1. Laser-based powder bed fusion of niobium with different build-up rates
- Author
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Stefan Kaierle, Arvid Abel, Markus Weinmann, Christian Hoff, Tjorben Griemsmann, and Jörg Hermsdorf
- Subjects
0209 industrial biotechnology ,Materials science ,Scanning electron microscope ,Mechanical Engineering ,Niobium ,chemistry.chemical_element ,02 engineering and technology ,021001 nanoscience & nanotechnology ,Microstructure ,Indentation hardness ,Industrial and Manufacturing Engineering ,Computer Science Applications ,020901 industrial engineering & automation ,Volume (thermodynamics) ,chemistry ,Control and Systems Engineering ,Ultimate tensile strength ,Vickers hardness test ,Relative density ,Composite material ,0210 nano-technology ,Software - Abstract
Niobium is an important material for high temperature applications, in space, in superconductors or in chemical process constructions. Laser-based powder bed fusion of niobium (PBF-LB/M/Nb) offers new opportunities in design, though it is still an expensive technique. The build-up rate is an important factor for economical manufacturing using PBF-LB/M/Nb. It is largely influenced by variation of process parameters, affecting the heat flow during the manufacturing process. In this work, an empirical model for PBF-LB/M/Nb is developed. Based on this model, manufacturing parameter sets using different volume build-up rates are predicted and confirmed. They enable the manufacture of parts with homogeneous and crack-free microstructure with more than 99.9% relative density. Tensile and hardness tests of specimens, which were manufactured using different parameter sets, are performed to determine the effects of the build-up rate—and thus the heat flow during manufacturing—on different mechanical properties. The ultimate tensile strength and yield strength of as-manufactured specimens reach values up to 525 MPa and 324 MPa, respectively, while the elongation at break ranges between approximately 8 and 16%. The Vickers hardness of all specimens was in the range of 149 ± 8 HV0.1. In addition, the microstructure of the manufactured samples is investigated by means of light as well as scanning electron microscopy.
- Published
- 2021
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