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Quantitative analyses produce important information concerning the microstructural characteristics of materials, which are reflected in the main properties of the materials. The secondary and backscattered electron modes represent the two main techniques most used in scanning electron microscopy, to produce images and, consequently, realize a quantitative analysis. However, each technique has its advantages and problems. The present work proposed evaluate what is the best SEM technique to quantify secondary phases in a cladding of Inconel 686, which can be extended to the other classes of nickel based alloys rich in Mo. It was performed a quantitative analysis of several images to characterize the microstructure of Inconel 686 weld cladding. The images were obtained using three modes: secondary electron (SE), Z contrast backscattered electron (BSE) and topographic backscattered electron (BSE). The segmentation and quantify of secondary phases was performed by SVRNA software. The statistical results revealed differences between the techniques. The secondary electron mode included several artefacts that reduced the precision of the quantification study. The BSE modes are shown to be the best techniques for quantification.

Dilution is an event that has a great influence on the microstructure and, consequently, in the properties of weld claddings. The present study evaluated the effect of dilution level on the...

The friction stir weld (FSW) method was developed in 1991 by The Welding Institute (TWI) and is very useful for manufacturing components with low fusion weldability. The success of this relatively new technique is due, in part, to an appropriate combination of some parameters. In order to understand the influence of the parameters such as rotation speed, axial force, and welding velocity, simulations were carried out using the AISI 304L stainless steel. In this work, the process was considered to be a 3D non-Newtonian fluid and the heat input was calculated from the friction between the tool and the plate and from the plastic deformation. The thermal results were compared with the experimental results from the thermocouple measurements. Furthermore, the material flow was related to the formation of defects observed in the experimental welds. The results of the simulation were able to determine the temperature distribution and heat flow, as well as to predict defects in the welding. The simulated viscosity values enabled the prediction of the parameters most likely to cause the formation of flashes. In addition, the injection of inert particles into the model made it possible to predict the formation of wormholes.

Friction stir welding (FSW) is a solid-state process, where a tool that consists of a shoulder and a pin rotates between the plates to be welded by plastic deformation. This process involves several physical phenomena. To better understand this complex phenomenon, simulations have been performed for a range of maximum viscosity values. The viscosity model used in friction stir welding simulations depends on two variables, the temperature and strain rate; however, the viscosity goes toward infinity for low values of temperature and strain rates. This study analyzed two different friction stir welding simulation, by observing how the viscosity functions behave for low values of temperature and strain rates. The maximum viscosity value was shown to be restricted to values, where the velocity field tends to zero. Furthermore, when the viscosity value exceeds the maximum value, the temperature and viscosity field is significantly impaired. In the correct results, the change in viscosity is restricted to stir zone.

Dilution and microsegregation are phenomena inherent to claddings, which, in turn, directly affect their main properties. This study evaluated microsegregation in the fusion zone with different dilution levels. The overlays were welded by the TIG cold wire feed process. Dilution was calculated from the geometric characteristics of the claddings and from the conservation of mass equation using chemical composition measurements. Microsegregation was calculated using energy dispersive X-ray spectroscopy measurements of the dendrites and the chemical composition of the fusion zone. The dilution of the claddings was increased by reducing the wire feed rate. Fe showed potential to be incorporated into the solid phase (k > 1), and this increased with the increase of dilution. Mo, in turn, was segregated into the liquid phase (k

The dilution is an event that have a high influence on the microstructure and, consequently, in the properties of weld claddings. The present study evaluated the effect of dilution level on the microstructure of the fusion zone of alloy Inconel 686 weld claddings. The claddings were welded by the TIG cold wire feed process. The dilution was calculated from the geometric characteristics and based on chemical composition of the materials obtained by energy dispersive X-ray spectroscopy and optical emission spectroscopy. The microstructure of all claddings were composed by a γ-FCC matrix with some minor precipitates. These particles are called in literature as topologically closed-packed phases (TCP). These precipitates assumed several morphological aspects, being the shapeless morphology observed in more frequency in all claddings evaluated, independent of dilution level. A phase with lamellar morphology, which growth establishing an orientation relationship with the γ-FCC matrix solidification direction, was observed only in claddings with a low dilution level. In addition, a shapeless phase with a fine precipitation aggregated was observed in claddings with a high dilution level., SCOPUS: ar.j, info:eu-repo/semantics/published