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Droplet impact on a granular layer results in various morphologies of the liquid–grain mixture. Some are concentrated and highly curved, some are extended and flatter. No matter how the morphology looks from the top, it is generally believed that its bottom is tightly connected to the concavely deformed granular target. In this paper we report the discovery of a hidden cavity below a droplet residual, formed upon impact on packings of hydrophilic grains and exposed by X-ray tomography. Its occurrence in the parameter space is explored. We elucidate the mechanism leading to this counterintuitive phenomenon using a dual-curvature model and an energy criterion. This research may shed new light onto the ongoing discussion about the origin of the so-called fossilized raindrop impressions.

A two-dimensional granular packing under horizontally circular shaking exhibits various collective motion modes depending on the strength of the oscillation and the global packing density. For intermediate packing density and oscillation amplitude, a high density phase travels along the container's side wall in clockwise direction, while the oscillation itself is anti-clockwise. Further increasing packing density towards the hexagonal packing, the whole packing rotates collectively in clockwise direction. The core of the packing rotates as a solid and is separated from the boundary by a fluid-like layer. Both motion modes are associated with the asymmetric motion of particles close to the side wall., 9 pages, 2 figures

How does the impact of a deformable droplet on a granular bed differ from that caused by a solid impactor of similar size and density? Here, we experimentally study this question and focus on the effect of intruder deformability on the crater shape. For comparable impact energies, we show that the crater diameter is larger for droplets than for solid intruders but that the impact of the latter results in deeper craters. Interestingly, for initially dense beds of packing fractions larger than 0.58, we find that the resultant excavated crater volume is independent of the intruder deformability, suggesting an impactor-independent dissipation mechanism within the sand for these dense beds.

Additive manufacturing strives to combine any combination of materials into 3D functional structures and devices, ultimately opening up the possibility of 3D printed machines. It remains difficult to actuate such devices, thus limiting the scope of 3D printed machines to passive devices or necessitating the incorporation of external actuators that are manufactured differently. Here, 3D printed hybrid thermoplast/conducter bilayers are explored, which can be actuated by differential heating caused by externally controllable currents flowing through their conducting faces. The functionality of such actuators is uncovered and it is shown that they allow to 3D print, in one pass, simple flexible robotic structures that propel forward under step-wise applied voltages. Moreover, exploiting the thermoplasticity of the nonconducting plastic parts at elevated temperatures, it is shown that how strong driving leads to irreversible deformations—a form of 4D printing—which also enlarges the range of linear response of the actuators. Finally, it is shown that how to leverage such thermoplastic relaxations to accumulate plastic deformations and obtain very large deformations by alternatively driving both layers of a bilayer; this is called ratcheting. The strategy is scalable and widely applicable, and opens up a new approach to reversible actuation and irreversible 4D printing of arbitrary structures and machines.

We study here the spontaneous clustering of a submonolayer of grains under horizontal circular shaking. The clustering of grains occurs when increasing the oscillation amplitude beyond a threshold. The dense area travels in a circular fashion at the driving frequency, even exceeds the speed of driving. It turns out that the observed clustering is due to the formation of density wave. The analysis of a phenomenological model shows that the instability of the uniform density profile arises by increasing the oscillation amplitude and captures the non-monotonic dependence of the transition amplitude of the clustering on the global density of the system. Here, the key ingredient is that the velocity of individual grains increases with the local density. The interplay of dissipative particle-particle interaction and the frictional driving of the substrate results into this dependence, which is tested with discrete element method simulations., 10 pages, 5 figures

Would a raindrop impacting on a coarse beach behave differently from that impacting on a desert of fine sand? We study this question by a series of model experiments, where the packing density of the granular target, the wettability of individual grains, the grain size, the impacting liquid, and the impact speed are varied. We find that by increasing the grain size and/or the wettability of individual grains the maximum droplet spreading undergoes a transition from a capillary regime towards a viscous regime, and splashing is suppressed. The liquid-grain mixing is discovered to be the underlying mechanism. An effective viscosity is defined accordingly to quantitatively explain the observations.

After a raindrop impacts on a granular bed, a crater is formed as both drop and target deform. After an initial, transient, phase in which the maximum crater depth is reached, the crater broadens outwards until a final steady shape is attained. By varying the impact velocity of the drop and the packing density of the bed, we find that avalanches of grains are important in the second phase and hence, affect the final crater shape. In a previous paper, we introduced an estimate of the impact energy going solely into sand deformation and here we show that both the transient and final crater diameter collapse with this quantity for various packing densities. The aspect ratio of the transient crater is however altered by changes in the packing fraction., 9 pages, 9 figures

International audience; We extend the Widom particle insertion method [B. Widom, J. Chem. Phys., 1963, 39, 2808-2812] to determine an upper bound s(ub) on the Edwards entropy in frictional hard-sphere packings. s(ub) corresponds to the logarithm of the number of mechanically stable configurations for a given volume fraction and boundary conditions. To accomplish this, we extend the method for estimating the particle insertion probability through the pore-size distribution in frictionless packings [V. Baranau, et al., Soft Matter, 2013, 9, 3361-3372] to the case of frictional particles. We use computer-generated and experimentally obtained three-dimensional sphere packings with volume fractions phi in the range 0.551-0.65. We find that sub has a maximum in the vicinity of the Random Loose Packing Limit phi(RLP) = 0.55 and decreases then monotonically with increasing phi to reach a minimum at phi = 0.65. Further on, sub does not distinguish between real mechanical stability and packings in close proximity to mechanical stable configurations. The probability to find a given number of contacts for a particle inserted in a large enough pore does not depend on phi, but it decreases strongly with the contact number

As a droplet impacts upon a granular substrate, both the intruder and the target undergo deformation, during which the liquid may penetrate into the substrate. These three aspects together distinguish it from other impact phenomena in the literature. We perform high-speed, double-laser profilometry measurements and disentangle the dynamics into three aspects: the deformation of the substrate during the impact, the maximum spreading diameter of the droplet, and the penetration of the liquid into the substrate. By systematically varying the impact speed and the packing fraction of the substrate, (i) the substrate deformation indicates a critical packing fraction [curly or open phi]* ≈ 0.585; (ii) the maximum droplet spreading diameter is found to scale with a Weber number corrected by the substrate deformation; and (iii) a model of the liquid penetration is established and is used to explain the observed crater morphology transition.

Jammed packings of granular materials differ from systems normally described by statistical mechanics in that they are athermal. In recent years a statistical mechanics of static granular media has emerged where the thermodynamic temperature is replaced by a configurational temperature X which describes how the number of mechanically stable configurations depends on the volume. Four different methods have been suggested to measure X. Three of them are computed from properties of the Voronoi volume distribution, the fourth takes into account the contact number and the global volume fraction. This paper answers two questions using experimental binary disc packings: First we test if the four methods to measure compactivity provide identical results when applied to the same dataset. We find that only two of the methods agree quantitatively. Secondly, we test if X is indeed an intensive variable; this becomes true only for samples larger than roughly 200 particles. This result is shown to be due to recently found correlations between the particle volumes [Zhao et al., Europhys. Lett., 2012, 97, 34004]., Comment: Open access under Creative Commons Attribution-NonCommercial 3.0 license

We measure the two-point correlation of free Voronoi volumes in binary disc packings, where the packing fraction $\phi_{\rm avg}$ ranges from 0.8175 to 0.8380. We observe short-ranged correlations over the whole range of $\phi_{\rm avg}$ and anti-correlations for $\phi_{\rm avg}>0.8277$. The spatial extent of the anti-correlation increases with $\phi_{\rm avg}$ while the position of the maximum of the anti-correlation and the extent of the positive correlation shrink with $\phi_{\rm avg}$. We conjecture that the onset of anti-correlation corresponds to dilatancy onset in this system.

Raman spectra have been measured on iron-based quaternary CeO$_{1-x}$F$_x$FeAs and LaO$_{1-x}$F$_x$FeAs with varying fluorine doping at room temperatures. A group analysis has been made to clarify the optical modes. Based on the first principle calculations, the observed phonon modes can be assigned accordingly. In LaO$_{1-x}$F$_x$FeAs, the E$_g$ and A$_{1g}$ modes related to the vibrations of La, are suppressed with increasing F doping. However F doping only has a small effect on the E$_g$ and A$_{1g}$ modes of Fe and As. The Raman modes of La and As are absent in rare-earth substituted CeO$_{1-x}$F$_x$FeAs, and the E$_g$ mode of oxygen, corresponding to the in-plane vibration of oxygen, moves to around 450 cm$^{-1}$ and shows a very sharp peak. Electronic scattering background is low and electron-phonon coupling is not evident for the observed phonon modes. Three features are found above 500 cm$^{-1}$, which may be associated with multi-phonon process. Nevertheless it is also possible that they are related to magnetic fluctuations or interband transitions of d orbitals considering their energies., Comment: 12 pages, 3 figures, 2 tables