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41. Stabilization Effect of Interfacial Solute Segregation on θ′ Precipitates in Al-Cu Alloys.

Author

Liang, Shangshang, Wen, Shengping, Liu, Baosheng, Hu, Yong, Wei, Wu, Wu, Xiaolan, Huang, Hui, Gao, Kunyuan, Xiong, Xiangyuan, and Nie, Zuoren

Abstract

The effects of Sc, Mg and Si elements in an Al-Cu alloy have been studied by means of hardness tests and transmission electron microscopy analysis. The experimental results show that additions of Sc, Mg and Si can improve the heat resistance of the Al-Cu alloy. The Sc/Mg/Si segregation-sandwiched structure is the most stable, when compared with Sc segregation or Si/Sc co-segregation at the interface of θ′/Al. The additions of Si and Mg promote the aging–hardening response of the Al-Cu alloy. Mg is a micro-alloying element with great potential in stabilizing the size of θ′ phases, which further promotes the number density greatly. Consequently, the Al-Cu alloy achieves a high strength, matched with excellent thermal stability, due to the microalloying of Sc/Mg/Si solutes. [ABSTRACT FROM AUTHOR]

Published
2024
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42. Influence of Grain Size and Film Formation Potential on the Diffusivity of Point Defects in the Passive Film of Pure Aluminum in NaCl Solution.

Author

Hu, Xiuhua, Gao, Kunyuan, Xiong, Xiangyuan, Huang, Hui, Wu, Xiaolan, Wen, Shengping, Wei, Wu, Nie, Zuoren, and Zhou, Dejing

Subjects
POINT defects, GRAIN refinement, CORROSION potential, GRAIN size, DIFFUSION coefficients
Abstract

The influence of grain size on the corrosion behavior of pure aluminum and the defect density and diffusion coefficient of surface passive films were investigated using electron backscatter diffraction (EBSD) and electrochemical testing techniques, based on the point defect model (PDM). Samples with three different grain sizes (23 ± 11, 134 ± 52, and 462 ± 203 μm) were obtained by annealing at different temperatures and times. The polarization curves and electrochemical impedance spectroscopy results for the pure aluminum in the 3.5% NaCl solution showed that with decreasing grain size, the corrosion current (icorr) decreased monotonously, giving rise to a noble corrosion potential and a large polarization resistance. The Motte–Schottky results showed that the passive films that formed on pure aluminum with fine grains of 23 ± 11 μm had a low density (3.82 × 1020 cm−3) of point defects, such as oxygen vacancies and/or metal interstitials, and a small diffusion coefficient (1.94 × 10−17 cm2/s). The influence of grain size on corrosion resistance was discussed. This work demonstrated that grain refinement could be an effective approach to achieving high corrosion resistance of passive metals. [ABSTRACT FROM AUTHOR]

Published
2024
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48. The Influence of Precipitated Particles on the Grain Size in Cold-Rolled Al–Mn Alloy Foils upon Annealing at 100–550 °C.

Author

Wang, Jianzhu, Gao, Kunyuan, Xiong, Xiangyuan, Zhang, Yue, Ding, Yusheng, Wang, Jingtao, Wu, Xiaolan, Wen, Shengping, Huang, Hui, Wei, Wu, Rong, Li, Nie, Zuoren, and Zhou, Dejing

Subjects
RECRYSTALLIZATION (Metallurgy), CRYSTAL grain boundaries, HIGH temperatures, TRANSMISSION electron microscopy, ALLOYS, GRAIN size, IRON-manganese alloys
Abstract

The Al–Mn alloy heat exchanger fin production process includes a brazing treatment at s high temperature of 600 °C, in which coarse grains are preferred for their high resistance to deformation at elevated temperatures by decreasing the grain boundary sliding. In this study, Al-1.57Mn-1.57Zn-0.58Si-0.17Fe alloy foils cold rolled by 81.7% (1.1 mm in thickness) and 96.5% (0.21 mm in thickness) were annealed at 100–550 °C for 1 h to investigate their recrystallization behavior, grain sizes, and precipitates by increasing the annealing temperature, using micro-hardness measurement, electron back-scattered diffraction (EBSD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) techniques. The micro-hardness results showed that the recrystallization finishing temperatures for the two samples were almost the same, 323 ± 2 °C. The EBSD results showed that when the annealing temperature decreased from 550 to 400 °C, the recrystallized grain sizes of the two samples were nearly identical—both increased slightly. Further decreasing the annealing temperature from 400 to 330 °C caused the grain sizes to increase more, with the thinner foil sample having a more significant increase. The SEM and TEM observations showed that the micron-sized primary-phase remained unchanged during the annealing process. The nano-sized secondary phase precipitates formed during the hot-rolling process experienced a coarsening and dissolving process upon annealing. The particle size of the secondary phase increased from 32 nm to 44 nm and the area fraction decreased from 4.2% to 3.8%. The nucleation analysis confirmed that the large primary-phase could act as a nucleation site through particle stimulated nucleation (PSN) mode. The relatively dense secondary phase precipitates with small sizes at lower temperatures could provide higher Zener drag to the grain boundaries, leading to fewer nuclei and thereafter coarser grains. The coarsening of the recrystallized grains in the foils could be implemented through thickness reduction and/or precipitation processes to form densely distributed nano-sized precipitates. [ABSTRACT FROM AUTHOR]

Published
2024
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