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Abstract In this publication, an in-process quality assurance method for electron beam welding based on a structure-borne sound emission test for the detection of weld irregularities arising in the process is presented. For this purpose, different sheet materials, i.e., AISI 304, AZ31 and AlMg3, were welded in a butt-joint and the resulting process noises were recorded by means of two acoustic emission sensors specifically designed for structure-borne sound. During the welding experiments, typical irregularities, e.g. incidence points, pore lines and cracks, were deliberately induced. Subsequently, the recorded acoustic signals were examined with regard to defect-specific abnormalities. Various methods in the time and frequency domain as well as pre-trained machine learning models were used to analyze the acoustic emission data. The results show that the investigated irregularities can be identified and distinguished from other process emissions, eventually enabling a robust means of identification for weld seam irregularities and, thus, opening pathways towards cost-effective in-process quality control.

IntroductionIn production forests, management can have cascading effects on biodiversity and ecosystem services. Acoustic diversity reflects the diversity of vocalizing animals and has also considerable recreational value for human well-being, but the relationship between acoustic diversity and forest management remains largely unexploredMethodWe recorded acoustic diversity on forest plots along a gradient of silvicultural management intensity (SMI) in three regions of Germany. We explored the diurnal and seasonal temporal dynamics in acoustic diversity index (ADI) from March to July using generalized additive mixed models (GAMMs). We further investigated the interrelation between acoustic diversity and silvicultural management intensity, forest structural diversity, as well as tree diversity, bird species richness and abundance using structural equation modeling (SEM).ResultsSilvicultural management intensity had significant effects on the temporal dynamics of ADI in May and June from dawn till dusk, but variance explained by SMI was low. We confirmed our hypothesis that ADI was reduced by SMI due to its cascading effects on forest structural diversity and bird species richness and abundance.DiscussionAcoustic diversity indices can provide valuable insights into how forest management affects the acoustic activity of soniferous communities. We discuss how this can indicate both changes in species diversity as well as their vocal activity. We further address potential implications for forest management.

Abstract Zinc nitride (Zn3N2) is a promising semiconductor for a range of optoelectronic and energy conversion applications, offering a direct bandgap of 1.0 eV, large carrier mobilities, and abundant constituent elements. However, the material is prone to bulk oxidation in ambient environments, which has thus far impeded its practical deployment. While previous approaches have focused on stabilizing the material via integration of ZnO surface layers, these strategies introduce additional challenges regarding elevated processing temperatures and limited control of interface properties. In this study, it is shown that amorphous GaN thin films can serve as highly stable protection layers on Zn3N2 surfaces and can be deposited at the same growth temperature and in the same deposition system as the underlying semiconductor. The GaN‐capped Zn3N2 structures exhibit long‐term stability, surviving over 3 years of exposure to ambient conditions with no discernible alterations in composition, structure, or electrical properties. Notably, the amorphous GaN coatings can even impede Zn3N2 oxidation under prolonged aqueous exposure. Thus, this study offers a solution to stabilize Zn3N2 in ambient conditions, providing a viable pathway to its utilization in robust and high‐performance electronic devices, such as thin film transistors and solar energy conversion systems.

In modified production landscapes, biodiversity faces unprecedented pressures from human actions, resulting in significant species declines of plant and animal taxa, including birds. Understanding the underlying mechanisms responsible for such declines is essential to counteract further loss and support practitioners in conserving biodiversity and associated ecosystem function. In this study, we used standardized bird monitoring data collected over 6 years in managed forest and grassland areas across different regions in Germany, Central Europe. We combined these data with morphometric, ecological, behavioral, and acoustic trait data and detailed information on local land use management practices to understand how management decisions affect species and functional diversity, as well as ecological processes shaping local species composition. Our results reveal that the ecosystem and regional context must be considered to understand how management practices affect bird diversity aspects and composition. In forests, regional management decisions related to tree species and stand age affected bird diversity, as well as community and functional composition, and indicated environmental sorting due to ecological and behavioral requirements, biotic interactions, and morphometric constraints. In grasslands, independent of local management practices, increased intensity of land use resulted in an overall loss in bird species richness and functional diversity. Predominantly, constraints due to ecological or behavioral requirements affected bird species assemblage composition. In addition, our results indicated the importance of woody vegetation near managed grasslands and of considering environmental conditions beyond the local scale to support bird diversity and associated ecosystem functions. Our results highlighted that local management decisions can support bird diversity and maintain ecological function. However, this needs a view beyond the local scale of management units. It also demands a joint effort of biologists and land managers to integrate targeted conservation actions into regional management practices and create a network of habitats within production landscapes to protect nature, guard against biotic and functional homogenization, and prevent further degradation of ecosystems in production landscapes.

Forest birds respond to a diverse set of environmental factors, including those altered by forest management intensity, such as resource and habitat availability in the form of food or nesting sites. Although resource/habitat availability and bird traits likely mediate responses of bird diversity to global change drivers, no study has assessed the direct and indirect effects of changes in forest management and traits on bird assemblages jointly at large spatial scales. In this context the questions remain whether (1) the birds' response to forest management changes through alterations in structural properties and/or food availability, or (2) if birds' eco-morphological traits act as environmental filters in response to environmental factors. We audio-visually recorded birds at 150 forest plots in three regions of Germany and assessed the forest structure (LiDAR) as well as the diversity of the herbaceous layer and diversity and biomass of arthropods. We further assessed eco-morphological traits of the birds and tested if effects on bird assemblages are mediated by changes in eco-morphological traits' composition. We found that abundance and species numbers of birds are explained best by models including the major environmental factors, forest structure, plants, and arthropods. Eco-morphological traits only increased model fit for indirect effects on abundance of birds. We found minor differences between the three regions in Germany, indicating spatial congruency of the processes at the local and regional scale. Our results suggest that most birds are not specialized on a particular food type, but that the size, diversity and species composition of arthropods are important. Our findings question the general view that bird traits adapt to the resources available.

In the present investigation, commercially pure titanium is welded to AISI 316L stainless steel by intermixing niobium as filler material in a lap joint configuration. For this purpose, a pulsed Nd:YAG laser with various pulse durations and pulse peak powers is employed to obtain different mixing conditions for the materials. It will be demonstrated that, despite the implementation of the filler material, the weld seams are characterized by a high affinity for cracking, which in turn can be attributed to the formation of hard intermetallic compounds. Nevertheless, utilization of optimized process parameters can yield crack-free specimens in a reproducible manner through equable intermixing of otherwise critical alloy elements. Lap-shear forces of up to 140 N can be achieved with a single weld seam measuring 2.5 mm in length. By increasing the joint area with four adjacent weld seams, maximum loads up to 320 N are attained, thus exceeding the yield strength of the applied stainless steel. Considering the biocompatibility of the niobium filler material used, this work provides the foundation for this dissimilar material combination to be implemented in future medical technology applications.

Despite the formation of a passive layer, corrosion also occurs in austenitic stainless steels. One of the most common and most dangerous types is pitting corrosion, in which the material beneath the surface is completely dissolved. Since this type of corrosion only produces small holes on the surface, it is difficult to detect without nondestructive testing. This paper presents induction-excited shearography as an optical, nondestructive testing method for quick inspection of inner defects and corrosion. The investigations were carried out on test specimens with blind holes made of austenitic stainless steel 1.4301 (AISI 304). The detection limits of different defect sizes were determined objectively based on the signal-to-noise ratio (SNR). The results show that inner defects with a size of Ø 2 mm can be detected via SNR in a depth of up to 1.5 mm. Larger defects can be detected in greater depth. The data obtained were validated on real test specimens. The measurement of a more realistic defect geometry showed higher SNR values compared to the idealized test specimens. From the measured SNR values of realistic defect geometry, it can be concluded that real irregularities have higher SNR values than defects with flat bottoms. The results show that induction-excited shearography is suitable for the nondestructive testing of austenitic stainless steels.

The present study provides an overview of previous studies on the welding of the AA7075-T6 aluminum alloy, followed by an investigation of the influence of short-time solution annealing on the mechanical properties of the weld. Conventional laser welding of Al-Zn-alloys leads to a low weld strength, which makes a post weld heat treatment (PWHT) favorable. The PWHT includes solution annealing, quenching and subsequent aging. For solution annealing, different holding times and cooling rates are investigated in this study. The focus of the investigation is on a short solution annealing time, which on the one hand is ecological and economically favorable and on the other hand offers great potential for inline heat treatments. The shortest solution annealing time of 10 s shows a significant increase in weld strength (joint efficiency of 72%), compared to the non-heat treated weld (joint efficiency of 52%). The microstructural analysis reveals that the cooling rate after solution heat treatment affects the formation of precipitates in the microstructure of the welded AA7075 alloy. Moreover, the enhancement of mechanical properties is related to the formation of Mg-Al-Cu and Mg-Zn rich precipitates.

The intergranular corrosion susceptibility of ferritic stainless-steel weldments is strongly dependent on chromium carbide precipitation phenomena. Hence, stabilization is widely used to mitigate the aforementioned precipitation. In contrast, stabilization has proved ineffective to fully prevent intergranular corrosion due to segregation of unreacted chromium during solid-state heat-treatments. To analyze the precipitation behavior of 17 wt.-% chromium ferritic stainless steels during laser welding, sheets of unstabilized and titanium-stabilized ferritic stainless steels were welded in a butt joint configuration and characterized with special consideration of precipitation behavior by means of transmission electron microscopy. While unstabilized ferritic stainless steels exhibit pronounced chromium precipitate formation at grain boundaries, titanium-stabilization leads to titanium precipitates without adjacent chromium segregation. However, corrosion tests reveal three distinctive corrosion mechanisms within the investigated ferritic stainless steels based on their inherent precipitation behaviors. In light of the precipitation formation, it is evident that immersion in sulfuric acid media leads to the dissolution of either grain boundaries or the grain boundary vicinity. As a result, the residual mechanical strength of the joint is substantially degraded.

Ferritic stainless steels are prone to localized corrosion phenomena such as pitting corrosion or intergranular corrosion, in particular when jointed by fusion welding processes. State-of-the-art techniques to avoid intergranular corrosion mainly consist of alternating alloy concepts or post-weld heat-treatments—all of which are associated with increased production costs. Hence, the present investigation seeks to introduce a novel approach for the inhibition of intergranular corrosion in ferritic stainless steel welds through the use of high-speed laser cladding. Here, vulnerable sites prone to intergranular corrosion along the weld seam area are coated with a chemically resistant alloy, whereby an overlap is achieved. Optical and electron microscopy as well as computer tomography and tensile tests reveal that the detrimental effects of intergranular corrosion in both stabilized and unstabilized ferritic stainless steel are substantially reduced. In addition to that, the effects of varying overlap widths on the identified corrosion phenomena are studied. Moreover, the resulting dilution and precipiation phenomena at the clad–sheet interface are thoroughly characterized by electron backscatter diffraction and energy dispersive X-ray spectroscopy, whereby interrelationships to corrosion resistance can be drawn. As a result of this investigation, the number of techniques for the inhibition of intergranular corrosion is enlarged, and substantial cost-saving potentials in the manufacturing industry are unlocked.

In the present study, compositionally-graded structures of AISI 316L and CoCrMo alloy are manufactured by powder-based laser-beam directed energy deposition (DED-LB). Through a process-integrated adjustment of powder flow, in situ alloying of the two materials becomes feasible. Thus, a sharp and a smooth transition with a mixture of both alloys can be realized. In order to investigate the phase formation during in situ alloying, a simulation approach considering equilibrium calculations is employed. The findings reveal that a precise compositional as well as functional gradation of the two alloys is possible. Thereby, the chemical composition can be directly correlated with the specimen hardness. Moreover, phases, which are identified by equilibrium calculations, can also be observed experimentally using scanning electron microscopy (SEM) and energy-dispersive X-ray-spectroscopy (EDS). Electron backscatter diffraction (EBSD) reveals epitaxial grain growth across the sharp transition region with a pronounced -texture, while the smooth transition acts as nucleus for the growth of new grains with -orientation. In light of envisaged applications in the biomedical sector, the present investigation demonstrates the high potential of an AISI 316L/CoCrMo alloy material combination.

Friction stir welding has become important in many areas of production and is increasingly used for joining aluminum components. For long welding seams, conventional tools with only one welding pin reach their technical limitations due to low gap bridgeability. When welding aluminum, the stirred in surface layers, such as oxides, lead to a decrease in static and dynamic strength since linear accumulations are formed in the welding seam. The aim of the present study is to increase the gap bridgeability using tools with various welding pins and to prevent linear accumulation in the welding seam. The results show that a gap bridgeability of up to 2 mm for 4 mm material thickness is possible for the aluminum alloys EN AW 5083 H111 and EN AW 7020 T651. With the help of multi-pin tools, no impact of the gap width on the tensile strength was observed for joint gaps of up to 0.9 mm when using butt joint with a sheet thickness of 4 mm. Furthermore, the use of multi-pin tools showed significant influence on the prevention of linear accumulations in the welding seam. In addition, the oxide layers were finely distributed in welded joints using multi-pin tools.

In the investigation at hand, sheets of ferritic and pearlitic grey cast iron with spheroidal graphite are welded using a fiber-laser. The influence of varying laser power and welding speed on the macroscopic characteristics of the weld seam and crack formation are analyzed and discussed. Substantial crack formation with crack densities of up to 2.93 cm−1 are found. Furthermore, hardness measurements are conducted to evaluate the formation of brittle phases within the weld metal and heat-affected zone. Peak hardness values of up to 860 HV0.3 and 975 HV0.3 are identified in EN-GJS-400-15 and EN-GJS-700-2, respectively. Subsequently, a proposition on the dependence of crack formation on weld seam width is given. Furthermore, the influence of nickel-containing filler material on the microstructure, crack formation and hardness is studied. It can be derived from the results that laser-beam welding of grey cast iron with spheroidal graphite requires further research in order to achieve crack-free weld seams and hinder the formation of undesirable, brittle phases.

Collision welding is a high-speed joining technology based on the plastic deformation of at least one of the joining partners. During the process, several phenomena like the formation of a so-called jet and a cloud of particles occur and enable bond formation. However, the interaction of these phenomena and how they are influenced by the amount of kinetic energy is still unclear. In this paper, the results of three series of experiments with two different setups to determine the influence of the process parameters on the fundamental phenomena and relevant mechanisms of bond formation are presented. The welding processes are monitored by different methods, like high-speed imaging, photonic Doppler velocimetry and light emission measurements. The weld interfaces are analyzed by ultrasonic investigations, metallographic analyses by optical and scanning electron microscopy, and characterized by tensile shear tests. The results provide detailed information on the influence of the different process parameters on the classical welding window and allow a prediction of the different bond mechanisms. They show that during a single magnetic pulse welding process aluminum both fusion-like and solid-state welding can occur. Furthermore, the findings allow predicting the formation of the weld interface with respect to location and shape as well as its mechanical strength.

In the present investigation, thin sheets of stabilized and unstabilized ferritic stainless steel were welded in butt joint configuration using irradiation of a 1070 nm fiber-laser. Using optical microscopy, the microstructural evolution upon alternating heat input was characterized. In addition to that, hardness and tensile tests were carried out on the specimens. Detailed focus was given to the intergranular corrosion properties, which were investigated on basis of the Strauss test with different times of exposure to the corrosive environment. Following these tests, the mechanical properties of the joints were characterized using tensile tests. A combination of the latter with an inspection by μ-CT analysis allows for the proposition of an intergranular corrosion rate with regard to the degradation of the joint strength.

Collision welding processes are accompanied by the ejection of a metal jet, a cloud of particles (CoP), or both phenomena, respectively. The purpose of this study is to investigate the formation, the characteristics as well as the influence of the CoP on weld formation. Impact welding experiments on three different setups in normal ambient atmosphere and under vacuum-like conditions are performed and monitored using a high-speed camera, accompanied by long-term exposures, recordings of the emission spectrum, and an evaluation of the CoP interaction with witness pins made of different materials. It was found that the CoP formed during the collision of the joining partners is compressed by the closing joining gap and particularly at small collision angles it can reach temperatures sufficient to melt the surfaces to be joined. This effect was proved using a tracer material that is detectable on the witness pins after welding. The formation of the CoP is reduced with increasing yield strength of the material and the escape of the CoP is hindered with increasing surface roughness. Both effects make welding with low-impact velocities difficult, whereas weld formation is facilitated using smooth surfaces and a reduced ambient pressure under vacuum-like conditions. Furthermore, the absence of surrounding air eases the process observation since exothermic oxidation reactions and shock compression of the gas are avoided. This also enables an estimation of the temperature in the joining gap, which was found to be more than 5600 K under normal ambient pressure.

In a bandsaw machine, the blade guides provide additional stiffness and help to align the blade near the cutting region. Typically, these are either in the form of blocks made of carbide or ceramics or as sealed bearings. Abrasive particles, generated while cutting hard and brittle materials like natural stones, settle between the contact surfaces of the guides and the blade causing wear and premature failure. The hydrostatic guide system, as presented in this work, is a contactless blade guiding method that uses the force of several pressurized water jets to align the blade to the direction of the cut. For this investigation, cutting tests were performed on a marble block using a galvanic diamond coated bandsaw blade with the upper roller guides replaced by hydrostatic guides. The results show that the hydrostatic guides help to reduce the passive force to a constant near zero in contrast with the traditional guides. This also resulted in reduced surface roughness of the stone plates that were cut, indicating a reduction in laterial vibration of the band. Additionally, it has also been shown that using hydrostatic guides the bandsaw blade can be tilted to counter the bandsaw drift, opening opportunities for further research in active alignment control. This original research work has shown that the hydrostatic guide systems are capable of replacing, and in fact, perform better than state-of-the-art bearing or block guides, particularly for stone-cutting applications.

Additive manufacturing (AM) is an advanced manufacturing process that provides the opportunity to build geometrically complex and highly individualized lightweight structures. Despite its many advantages, additively manufactured components suffer from poor surface quality. To locally improve the surface quality and homogenize the microstructure, friction stir processing (FSP) technique was applied on Al-Si12 components produced by selective laser melting (SLM) using two different working media. The effect of FSP on the microstructural evolution, mechanical properties, and corrosion resistance of SLM samples was investigated. Microstructural investigation showed a considerable grain refinement in the friction stirred area, which is due to the severe plastic deformation and dynamic recrystallization of the material in the stir zone. Micro-hardness measurements revealed that the micro-hardness values of samples treated using FSP are much lower compared to SLM components in the as-built condition. This reduction of hardness values in samples treated with FSP can be explained by the dissolution of the very fine Si-phase network, being characteristic for SLM samples, during FSP. Surface topography also demonstrated that the FSP results in the reduction of surface roughness and increases the homogeneity of the SLM microstructure. Decreased surface roughness and grain size refinement in combination with the dissolved Si-phase network of the FSP treated material result in considerable changes in corrosion behavior. This work addresses the corrosion properties of surface treated additive manufactured Al-Si12 by establishing adequate microstructure-property relationships. The corrosion behavior of SLM-manufactured Al-Si12 alloys is shown to be improved by FSP-modification of the surfaces.

The high-strength aluminum alloys offer great potential for realizing lightweight constructions in car body construction. However, the use of aluminum alloys increases the overall thickness of the material, which poses new challenges for potential joining processes. This paper examines a process combination of friction stir spot welding (FSSW) and bonding for 4 mm EN AW 6082-T6 sheets. For the investigations, adhesive or glass beads were applied between the joining components and then the sheets were welded using FSSW. The analysis shows that the adhesive and the glass beads have a very small influence on the joint formation. The use of glass beads in FSSW with bonding is recommended because less adhesive is displaced from the joint area, which increases the joint strength. The target of obtaining high weld spot strengths without strength-reducing adhesive burn-off could not be achieved because a certain residence time is necessary to form a weld spot with high strength at this sheet thickness in order to sufficiently plasticize the material. Adhesive burn-up cannot be completely avoided. For this reason, it is necessary to weigh up which characteristics are required for the specific application and adjust the welding parameters accordingly.

The effect of micro patterning of cemented carbide surface using nanosecond diode pumped solid-state pulsed laser on the strength of induction brazed carbide and steel joints has been investigated. Surface patterns increase the total surface area of the joint and, for an originally hydrophilic surface, increase the wettability of a liquid on a solid surface such that, instead of building droplets, the liquid spreads and flows on the surface. Microcomputed tomography (µ-CT) was used to observe the filler/carbide interface after brazing and to analyze the presence of porosity or remnant flux in the joint. Microstructures of the brazed joints with various surface patterns were analyzed using scanning electron microscopy. The strength of the joints was measured using shear tests. Results have shown that the groove pattern on the surface of carbide increases the joint strength by 70−80%, whereas, surface patterns of bi-directional grooves (grid) reduced the joint strength drastically. Dimples on the carbide surface did not show any improvement in the strength of the brazed joints compared to samples with no surface pattern.

Although the joining of aluminum and copper is a difficult task, several studies have shown that friction stir welding (FSW) is capable of producing aluminum-copper-joints with excellent performance. Therefore, it is desirable to use this joining technique for the production of cost- and weight-reduced conductors for the automotive sector. The exposed copper contact spots in automobiles are usually coated with tin for design reasons and in order to improve their corrosion resistance. In this context, it is possible to perform the weld at first and to coat afterwards, or to weld already coated copper workpieces. Taking this into account, this paper presents results on the influence of copper-sided tinning on the joint formation as well as the achievable mechanical and electrical properties of friction stir butt welded aluminum-copper joints. Two variants were considered. The first variant included copper blanks with a tinned surface. For the second variant the surface and the abutting edge of the copper were coated. The best welds achieved excellent electrical properties and their tensile strength was only slightly reduced compared to the aluminum base material. Thus, it was shown that if these tensile strength losses are acceptable, FSW of aluminum to tin coated copper is applicable.

Producing joints of aluminum and copper by means of fusion welding is a challenging task. However, the results of various studies have proven the potential of friction stir welding (FSW) for manufacturing aluminum-copper joints. Despite the proven feasibility, there is currently no series application in automotive industry to produce aluminum-copper joints for electrical contacts by means of FSW. To make FSW as efficient as possible for large-scale production, maximized welding speed is desired. Taking this into account, this paper presents results of a parametric investigation, the objective of which was to increase the welding speed for FSW of aluminum and copper in comparison to welding speeds that are considered to be state of the art. Taguchi method was used to design an experimental plan and target figures of the investigations were the resultant tensile strengths and electrical resistances. Dependencies between input parameters and target figures were determined systematically. The optimal welding parameters, at which joints failed in the weaker aluminum material, included a welding speed of 700 mm/min. Consequently, it could be shown that joints with a performance similar to those of the base materials can be obtained using significantly higher welding speeds than reported in the relevant literature.