experiments are required to screen for radioactive impurities in $\mathrm{{Gd_{2}(SO_{4})_{3}\cdot 8H_{2}O}}$ before dissolution. This study developed a new method to rapidly measure the radium-226($\mathrm{^{226}Ra}$) concentration in $\mathrm{{Gd_{2}(SO_{4})_{3}\cdot 8H_{2}O}}$. This method requires only three days to measure a batch of samples, as opposed to the usual method using high-purity germanium detectors, which takes approximately 20 days after arrival. The detection limit for the measurement of $\mathrm{^{226}Ra}$ is 0.32 mBq/kg. This method has been already used for $\mathrm{{Gd_{2}(SO_{4})_{3}\cdot 8H_{2}O}}$ screening at the Super-Kamiokande Gd(SK-Gd) project, and it can be applied to future experiments., Comment: 10 pages, 3 figures

Published
2023

4. Second gadolinium loading to Super-Kamiokande

Author

Abe, K., primary, Bronner, C., additional, Hayato, Y., additional, Hiraide, K., additional, Hosokawa, K., additional, Ieki, K., additional, Ikeda, M., additional, Kameda, J., additional, Kanemura, Y., additional, Kaneshima, R., additional, Kashiwagi, Y., additional, Kataoka, Y., additional, Miki, S., additional, Mine, S., additional, Miura, M., additional, Moriyama, S., additional, Nakano, Y., additional, Nakahata, M., additional, Nakayama, S., additional, Noguchi, Y., additional, Sato, K., additional, Sekiya, H., additional, Shiba, H., additional, Shimizu, K., additional, Shiozawa, M., additional, Sonoda, Y., additional, Suzuki, Y., additional, Takeda, A., additional, Takemoto, Y., additional, Tanaka, H., additional, Yano, T., additional, Han, S., additional, Kajita, T., additional, Okumura, K., additional, Tashiro, T., additional, Tomiya, T., additional, Wang, X., additional, Yoshida, S., additional, Fernandez, P., additional, Labarga, L., additional, Ospina, N., additional, Zaldivar, B., additional, Pointon, B.W., additional, Kearns, E., additional, Raaf, J.L., additional, Wan, L., additional, Wester, T., additional, Bian, J., additional, Griskevich, N.J., additional, Smy, M.B., additional, Sobel, H.W., additional, Takhistov, V., additional, Yankelevich, A., additional, Hill, J., additional, Jang, M.C., additional, Lee, S.H., additional, Moon, D.H., additional, Park, R.G., additional, Bodur, B., additional, Scholberg, K., additional, Walter, C.W., additional, Beauchêne, A., additional, Drapier, O., additional, Giampaolo, A., additional, Mueller, Th.A., additional, Santos, A.D., additional, Paganini, P., additional, Quilain, B., additional, Rogly, R., additional, Nakamura, T., additional, Jang, J.S., additional, Machado, L.N., additional, Learned, J.G., additional, Choi, K., additional, Iovine, N., additional, Cao, S., additional, Anthony, L.H.V., additional, Martin, D., additional, Prouse, N.W., additional, Scott, M., additional, Uchida, Y., additional, Berardi, V., additional, Calabria, N.F., additional, Catanesi, M.G., additional, Radicioni, E., additional, Langella, A., additional, De Rosa, G., additional, Collazuol, G., additional, Iacob, F., additional, Mattiazzi, M., additional, Ludovici, L., additional, Gonin, M., additional, Périssé, L., additional, Pronost, G., additional, Fujisawa, C., additional, Maekawa, Y., additional, Nishimura, Y., additional, Okazaki, R., additional, Akutsu, R., additional, Friend, M., additional, Hasegawa, T., additional, Ishida, T., additional, Kobayashi, T., additional, Jakkapu, M., additional, Matsubara, T., additional, Nakadaira, T., additional, Nakamura, K., additional, Oyama, Y., additional, Sakashita, K., additional, Sekiguchi, T., additional, Tsukamoto, T., additional, Bhuiyan, N., additional, Burton, G.T., additional, Di Lodovico, F., additional, Gao, J., additional, Goldsack, A., additional, Katori, T., additional, Migenda, J., additional, Ramsden, R.M., additional, Xie, Z., additional, Zsoldos, S., additional, Suzuki, A.T., additional, Takagi, Y., additional, Takeuchi, Y., additional, Zhong, H., additional, Feng, J., additional, Feng, L., additional, Hu, J.R., additional, Hu, Z., additional, Kawaue, M., additional, Kikawa, T., additional, Mori, M., additional, Nakaya, T., additional, Wendell, R.A., additional, Yasutome, K., additional, Jenkins, S.J., additional, McCauley, N., additional, Mehta, P., additional, Tarant, A., additional, Wilking, M.J., additional, Fukuda, Y., additional, Itow, Y., additional, Menjo, H., additional, Ninomiya, K., additional, Yoshioka, Y., additional, Lagoda, J., additional, Mandal, M., additional, Mijakowski, P., additional, Prabhu, Y.S., additional, Zalipska, J., additional, Jia, M., additional, Jiang, J., additional, Shi, W., additional, Yanagisawa, C., additional, Harada, M., additional, Hino, Y., additional, Ishino, H., additional, Koshio, Y., additional, Nakanishi, F., additional, Sakai, S., additional, Tada, T., additional, Tano, T., additional, Ishizuka, T., additional, Barr, G., additional, Barrow, D., additional, Cook, L., additional, Samani, S., additional, Wark, D., additional, Holin, A., additional, Nova, F., additional, Jung, S., additional, Yang, B.S., additional, Yang, J.Y., additional, Yoo, J., additional, Fannon, J.E.P., additional, Kneale, L., additional, Malek, M., additional, McElwee, J.M., additional, Thiesse, M.D., additional, Thompson, L.F., additional, Wilson, S.T., additional, Okazawa, H., additional, Lakshmi, S.M., additional, Kim, S.B., additional, Kwon, E., additional, Seo, J.W., additional, Yu, I., additional, Ichikawa, A.K., additional, Tairafune, S., additional, Nishijima, K., additional, Eguchi, A., additional, Nakagiri, K., additional, Nakajima, Y., additional, Shima, S., additional, Taniuchi, N., additional, Watanabe, E., additional, Yokoyama, M., additional, de Perio, P., additional, Fujita, S., additional, Jesús-Valls, C., additional, Martens, K., additional, Tsui, K.M., additional, Vagins, M.R., additional, Xia, J., additional, Izumiyama, S., additional, Kuze, M., additional, Matsumoto, R., additional, Terada, K., additional, Ishitsuka, M., additional, Ito, H., additional, Ommura, Y., additional, Shigeta, N., additional, Shinoki, M., additional, Yamauchi, K., additional, Yoshida, T., additional, Gaur, R., additional, Gousy-Leblanc, V., additional, Hartz, M., additional, Konaka, A., additional, Li, X., additional, Chen, S., additional, Xu, B.D., additional, Zhang, B., additional, Posiadala-Zezula, M., additional, Boyd, S.B., additional, Edwards, R., additional, Hadley, D., additional, Nicholson, M., additional, O’Flaherty, M., additional, Richards, B., additional, Ali, A., additional, Jamieson, B., additional, Amanai, S., additional, Marti, Ll., additional, Minamino, A., additional, Suzuki, S., additional, Scovell, P.R., additional, Meehan, E., additional, Bandac, I., additional, Peña-Garay, C., additional, Pérez, J., additional, Gileva, O., additional, Lee, E.K., additional, Leonard, D.S., additional, Sakakieda, Y., additional, Sakaguchi, A., additional, Sueki, K., additional, Takaku, Y., additional, and Yamasaki, S., additional

Published
2024
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