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29. Effect of rare earth Y on microstructure and texture of oriented silicon steel during hot rolling and cold rolling processes

Author

Zhu Liguang, Li Xiangyang, Zheng Yaxu, Guo Zhihong, Zhang Yuanxiang, Sun Huilan, Liu Pengjun, Liu Yu, and Cao Ruifang

Subjects
oriented silicon steel, rare earth y, hot rolling, cold rolling, texture, precipitates, Technology, Chemical technology, TP1-1185, Chemicals: Manufacture, use, etc., TP200-248
Abstract

The effect of rare earth Y on precipitates and textures of the grain-oriented silicon steels, the composition, morphology, size, quantity of inclusions and texture evolution of hot-rolled and cold-rolled oriented silicon steel containing rare earth Y were studied using transmission electron microscopy, field emission scanning electron microscope, and electron backscatter diffraction. The results show that there are mainly spherical or ellipsoidal Y2O2S precipitates in the Y bearing silicon steel. Rare earth treatment effectively improves the precipitates’ morphology and restrains the precipitation of the long-strip MnS in the hot-rolled plate. Meanwhile, the microstructure is more uniform, and the recrystallized grains on the surface and the fiber structure in the central layer are larger after hot rolling compared with Y-free steel. Furthermore, with the addition of rare earth Y, the unfavorable brass texture and rotational cube texture in the hot-rolled plate are reduced. Meanwhile, the number of shear bands is increased and the strength of the favorable {111} 〈112〉 texture is improved in the cold-rolled plate, which helps develop the Goss texture during the annealing process.

Published
2022
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41. Effect of cold-rolling deformation and rare earth yttrium on microstructure and texture of oriented silicon steel

Author

Guo Zhihong, Liu Pengjun, Zheng Yaxu, Zhu Liguang, Zhang Yuanxiang, Sun Huilan, Li Xiangyang, Liu Yu, and Cao Ruifang

Subjects
oriented silicon steel, cold rolling, rare earth y, texture, Technology, Chemical technology, TP1-1185, Chemicals: Manufacture, use, etc., TP200-248
Abstract

In order to study the effect of cold-rolling deformation and rare earth Y on the microstructure and texture of 3.0% Si-oriented silicon steel, the microstructure and texture of cold-rolled oriented silicon steel with 60, 72, and 86% deformation are analyzed using electron backscatter diffraction and image analysis software. The experimental results show that the deformation band becomes narrower and the distribution of shear bands becomes denser with increasing cold-rolling deformation. Compared to the Y-free steel, cold-rolled sheet containing rare earth Y has greater shear bands. The pinning effect of rare earth Y hinders the dislocation movement, which leads to the increase of kernel average misorientation value and shear bands. With the increase of cold-rolling deformation, the texture concentrates on α and λ. This is mainly due to the change from {100} 〈001〉 to {001} 〈110〉, intensifying λ texture, and the change from {111} 〈112〉 to {111} 〈110〉, thus strengthening the α texture. The texture strength of cold-rolled sheets can be decreased by rare earth Y. But the γ texture strength in cold-rolled sheets containing Y is significantly higher than in those without Y. The γ texture strength can reach up to 7.3, and the strong points are mainly {111} 〈112〉. This is because the number of inclusions in steel increases with the addition of rare earth Y. In the process of grain nucleation, the {111} oriented grains nucleate heterogeneously on the inclusions. It forms a large number of {111} oriented grains and improves the γ texture strength.

Published
2023
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49. Carbon Mediated Multifunctional Sb2Se3–WSe2 Heterostructure Nanofiber Facilitates Rapid and Stable Na+ Transport.

Author

Wang, Jian, Zhang, Di, Wang, Qiujun, Sun, Qujiang, Sun, Huilan, Li, Zhaojin, Woo, Haw Jiunn, Ramesh, S., and Wang, Bo

Abstract

Alloying metal selenides as advanced anode materials for sodium‐ion devices requires overcoming the challenges of high diffusion energy barriers and large volume expansion at high‐power densities. The typical dealloying process is difficult to trigger under fast kinetics, leading to limited capacity utilization. Here, Sb/W‐hybridization precursor is synthesized by one‐step reaction, followed by electrostatic spinning strategy to achieve a localized domain‐limiting effect. Finally, the carbon mediated Sb2Se3–WSe2 heterostructure nanofiber (SbWSe/C/NF) are obtained after carbonization/selenization process. Physical characterization and theoretical calculations reveal that the SbWSe/C/NF‐500 has a heterogeneous structure and abundant edge carbon defects, facilitating rapid Na+ transfer from exterior to interior. Furthermore, compared with the Sb2Se3/C monomer, the SbWSe/C heterostructure shows a significant dealloying reaction at high current densities, enhancing capacity utilization. Resultantly, the Na half‐cell with SbWSe/C/NF‐500 electrode demonstrates excellent rate capability and a high specific capacity of 553.7 mA h g−1 after 250 cycles at 2 A g−1. Meanwhile, the assembled sodium‐ion capacitor exhibits 80.83% capacity retention after 8000 cycles at 3800 W kg−1. The structure design strategy of cationic heterostructures with dual‐carbon introduction provides a reference for developing high‐power anodes. [ABSTRACT FROM AUTHOR]

Published
2024
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