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Binary interactions have been proposed to explain a variety of circumstellar structures seen around evolved stars, including asymptotic giant branch (AGB) stars and planetary nebulae. Studies resolving the circumstellar envelopes of AGB stars have revealed spirals, discs and bipolar outflows, with shaping attributed to interactions with a companion. For the first time, we have used a combined chemical and dynamical analysis to reveal a highly eccentric and long-period orbit for W Aquilae, a binary system containing an AGB star and a main sequence companion. Our results are based on anisotropic SiN emission, the first detections of NS and SiC towards an S-type star, and density structures observed in the CO emission. These features are all interpreted as having formed during periastron interactions. Our astrochemistry-based method can yield stringent constraints on the orbital parameters of long-period binaries containing AGB stars, and will be applicable to other systems., Comment: This version of the article has been accepted for publication, after peer review (when applicable) and is subject to Springer Nature's AM terms of use, but is not the Version of Record and does not reflect post-acceptance improvements, or any corrections. The Version of Record is available online at: https://doi.org/10.1038/s41550-023-02154-y

The dusty winds of cool evolved stars are a major contributor of the newly synthesised material enriching the Galaxy and future generations of stars. However, the details of the physics and chemistry behind dust formation and wind launching have yet to be pinpointed. Recent spatially resolved observations show the importance of gaining a more comprehensive view of the circumstellar chemistry, but a comparative study of the intricate interplay between chemistry and physics is still difficult because observational details such as frequencies and angular resolutions are rarely comparable. Aiming to overcome these deficiencies, ATOMIUM is an ALMA Large Programme to study the physics and chemistry of the circumstellar envelopes of a diverse set of oxygen-rich evolved stars under homogeneous observing conditions at three angular resolutions between ~0.02"-1.4". Here we summarize the molecular inventory of these sources, and the correlations between stellar parameters and molecular content. Seventeen oxygen-rich or S-type asymptotic giant branch (AGB) and red supergiant (RSG) stars have been observed in several tunings with ALMA Band 6, targeting a range of molecules to probe the circumstellar envelope and especially the chemistry of dust formation close to the star. We systematically assigned the molecular carriers of the spectral lines and measured their spectroscopic parameters and the angular extent of the emission of each line from integrated intensity maps. Across the ATOMIUM sample, we detect 291 transitions of 24 different molecules and their isotopologues. This includes several first detections in oxygen-rich AGB/RSG stars: PO v=1, SO2 v1=1 and v2=2, and several high energy H2O transitions. We also find several first detections in S-type AGB stars: vibrationally excited HCN v2=2,3 and SiS v=4,5,6, as well as first detections of the molecules SiC, AlCl, and AlF in W Aql..., Comment: 19 pages plus appendices, forthcoming publication in Astronomy & Astrophysics

Water and the hydroxyl radical are major constituents of the envelope of O-rich late-type stars. Transitions involving energy levels that are highly excited have been observed in both H$_2$O and OH. These and more recently discovered transitions can now be observed at a high sensitivity and angular resolution with the ALMA Array. Spectra and maps of H$_2$O and OH observed with an angular resolution of 20 to $\sim$200 mas were obtained at two epochs with the ALMA array. Observations with the Compact Array were also used to check for time variability of water transitions. Radiative transfer models of water were revisited to characterize masing conditions and up-to-date chemical models were used for comparison with our observations. Ten rotational transitions of H$_2$O with energies up to 9000 K were observed in various vibrational states. All but one are new detections in space, and from these we have derived accurate rest frequencies. Hyperfine split $\Lambda$-doubling transitions in v = 0, J = 27/2 and 29/2 levels of the $^2\Pi_{3/2}$ state and, $J = 33/2$ and 35/2 of the $^2\Pi_{1/2}$ state of OH with excitation energies up to 8900 K were also observed. Four of these transitions are new detections in space. Combining our measurements with earlier observations of OH, the v = 0 and v = 1 $\Lambda$-doubling frequencies have been improved. Our H$_2$O maps show compact emission and extensions up to twelve stellar radii or more. The 268.149 GHz emission line of water in the v$_2$ = 2 state is time variable, tends to be masing with dominant radiative pumping, and is widely excited. The widespread but weaker 262.898 GHz water line in v$_2$ = 1 also shows signs of maser emission. Emission and absorption of both H$_2$O and OH reveal an infall of matter and complex kinematics influenced by binarity. From our observed column densities, we derived OH/H$_2$O abundance ratios in a few stars., Comment: 41 pages with references and 25 figures in main text. 4 Tables in Appendix A. 10 figures in Appendix B. 2 figures in Appendix C. 14 figures in Appendix D. 5 figures in Appendix E. 2 figures in Appendix F

Aims. Through the ATOMIUM project, based on an ALMA large program, we aim to present a consistent view of a sample of 17 nearby cool evolved stars (Aymptotic Giant Branch and red supergiant stars). Methods. Here we present VLT/SPHERE-ZIMPOL polarimetric maps obtained in the visible of 14 out of the 17 ATOMIUM sources. They were obtained contemporaneously with the ALMA high spatial resolution data. To help interpret the polarized signal, we produced synthetic maps of light scattering by dust, through 3D radiative transfer simulations with the RADMC3D code. Results. The degree of linear polarization (DoLP) observed by ZIMPOL spreads across several optical filters. We infer that it primarily probes dust located just outside of the point spread function, and in or near the plane of the sky, with a total optical depth close to unity in the line of sight, representing only a fraction of the total circumstellar dust. The maximum DoLP ranges from 0.03-0.38 depending on the source, fractions that can be reproduced by our 3D pilot models for grains composed of common dust species. The spatial structure of the DoLP shows a diverse set of shapes. Only for three sources do we note a correlation between the ALMA CO and SiO lines, which trace the gas density, and the DoLP, which traces the dust. Conclusion. The clumpiness of the DoLP and the lack of a consistent correlation between the gas and the dust location show that, in the inner circumstellar environment (CSE), dust formation occurs at very specific sites. This has potential consequences for the derived mass-loss rates and dust-to-gas ratio in the inner region of the CSE. Except for $\pi^1$~Gru and perhaps GY Aql, we do not detect interactions between the circumstellar wind and the hypothesized companions that shape the wind at larger scales. This suggests that the orbits of any other companions are tilted out of the plane of the sky., Comment: Accepted for publication in Astronomy & Astrophysics. 22 pages, 15 figures, 5 tables

This overview paper presents ATOMIUM, a Large Programme in Cycle 6 with the Atacama Large Millimeter-submillimeter Array (ALMA). The goal of ATOMIUM is to understand the dynamics and the gas phase and dust formation chemistry in the winds of evolved asymptotic giant branch (AGB) and red supergiant (RSG) stars. A more general aim is to identify chemical processes applicable to other astrophysical environments. 17 oxygen-rich AGB and RSG stars spanning a range in (circum)stellar parameters and evolutionary phases were observed in a homogeneous observing strategy allowing for an unambiguous comparison. Data were obtained between 213.83 and 269.71 GHz at high (0.025-0.050 arcsec), medium (0.13-0.24 arcsec), and low (about 1 arcsec) angular resolution. The sensitivity per 1.3 km/s channel was 1.5-5 mJy/beam. 13 molecules were designated as primary molecules in the survey: CO, SiO, AlO, AlOH, TiO, TiO2, HCN, SO, SO2, SiS, CS, H2O, and NaCl. The scientific motivation, survey design, sample properties, data reduction, and an overview of the data products are described; and we highlight one scientific result - the wind kinematics of the ATOMIUM sources. The ATOMIUM sources often have a slow wind acceleration, and a fraction of the gas reaches a velocity which can be up to a factor of two times larger than previously reported terminal velocities assuming isotropic expansion, and the wind kinematic profiles establish that the radial velocity described by the momentum equation for a spherical wind structure cannot capture the complexity of the velocity field. In 15 sources, some molecular transitions other than 12CO v=0 J=2-1 reach a higher outflow velocity, with a spatial emission zone that is often greater than 30 stellar radii, but much less than the extent of CO. Binary interaction with a (sub)stellar companion might (partly) explain the non-monotonic behaviour of the projected velocity field.

The latest evolutionary phases of low- and intermediate mass stars are characterized by complex physical processes like turbulence, convection, stellar pulsations, magnetic fields, condensation of solid particles, and the formation of massive outflows that inject freshly produced heavy elements and dust particles into the interstellar medium. We use the Northern Extended Millimeter Array (NOEMA) to obtain spatially and spectrally resolved observations of the semi-regular Asymptotic Giant Branch star RS Cancri to shed light on the morpho-kinematic structure of its inner, wind forming environment by applying detailed 3-D reconstruction modeling and LTE radiative transfer calculations. We detect 32 lines of 13 molecules and isotopologs (CO, SiO, SO, SO$_2$, H$_2$O, HCN, PN), including several transitions from vibrationally excited states. HCN, H$^{13}$CN, millimeter vibrationally excited H$_2$O, SO, $^{34}$SO, SO$_2$, and PN are detected for the first time in RS Cnc. Evidence for rotation is seen in HCN, SO, SO$_2$, and SiO(v=1). From CO and SiO channel maps, we find an inner, equatorial density enhancement, and a bipolar outflow structure with a mass loss rate of $1 \times 10^{-7}M_\odot{\rm yr}^{-1}$ for the equatorial region and of $2 \times 10^{-7}M_\odot{\rm yr}^{-1}$ for the polar outflows. The $^{12}$CO/$^{13}$CO ratio is measured to be $\sim20$ on average, $24\pm2$ in the polar outflows and $19\pm3$ in the equatorial region. We do not find direct evidence of a companion that might explain this kind of kinematic structure, and explore the possibility that a magnetic field might be the cause of it. The innermost molecular gas is influenced by stellar pulsation and possibly by convective cells that leave their imprint on broad wings of certain molecular lines, such as SiO and SO., Comment: 28 pages, 40 figures, accepted for publication in Astronomy & Astrophysics

S-type asymptotic giant branch (AGB) stars are thought to be intermediates in the evolution of oxygen- to carbon-rich AGB stars. The chemical compositions of their circumstellar envelopes are also intermediate, but have not been studied in as much detail as their carbon- and oxygen-rich counterparts. We aim to determine the abundances of AlCl and AlF from rotational lines, which have been observed for the first time towards an S-type AGB star, W Aql. In combination with models based on PACS observations, we aim to update our chemical kinetics network based on these results. We analyse ALMA observations towards W Aql of AlCl in the ground and first two vibrationally excited states and AlF in the ground vibrational state. Using radiative transfer models, we determine the abundances and spatial abundance distributions of Al$^{35}$Cl, Al$^{37}$Cl, and AlF. We also model HCl and HF emission and compare these models to PACS spectra to constrain the abundances of these species. AlCl is found in clumps very close to the star, with emission confined within 0.1$^{\prime\prime}$ of the star. AlF emission is more extended, with faint emission extending 0.2$^{\prime\prime}$ to 0.6$^{\prime\prime}$ from the continuum peak. We find peak abundances, relative to H$_2$, of $1.7\times 10^{-7}$ for Al$^{35}$Cl, $7\times 10^{-8}$ for Al$^{37}$Cl and $1\times 10^{-7}$ for AlF. From the PACS spectra, we find abundances of $9.7\times 10^{-8}$ and $\leq 10^{-8}$, relative to H$_2$, for HCl and HF, respectively. The AlF abundance exceeds the solar F abundance, indicating that fluorine synthesised in the AGB star has already been dredged up to the surface of the star and ejected into the circumstellar envelope. From our analysis of chemical reactions in the wind, we conclude that AlF may participate in the dust formation process, but we cannot fully explain the rapid depletion of AlCl seen in the wind., Comment: Accepted for publication in Astronomy & Astrophysics

Binary interactions dominate the evolution of massive stars, but their role is less clear for low- and intermediate-mass stars. The evolution of a spherical wind from an asymptotic giant branch (AGB) star into a nonspherical planetary nebula (PN) could be due to binary interactions. We observed a sample of AGB stars with the Atacama Large Millimeter/submillimeter Array (ALMA) and found that their winds exhibit distinct nonspherical geometries with morphological similarities to planetary nebulae (PNe). We infer that the same physics shapes both AGB winds and PNe; additionally, the morphology and AGB mass-loss rate are correlated. These characteristics can be explained by binary interaction. We propose an evolutionary scenario for AGB morphologies that is consistent with observed phenomena in AGB stars and PNe., Comment: 19 pages main journal, 97 pages Supplementary Information

CK Vul erupted in 1670 and is considered a stellar-merger candidate. Its remnant contains a molecular component of surprisingly rich composition. We present interferometric line surveys with subarcsec resolution with ALMA and SMA. The observations provide interferometric maps of molecular line emission at frequencies between 88 and 243 GHz that allow imaging spectroscopy of more than 180 transitions of 26 species. We present, classify, and analyze the different morphologies of the emission regions displayed by the molecules. We also perform a non-LTE radiative-transfer analysis of emission of most of the observed species, deriving temperatures and column densities in five parts of the nebula. Non-LTE effects are clearly seen in complex species including methanol absorption against the CMB. The temperatures are 17 K in the inner remnant and 14 K in the extended lobes. We find total (hydrogen plus helium) densities in the range of $10^4-10^6$ cm$^{-3}$. The column densities provide relative abundance patterns in the remnant which currently are not understood. Attempts to derive elemental abundances within the assumption of a chemical equilibrium give only loose constraints on the CNO elements. That the formation of many of the observed molecules requires a major involvement of circumstellar shocks remains the preferred possibility. The molecular gas could have formed 350 yr ago or more recently. The molecules are well shielded from the interstellar radiation field by the circumstellar dust. Their presence alone indicates that the unobservable central star cannot be a hot object such as a white dwarf. This excludes some of the proposed scenarios on the nature of CK Vul. The general characteristics of the molecular environment of CK Vul derived in this study resemble quite well those of some pre-planetary nebulae and AGB stars, most notably that of OH231.8., Comment: submitted to A&A; comments welcome

The circumstellar ammonia (NH$_3$) chemistry in evolved stars is poorly understood. Previous observations and modelling showed that NH$_3$ abundance in oxygen-rich stars is several orders of magnitude above that predicted by equilibrium chemistry. In this article, we characterise the spatial distribution and excitation of NH$_3$ in the O-rich circumstellar envelopes (CSEs) of four diverse targets: IK Tau, VY CMa, OH 231.8+4.2, and IRC +10420 with multi-wavelength observations. We observed the 1.3-cm inversion line emission with the Very Large Array (VLA) and submillimetre rotational line emission with the Heterodyne Instrument for the Far-Infrared (HIFI) aboard Herschel from all four targets. For IK Tau and VY CMa, we observed the rovibrational absorption lines in the $\nu_2$ band near 10.5 $\mu$m with the Texas Echelon Cross Echelle Spectrograph (TEXES) at the NASA Infrared Telescope Facility (IRTF). We also attempted to search for the rotational transition within the $v_2=1$ state near 2 mm with the IRAM 30m Telescope towards IK Tau. Non-LTE radiative transfer modelling, including radiative pumping to the vibrational state, was carried out to derive the radial distribution of NH$_3$ in these CSEs. Our modelling shows that the NH$_3$ abundance relative to molecular hydrogen is generally of the order of $10^{-7}$, which is a few times lower than previous estimates that were made without considering radiative pumping and is at least 10 times higher than that in the C-rich CSE of IRC +10216. Incidentally, we also derived a new period of IK Tau from its $V$-band light curve. NH$_3$ is again detected in very high abundance in O-rich CSEs. Its emission mainly arises from localised spatial-kinematic structures that are probably denser than the ambient gas. Circumstellar shocks in the accelerated wind may contribute to the production of NH$_3$. (Abridged abstract), Comment: 38 pages, 28 figures, 6 tables, accepted for publication in Astronomy and Astrophysics, cross-listed to astro-ph.GA as per request by arXiv

In biomedical applications, the similarity between a signal measured from an injured subject and a reference signal measured from a normal subject can be used to quantify the injury severity. This paper proposes a generalization of the adaptive signed correlation index (ASCI) to account for specific signal features of interest and extend the trichotomization of conventional ASCI to an arbitrary number of levels. In the context of spinal cord injury assessment, a computational example is presented to illustrate the enhanced resolution of the proposed measure and its ability to offer a more refined measure of the level of injury., Comment: 2 two-column pages, 3 figures

The formation of silicate dust in oxygen-rich envelopes of evolved stars is thought to be initiated by formation of seed particles that can withstand the high temperatures close to the stellar photosphere and act as condensation cores farther away from the star. Candidate species considered as first condensates are TiO and TiO$_2$. We aim to identify and characterize the circumstellar gas-phase chemistry of titanium that leads to the formation of solid titanium compounds in the envelope of $o$ Cet, the prototypical Mira, and seek an observational verification of whether titanium oxides play a major role in the onset of dust formation in M-type AGB stars. We present high angular-resolution ALMA observations at submillimeter (submm) wavelengths supplemented by APEX and Herschel spectra of the rotational features of TiO and TiO$_2$. In addition, circumstellar features of TiO and TiI are identified in optical spectra which cover multiple pulsation cycles of $o$ Cet. The submm ALMA data reveal TiO and TiO$_2$ bearing gas within the extended atmosphere of Mira. While TiO is traceable up to a radius (FWHM/2) of 4.0 R$_{\star}$, TiO$_2$ extends as far as 5.5 R$_{\star}$ and unlike TiO appears to be anisotropically distributed. Optical spectra display variable emission of TiI and TiO from inner parts of the extended atmosphere (<3 R$_{\star}$). Chemical models which include shocks are in general agreement with the observations of gas-phase titanium-bearing molecules. It is unlikely that substantial amounts of titanium is locked up in solids because the abundance of the gaseous titanium species is very high. In particular, formation of hot titanium-rich condensates is very improbable because we find no traces of their hot precursor species in the gas phase. It therefore appears unlikely that the formation of dust in Mira, and possibly other M-type AGB stars, is initiated by titanium oxides., Comment: 19 pages plus spectral atlas of the TiO gamma' band in 1998-2014 submitted to A&A

Context: Dust is efficiently produced by cool giant stars, but the condensation of inorganic dust is poorly understood. Aims: Identify and characterize aluminum bearing species in the circumstellar gas of Mira ($o$ Ceti) in order to elucidate their role in the production of Al$_2$O$_3$ dust. Methods: Multiepoch spectral line observations at (sub-)millimeter, far-infrared, and optical wavelengths including: maps with ALMA which probe the gas distribution in the immediate vicinity of the star at ~30 mas; observations with ALMA, APEX, and Herschel in 2013-2015 for studying cycle and inter-cycle variability of the rotational lines of Al bearing molecules; optical records as far back as 1965 to examine variations in electronic transitions over time spans of days to decades; and velocity measurements and excitation analysis of the spectral features which constrain the physical parameters of the gas. Results: Three diatomic molecules AlO, AlOH, and AlH, and atomic Al I are the main observable aluminum species in Mira, although a significant fraction of aluminum might reside in other species that have not yet been identified. Strong irregular variability in the (sub-)millimeter and optical features of AlO (possibly the direct precursor of Al$_2$O$_3$) indicates substantial changes in the excitation conditions, or varying abundance that is likely related to shocks in the star. The inhomogeneous distribution of AlO might influence the spatial and temporal characteristics of dust production. Conclusions: We are unable to quantitatively trace aluminum depletion from the gas, but the rich observational material constrains time dependent chemical networks. Future improvements should include spectroscopic characterization of higher aluminum oxides, coordinated observations of dust and gas species at different variability phases, and tools to derive abundances in shock excited gas., Comment: submitted to A&A, 23 pages plus an atlas of spectral variability of Mira in Al-bearing species since 1965 (90 pages total)

The prototypical Mira variable, $o$ Cet (Mira), has been observed as a Science Verification target in the 2014 ALMA Long Baseline Campaign with a longest baseline of 15 km. ALMA clearly resolves the images of the continuum and molecular line emission/absorption at an angular resolution of ~30 mas at 220 GHz. We image the data of the $^{28}$SiO v=0, 2 $J$=5-4 and H$_2$O $\nu_2$=1 $J(K_a,K_c)$=5(5,0)-6(4,3) transitions and extract spectra from various lines-of-sight towards Mira's extended atmosphere. In the course of imaging, we encountered ambiguities in the resulting images and spectra that appear to be related to the performance of the CLEAN algorithm. We resolve Mira's millimetre continuum emission and our data are consistent with a radio photosphere with a brightness temperature of 2611$\pm$51 K, in agreement with recent results obtained with the VLA. We do not confirm the existence of a compact region (<5 mas) of enhanced brightness. We derive the gas density, kinetic temperature, molecular abundance and outflow/infall velocities in Mira's extended atmosphere by modelling the SiO and H$_2$O lines. We find that SiO-bearing gas starts to deplete beyond 4$R_\star$ and at a kinetic temperature of $\lesssim$600 K. The inner dust shells are probably composed of grain types other than pure silicates. During this observation, Mira's atmosphere generally exhibited infall motion, with a shock front of velocity $\lesssim$12 km/s outside the radio photosphere. The structures predicted by the hydrodynamical model CODEX can reproduce the observed spectra in astonishing detail; while some other models fail when confronted with the new data. Combined with radiative transfer modelling, ALMA successfully demonstrates the ability to reveal the physical conditions of the extended atmospheres and inner winds of AGB stars in unprecedented detail. (Abbreviated abstract), Comment: 55 pages, 42 figures, accepted for publication in Astronomy and Astrophysics