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A low-carbon micro-alloyed (LCMA) steel with a body-centered cubic (bcc) crystal structure suitable for extremely low temperatures was developed by overcoming the intrinsic ductile-to-brittle transition in bcc alloys at cryogenic temperatures. The excellent cryogenic-to-ambient impact toughness in the LCMA rolled plate results from its heterogeneous microstructure, which gradually changes from bamboo-like ultrafine grains (∼ 1.1 μm) on the surface to relatively equiaxed coarse grains in the core (∼ 3.4 μm), accompanied by a distinct texture gradient variation. The heterostructured LCMA steel displays a cryogenic impact toughness of ∼200 J/cm2 at 77 K, which is 24 times higher than the coarse-grained LCMA steel. Such high impact toughness of heterostructured LCMA arises from the coordinated deformation mechanisms over different length-scales coupled with delamination toughening. At 77 K, the heterostructured steel plate deforms by forming cellular sub-structures at the core to the surface, which refines the microstructure and promotes hetero-deformation induced (HDI) hardening to improve intrinsic toughening. Moreover, the subsequent delamination process induces extrinsic toughening by shielding and blunting the cracks, with the local plane-stress conditions induced by delamination promoting ductile fracture of the coarse grains in the core regions. This low alloy steel with its heterogeneous microstructure exhibits extraordinary impact toughness at cryogenic temperatures highlights the possibility of materials design strategies for sustainable development.

Introduction: The availability of high-quality gilthead seabream (Sparus aurata) larvae in larviculture represents a major bottleneck to the aquaculture. This challenge can be compounded by losses resulting from the emergence of a clinical disorder's symptomatology. In this study, the observed syndrome included a rotated positioning of the larval sagittal plane and in most cases leading eventually to death. Methods: Herein, we examined using amplicon sequencing of the 16S rDNA the bacterial communities associated with S. aurata larvae at different conditions (including both fish with no evidence of the syndrome and fish with syndrome) during the early developmental stages along with the contribution of rearing water, organic matter and provided feed in the microbiota during an experiment of 18 days. Results: Over the development of larvae, differences were observed in the bacterial composition between healthy and symptomatic larvae as well as between components of the system. A remarkable presence of members of the Psychrobacter genus was observed in symptomatic larvaewith a significant increase at 18dph. The healthy larvae harbor different bacterial profile with a dominance of Vibrio and Bacillus genera during 3-8dph, various members of Alphaproteobacteria during 11-14dph and Marinifilum at 18dph. The rearing water showed a different bacterial profile compared to the other components, with a slight effect of healthy larvae at 3-8dph. The bacteriome of feeds provided during the rearing of larvae was found to be diverse. Chlorella was mainly dominated by members of Firmicutes, while Rotifer and Artemia were mainly dominated bymembers of Proteobacteria including different species of Psychrobacter. At 18dph, Artemia feed seems to affect the symptomatic larvae bacteriome, where it enhanced the presence of Psychrobacter spp. Discussion: Interestingly, the comparative network analysis at 18dph indicated that the bacterial associations in symptomatic larvae were primarily driven by members of the Psychrobacter genus. While various phyla contributed to bacterial associations in healthy larvae with different frequencies including mainly members of Proteobacteria, Bacteroidota and Firmicutes phyla. Finally, the Gammaproteobacteria/Alphaproteobacteria ratio was found to be related to the health condition of larvae. This study provides valuable informationwhich can be used as indicators for monitoring the health status of S. aurata larvae. [ABSTRACT FROM AUTHOR]

This work introduces two innovative rolling pair concepts to minimize slippage and reduce mass in cam-roller systems of large-scale hydraulic drivetrains: The variable contact length and the Shifting Contact Geometry concepts. Both aim to improve traction in the low contact force phase in cyclically loaded rolling contacts. The shifting contact geometry concept was validated using three custom rolling contacts: a line contact, a double elliptical contact, and a combination of both (i.e., shifting contact geometry). The tests were conducted under synchronized cyclic loading to mimic the conditions in a hydraulic drivetrain. Furthermore, a model from previous work was implemented to make predictions and compare them against the experimental results. During preliminary tests, the double elliptical contact displayed superior tractive behavior than the line contact under the same load thanks to higher contact pressures. Under synchronized cyclic loading, the line contact displayed high sensitivity to applied resisting torques at low contact forces, leading to high slide-to-roll ratios and traction force peaks. In contrast, the rolling pair with shifting contact geometry exhibited minimum slippage even under high resisting torques, resulting in substantially lower (and in most cases negligible) slide-to-roll ratio and traction force peaks. The simulations also captured this behavior, proving the validity of the model for predicting and comparing the rolling-sliding dynamics of these two different rolling pairs. This study demonstrates that rolling pairs with shifting contact geometry can not only improve the tribological performance of cam-roller contacts in large-scale hydraulic drivetrains but also yield a more favorable dynamic behavior. [ABSTRACT FROM AUTHOR]

Sunflower (Helianthus annuus L.), a vital crop for global vegetable oil production, encounters sustainability challenges in its cultivation. This study assesses the effects of incorporating a winter cover crop (CC), Avena sativa (L.), on the subsequent growth of sunflower crops and the vitality of their rhizosphere microbial communities over a two-year period. It examines the impact of two methods for suppressing winter CC--chemical suppression using glyphosate and mechanical suppression via rolling--both with and without the addition of phosphorus (P) starter fertilizer. These approaches are evaluated in comparison to the regional best management practices for sunflower cultivation, which involve a preparatory chemical fallow period and the subsequent application of starter P fertilizer. The methodology utilized Illumina sequencing for the analysis of rhizosphere bacterial 16S rRNA genes and fungal internal transcribed spacer (ITS) amplicons. Findings indicate a significant improvement (9-37%) in sunflower growth parameters (plant height, stem diameter, head diameter, and head dry weight) when cultivated after glyphosate-suppressed winter CC compared to the chemical fallows. Conversely, rolling of winter CC generally negatively affected sunflower growth. Rhizosphere bacterial communities following chemical suppression of winter CC showed greater Pielou's evenness, indicating a uniform distribution of species. In general, this treatment had more detrimental effects on beneficial sunflower rhizosphere bacteria such as Hymenobacter and Pseudarthrobacter than rolling of the winter CC, suggesting that the overall effect on sunflower growth may be mitigated by the redundancy within the bacterial community. As for fungal diversity, measured by the Chao-1 index, it increased in sunflowers planted after winter CC and receiving P fertilization, underscoring nutrient management's role in microbial community structure. Significant positive correlations between fungal diversity and sunflower growth parameters at the reproductive stage were observed (r = 0.41-0.72; p < 0.05), highlighting the role of fungal communities in plant fitness. The study underscores the positive effects of winter CC inclusion and management for enhancing sunflower cultivation while promoting beneficial microbes in the crop's rhizosphere. We advocate for strategic winter CC species selection, optimization of mechanical suppression techniques, and tailored phosphorus fertilization of sunflower to foster sustainable agriculture. [ABSTRACT FROM AUTHOR]

In this study, using an example of cold-rolled sheets, the separate effect of magnesium and zinc in an amount up to 2% upon the structure and mechanical properties of a thermally non-hardening heat-resistant alloy Al–2%Cu–1.5%Mn, the composition of which is optimized to obtain the maximum fraction of Al20Cu2Mn3 phase, is studied. It is found that in a cast state, zinc is completely contained within aluminum solid solution, and magnesium is partially included within eutectic particles of the Al2CuMg phase. These elements hardly affect the amount of Al20Cu2Mn3 phase, which is formed during deformation and heat treatment in the form of nanoscale dispersoids. It is found that addition of 1% magnesium increases the strength of cold-rolled sheets of the base alloy by 15% after 3‑hour annealing at 400 °C, without reducing the ductility. In turn, alloying with zinc does not have a significant effect on strength. [ABSTRACT FROM AUTHOR]

The aim of the work is to develop a physical and mathematical model of the process under complex asymmetric loading in conditions of single-area and two-area deformation zone during plastic processing of medium-thickness strips. The stress state in case of loss of stability during rolling of strips of medium thickness was investigated. The patterns of changes in the stress state of the strip under conditions of reach of the limiting deformation zone, as well as the effects of plastic shaping determined by a decrease in contact stresses under conditions of increasing deformation loading, are revealed. The described method is a visual approach to assessing the stress state of a plastic medium under conditions of complex interaction and asymmetric loading. [ABSTRACT FROM AUTHOR]

In this study, intermediate rolling processes, such as warm rolling (WR) before aging, hot rolling (HR) before quenching, and a combination of these processes, were used to process 7055 and 7075 alloys with solution and aging treatment. Intermediate rolling did not change the grain structure of 7055 alloy, but it refined the grain of 7075 alloy. Moreover, it led to the formation of dislocations in the alloys, thereby promoting the precipitation of η′ phases during subsequent aging. The low cooling rate resulted in the formation of η phases with large size and high-volume fraction in HR 7055 alloy. However, intermediate rolling did not seriously coarsen the precipitates of 7075 alloy due to its low Zn + Mg content, low Zn/Mg ratio, and high density of Cr-rich phases. WR before aging enhanced the strength of 7055 alloy, but other intermediate rolling processes seriously deteriorated its mechanical properties. The strength of 7075 alloy could be enhanced by all intermediate rolling processes, and the dislocation strengthening effect in 7075 alloy was more significant than its precipitation strengthening. [ABSTRACT FROM AUTHOR]

In classical experiments, it has been found that a rigid cylinder can roll both on and under an inclined rubber plane with a friction force that depends on a power law of velocity, independent of the sign of the normal force. Further, contact area increases significantly with velocity with a related power law. We try to model qualitatively these experiments with a numerical boundary element solution with a standard linear solid and we find for sufficiently large Maugis–Tabor parameter λ qualitative agreement with experiments. However, friction force increases linearly with velocity at low velocities (like in the case with no adhesive hysteresis) and then decays at large speeds. Quantitative agreement with the Persson–Brener theory of crack propagation is found for the two power law regimes, but when Maugis–Tabor parameter λ is small, the cut-off stress in Persson–Brener theory depends on all the other dimensionless parameters of the problem. [ABSTRACT FROM AUTHOR]

Acne scarring is common and can occur even with effective acne management. In addition, patients with acne scarring suffer from significant psychosocial morbidity, including depression and suicidality. Despite the availability and advancement of therapeutic modalities, treatment for acne scarring is not always optimized and often overlooked in patients with acne encounters. Using acne scarring assessment tools and identifying specific acne scar subtypes allows for a tailored therapeutic approach. Part I of this continuing medical education series covers the pathophysiology and morphology of textural and pigmented acne scars, scarring assessment tools, and medical treatment options. The principles reviewed will aid in approaching and initiating acne scar treatment in the outpatient setting. [ABSTRACT FROM AUTHOR]

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Tibiofemoral slip velocity is a key contributor to total knee arthroplasty (TKA) component wear, yet few studies have evaluated this quantity in vivo. The aim of the present study was to measure and compare tibiofemoral slip velocities in 3 TKA designs for a range of daily activities. Mobile biplane X-ray imaging was used to measure 6-degree-of-freedom tibiofemoral kinematics and the locations of articular contact in 75 patients implanted with a posterior-stabilized, cruciate-retaining, or medial-stabilized design while each patient performed level walking, step up, step down, sit-to-stand, and stand-to-sit. Using these data, tibiofemoral slip velocity was calculated for the duration of each activity for each TKA design. The pattern of tibiofemoral slip velocity was similar for all 3 TKA designs within each activity but markedly different across the 5 activities tested, with the magnitude of peak slip velocity being significantly higher in level walking (range: 158–211 mm/s) than in all other activities (range: 43–75 mm/s). The pattern of tibiofemoral slip velocity in both the medial and lateral compartments closely resembled the pattern of tibiofemoral (knee) flexion angular velocity, with a strong linear relationship observed between slip velocity and flexion angular velocity (r = 0.81–0.97). Tibiofemoral slip velocity was invariant to TKA design but was significantly affected by activity type. Our measurements of slip velocity and articular contact locations for a wide range of daily activities may be used as inputs in joint simulator testing protocols and computational models developed to estimate TKA component wear. [ABSTRACT FROM AUTHOR]

For bulk material it is very well known, that the material properties differ between the material near the surface and the inner material (i.e. segregations). However, for sheet material a gradient of material properties in depth direction and its influence on forming processes was not yet investigated. Within experiments on sheet steel 1.0338 (DC04) a gradient in material properties was proven by hardness measurements for both unprocessed material as well as after conducting forming and milling processes. The characterisation shows a gradient in material hardness over the entire sheet thickness. The experimental results regarding forming processes, such as rolling and bending, additionally show an increase of the materials hardness due to work hardening. The problem from the inhomogeneous material properties leads to an inaccurate prediction of the forming behaviour of the workpiece in further processing. Machining experiments were conducted for transferring the knowledge of modified surface and subsurface layers onto forming processes and their simulation. The bending experiments and the corresponding process simulation of the spring back behaviour show, that the implementation of an inhomogeneous material property increases the prediction accuracy. Notably the prediction of the spring back behaviour of thinner sheet metals is highly improved. Therefore, an analysis of sheet metal properties in thickness direction and their consideration in forming process simulations is inevitable for the implementation of accurate material models. [ABSTRACT FROM AUTHOR]

In an industrial context, selecting an appropriate crystal plasticity (CP) model that balances efficiency and accuracy when modelling deformation texture (DT) is crucial. This study compared DTs in IF-steel after undergoing cold rolling reductions using different CP models for two input texture scenarios. Three mean-field (MFCP) models were utilised in their most basic configurations, without considering grain fragmentation or strain hardening, in addition to a dislocation-density-based full-field (FFCP) model. The study quantitatively compared the results from the MFCP models with those from the FFCP models. Furthermore, all CP model results were compared with experimental textures obtained from electron back-scatter diffraction (EBSD) experiments. The findings revealed that certain MFCP models could predict deformation textures as accurately as the FFCP models. Notably, one of the MFCP models exhibited a superior match with experimental textures for cold rolling reductions at 60%. Upon closer examination of specific crystallographic components, it was observed that MFCP models tended to predict a stronger {111}〈211〉 component, while the full-field model favours the {111}〈011〉 component. It is crucial to emphasise the importance of quantifying the texture within individual grains when assessing the macro-level deformation texture in rolling simulations.

This work investigated the effect of rolling temperature (25–800 °C) on rolling-texture development and sheet formability of pure Ti. The rolling temperature significantly affected the development of the typical transverse-direction (TD)-split basal texture in pure Ti sheet by altering the tilting angle of (0001) basal poles. Notably, a normal-direction (ND) basal texture, where the tilting angle of (0001) basal poles was approximately 0°, developed at an intermediate rolling temperature of 400 °C. This result is remarkable because the ND basal texture is rare in pure Ti. Formation of this unusual ND basal texture was attributed to significant activation of basal slip. In contrast, a typical TD-split basal texture was dominant at the other rolling temperatures. Formation of this typical texture was attributed to pyramidal slip. After subsequent recrystallization annealing, sheet formability was examined. Despite their different textures, the sheets previously rolled at the different rolling temperatures showed similar formability. This similarity occurred because any given texture could not simultaneously provide in-plane stretching uniformity and thinning capability during sheet forming. The present study suggests an important guidance for modifying texture of pure Ti sheets to effectively increase their formability.

In this work, Mg–7Y–5Zn-0.1V alloys were prepared by 1-D forging followed by multi-step rolling. The rolling reduction dependence of the microstructure and tensile properties of the Mg–7Y–5Zn-0.1V alloy was experimentally investigated. The results indicated that the bimodal matrix microstructures are formed, and the fibrous 18R long-period stacking ordered (LPSO) phase and kinked 14H-LPSO phase are observed after 1-D forging. As the rolling deformation increased, the fibrous 18R-LPSO fractured into block and distributed more homogeneous. The lamellar 14H-LPSO fractured more severely, and it re-precipitated within the matrix when the deformation reached 50 %. The average grain size decreased gradually with increasing rolling deformation, and the minimum was 5.07 μm. After rolling, the {0001} and {0001} textures disappeared. The grain refinement of rolling alloy was mainly due to the fact that dynamic recrystallization (DRX) and substructures were generated within some grains, while the forging alloy was mainly due to DRX. The mechanisms of DRX were discontinuous DRX (DDRX) and twin-induced DRX (TDRX) after forging, and continuous DRX (CDRX) and DDRX after rolling. The strength reached its maximum when the rolling deformation amount reached 60 %, with a yield strength (YS) of 350 MPa and an ultimate tensile strength (UTS) of 385 MPa. Compared to the as-cast Mg–7Y–5Zn-0.1V alloy, its strength increased by 56 % and 63 %, respectively. The improvement of mechanical properties was mainly attributed to fine grain strengthening and dislocation strengthening.

Micro-alloyed Zn–Mg alloys have attracted extensive attention in the field of medical implant due to their excellent biosafety and moderate degradation rate. The low Mg content could compromise the improvement of strength, therefore, the appropriate rolling process was investigated to enchance strength and inhibit strain softening behavior of Zn-0.06 Mg alloy. The observed changes in microstructures, mechanical properties, and strain softening behavior of the as-cast alloy after three different rolling processing were consistent with those exhibited by the solid-solution alloy. The cold rolled alloys showed excellent strength due to their small average grain size and high initial dislocation density, however, they also exhibited noticeable strain softening behavior. Hot rolling processing can result in coarsening of the grains, reduction in dislocation density and introducing a large number of twins, which inhibited strain softening behavior but also leaded to a decrease in the strength compared with cold rolling. The hot-cold rolling processing can induce the formation of heterostructure, wherein coarse grains encircled fine grains, while high density dislocation regions and low density dislocation regions were uniformly distributed, which effectively inhibited strain softening behavior on the basis of maintaining good mechanical properties.

Every year, almost 4 million patients received medical care for knee osteoarthritis. Osteoarthritis involves progressive deterioration or degenerative changes in the cartilage, leading to inflammation and pain as the bones and ligaments are affected. To enhance treatment and surgical outcomes, various studies analyzing the biomechanics of the human skeletal system by fabricating simulated bones, particularly those reflecting the characteristics of patients with knee osteoarthritis, are underway. In this study, we fabricated replicated bones that mirror the bone characteristics of patients with knee osteoarthritis and developed a skeletal model that mimics the actual movement of the knee. To create patient-specific replicated bones, models were extracted from computerized tomography (CT) scans of knee osteoarthritis patients. Utilizing 3D printing technology, we replicated the femur and tibia, which bear the weight of the body and support movement, and manufactured cartilage capable of absorbing and dispersing the impact of knee joint loads using flexible polymers. Furthermore, to implement knee movement in the skeletal model, we developed artificial muscles based on shape memory alloys (SMAs) and used them to mimic the rolling, sliding, and spinning motions of knee flexion. The knee movement was investigated by changing the SMA spring's position, the number of coils, and the applied voltage. Additionally, we developed a knee-joint-mimicking system to analyze the movement of the femur. The proposed artificial-skeletal-model-based knee-joint-mimicking system appears to be applicable for analyzing skeletal models of knee patients and developing surgical simulation equipment for artificial joint replacement surgery. [ABSTRACT FROM AUTHOR]

Magnesium and magnesium alloy foils have great potential for application in battery anodes, electromagnetic shielding, optics and acoustics, and biology because of their excellent specific damping, internal dissipation coefficients, magnetic and electrical conductivities, as well as high theoretical specific capacity. However, magnesium alloys exhibit poor deformation ability due to their hexagonal close-packed crystal structure. Preparing magnesium and magnesium alloy foils with thicknesses of less than 0.1 mm is difficult because of surface oxidation and grain growth at high temperatures or severe anisotropy after cold rolling that leads to cracks. Numerous methods have been applied to prepare magnesium alloy foils. They include warm rolling, cold rolling, accumulative roll bonding, electric plastic rolling, and on-line heating rolling. Defects of magnesium and magnesium alloy foils during preparation, such as edge cracks and breakage, are important factors for consideration. Herein, the current status of the research on magnesium and magnesium alloy foils is summarized from the aspects of foil preparation, defect control, performance characterization, and application prospects. The advantages and disadvantages of different preparation methods and defect (edge cracks and breakage) mechanisms in the preparation of foils are identified. [ABSTRACT FROM AUTHOR]

During the sea launch of a launch vehicle in low sea state, a rolling phenomenon of the launch vehicle has been observed. In rough sea conditions, launch may failure. This study utilizes dimensionality reduction-driven spatial system projection methods and virtual prototype modeling technology to reveal that the launch vehicle's rolling is caused by differences in the motion paths of the center of mass. Additionally, during the prelaunch stage, the variation in the trajectory of the launch vehicle's center of mass caused by the rolling and pitching motions of the transportation vessel has a significant impact on the roll motion of the launch vehicle. The motion in other degrees of freedom has minimal influence on the launch vehicle's rolling. The minimum rocket rolling occurs when the dynamic coefficient of friction of the launchpad–launch vehicle contact is 0.05, and the dynamic coefficient of friction of the adapters and guideways is 0.4. The conclusions provide a theoretical foundation for optimizing the sea launch system and enhancing the reliability of sea launch in rough sea conditions. [ABSTRACT FROM AUTHOR]

The article contains experimental evaluation of technological possibilities of the wave-shaped profiles and confirmation of classical metal flow on profiles of wheel rims with toroidal flanges. The following parameters are recorded during the experiments: temperature in the finishing gauge, rolling force in the 2nd, 4th, 6th and 7th passes, current, voltages and motor speeds. The analysis of experimental data of rolling profiles 7.0-20-03, 8.5-20-03 and 228G-020-01 shows that technological capabilities of special rolled products for the truck wheel rims with wavy central part are much higher than serial profiles, where the central zone is of rectangular shape. It is possible to reduce the mass of profiles without changing the process parameters, i.e., rolling force and torque. This indicates the influence of additional and kinematic effects on the deformation zone in real production conditions. [ABSTRACT FROM AUTHOR]

This work reports the evolution of "Structure, Processing, Property Correlation of Metastable β Titanium Ti-5Al-5Mo-5V-3Cr alloy" as a function of different aging temperatures (625,725 and 775 °C) for 4 h subsequent to solution heat treatment. The hot-rolled sheet was heat treated in β phase field and then water quenched. The solution heat treated in β phase field and then water quenched samples were aged at 625, 725 and 775 °C for 4 h. The hot-rolled sample shows the presence of α and β phases. The β-solution heat treated in β phase field and then water quenched sample of the alloy exhibits single β phase. The intensities of X-ray peaks are varying and β (211) peak shows the maximum intensity. The maximum intensity can be ascribed to β (211) texture. The solution heat treated in β phase field and then water quenched sample aged at 625 °C for 4 h shows the very fine hexagonal α phase precipitates as compared to the samples aged at 725 and 775 °C for 4 h. The samples aged at 725 and 775 °C for 4 h has resulted in precipitate-free zones as a result of the rejection of Mo, V, and Cr (β stabilizing elements) during nucleation and growth of α precipitates along the β grain boundaries. The Vickers hardness values of the alloy increase from solution heat treated in β phase field and then water quenched to all aging temperatures. The sample aged at 625 °C for 4 h shows the maximum hardness which is due to the presence of fine α phase precipitates. This can be ascribed to typical precipitation hardening. [ABSTRACT FROM AUTHOR]

Ultrafine grained (UFG) material has received significant research interest due to its combination of strength and toughness when compared with its coarse-grained counterpart. In the present investigation, a distinct UFG microstructure of Al 5083 alloy fabricated through cryorolling (CR), CR followed by warm rolling (WR), and CR followed by short annealing (SA) have been subjected to salt immersion, polarization, and intergranular corrosion tests in 3.5% NaCl solution. A salt immersion test revealed that UFG structures have resistance to pitting corrosion for all conditions when compared to their coarse-grained counterpart. The presence of coarse intermetallic second phase particles leads to the formation of micro galvanic cells with matrix resulting in highly localized pitting corrosion in the solution treated (ST) material, whereas crystallographic pits along the lateral direction have been observed in deformed material. The lower values of corrosion current density (i corr = 3.640 and 3.910 μA/cm2) were observed for CR and WR conditions, respectively, than ST samples (i corr = 8.140 μA/cm2) were attributed to the presence of a higher volume fraction of low angle grain boundaries along with a high density of dislocations. SA after CR has slightly increased the corrosion current (i corr = 3.8 μA/cm2) values thereby shifting the corrosion potentials to a noble direction. [ABSTRACT FROM AUTHOR]

In the present work, 6063 Al alloy was subjected to cross cryo-rolling (XCR) at liquid nitrogen and room temperature for producing the ultrafine grained Al alloy. The XCR and cross room temperature rolling (XRTR) were performed by doing a reduction of 90%. The mechanical properties were investigated by measuring the hardness and tensile properties of investigated alloys. The increases in the average ultimate tensile strength (332 MPa), yield strength (300 MPa), and ductility (11.66%) of the XCR sample were observed as compared to the XRTR sample. The increase in the strength of the XCR sample was due to the extensive dislocation strengthening as compared to the XRTR sample. The increase in the ductility of the XCR sample was due to the softening mechanism dominated during the rolling. The microstructural properties were reported with the help of transmission electron microscopy (TEM), scanning electron microscopy and X-ray diffraction analysis and correlated with the mechanical properties. The TEM investigation revealed that XCR promotes the formation of heavily deformed sub-grains, dislocation tangles, and fragmented initial grains. The presence of dislocations inside the XRTR sample was low as compared to the XCR sample. It was observed that cross rolling at liquid nitrogen temperature further helped in the accumulation of a large number of dislocations and further improved the strength of 6063 Al alloy by suppressing the dislocations annihilations. [ABSTRACT FROM AUTHOR]

The production of homogeneous Ti–10Nb–(1–3)Mo (at %) alloys in the form of semifinished products (plates) was studied through multiple remeltings and homogenization annealing. Metallographic studies of the resulting materials in cast, rolled, and annealed states were carried out. The effect of annealing and composition on the structure, phase composition, and mechanical properties of the Ti–10Nb–(1–3)Mo alloy was revealed. Homogeneity after smelting was achieved by annealing at a temperature of 950°C for 12 h. An increase in the Mo content in the Ti–10Nb–(1–3)Mo alloy led to an increase in the strength of the alloys, while the ductility decreased. The achievement of high strength characteristics in selected alloys was associated with the development of annealing parameters after plastic deformation, namely, controlling the size of recrystallized grains and separating the α and β phases. In addition to α-Ti and β-Ti, the samples contained small amounts of ω-Ti, which led to a sharp increase in the hardness of the samples. [ABSTRACT FROM AUTHOR]

The physical and mechanical properties and structural condition of flexible graphite foils produced by processing natural graphite with nitric acid, hydrolysis, thermal expansion of graphite and subsequent rolling were studied. The processes of obtaining materials and changing their characteristics has been thoroughly described and demonstrated. The structural transformations of graphite in the manufacture of foils were studied by X-ray diffraction analysis (XRD) and transmission electron microscopy (TEM). A decrease in the average size of the coherent scattering regions (CSR) of nanocrystallites was revealed during the transition from natural graphite to thermally expanded graphite from 57.3 nm to 20.5 nm at a temperature of 900 °C. The rolling pressure ranged from 0.05 MPa to 72.5 MPa. The thickness of the flexible graphite foils varied from 0.11 mm to 0.75 mm, the density—from 0.70 to 1.75 g/cm3. It was shown that with an increase in density within these limits, the compressibility of the graphite foil decreased from 65% to 9%, the recoverability increased from 5% to 60%, and the resiliency decreased from 10% to 6%, which is explained by the structural features of nanocrystallites. The properties' anisotropy of graphite foils was studied. The tensile strength increased with increasing density from 3.0 MPa (ρ = 0.7 g/cm3) to 14.0 MPa (ρ = 1.75 g/cm3) both in the rolling direction L and across T. At the same time, the anisotropy of physical and mechanical properties increased with an increase in density along L and T to 12% with absolute values of 14.0 MPa against 12.5 MPa at a thickness of 200 μm. Expressed anisotropy was observed along L and T when studying the misorientation angles of nanocrystallites: at ρ = 0.7 g/cm3, it was from 13.4° to 14.4° (up to 5% at the same thickness); at ρ = 1.3 g/cm3—from 11.0° to 12.8° (up to 7%); at ρ = 1.75 g/cm3—from 10.9° to 12.4° (up to 11%). It was found that in graphite foils, there was an increase in the coherent scattering regions in nanocrystallites with an increase in density from 24.8 nm to 49.6 nm. The observed effect can be explained by the coagulation of nanocrystallites by enhancing the Van der Waals interaction between the surface planes of coaxial nanocrystallites, which is accompanied by an increase in microstrains. The results obtained can help discover the mechanism of deformation of porous graphite foils. The obtained results can help discover the deformation mechanism of porous graphite foils. We assume that this will help predict the material behavior under industrial operating conditions of products based flexible graphite foils. [ABSTRACT FROM AUTHOR]

The cold ‐ rolled 5059 aluminum alloy plate was annealed at different temperatures (125～275 ℃) for 1 h, and the effects of stabilizing annealing temperature on the microstructure and properties of the plate were studied. The results showed that shear bands passing through multiple fibrous grains were formed in the deformed microsturcture of the cold‐rolled plate with deformation 62. 8%. After annealing at different temperatures (150~225 ℃) for 1 h, the β phase was precipitated continuously along the shear bands, leading to the formation of corrosion grooves during intergranular corrosion processes. As the annealing temperature increased from 125 ℃ to 275 ℃, the yield strength and tensile strength of the 5059 plate decreased from 386 and 474 MPa to 301 and 407 MPa, respectively, while the elongation increased from 10. 4% to 18. 1%. The corrosion amount per unit area of 5059 aluminum alloy cold‐rolled plates increased from 13. 7 mg/cm² of 125 ℃ ×1 h annealed plate to 53. 8 mg/cm² of 200 ℃ ×1 h, and then gradually decreased to 4. 9 mg/cm² of 275 ℃×1 h annealed plate. [ABSTRACT FROM AUTHOR]

The paper analyzes the occurrence of evenly spaced cracks on the surface of lamellar specimens of Fe-28Mn-6Si-5Cr (mass %) shape-memory alloy (SMA), during cold rolling. The specimens were hot rolled and normalized and developed cold rolling cracks with an approximate spacing of about 1.3 mm and a depth that increased with the thickness-reduction degree. At normalized specimens, X-ray diffraction patterns revealed the presence of multiple crystallographic variants of brittle α′ body-bcc martensite, which could be the cause of cold-rolling cracking. Both normalized and cold-rolled specimens were analyzed using scanning electron microscopy SEM. SEM micrographs revealed the presence of several crystallographic variants of α′-body-centered cubic (bcc) and ε hexagonal close-packed (hcp) martensite plates within a γ-face-centered cubic (fcc) austenite matrix in a normalized state. High-resolution SEM, recorded after 25% thickness reduction by cold-rolling, emphasized the ductile character of the cracks by means of an array of multiple dimples. After additional 33% cold-rolling thickness reduction, the surface of crack walls became acicular, thus revealing the fragile character of failure. It has been argued that the specimens cracked in the neutral point but preserved their integrity owing to the ductile character of γ-fcc austenite matrix. [ABSTRACT FROM AUTHOR]

The two-dimensional motion of an object on a moving rough horizontal plane is investigated. Two cases are studied: the plane having a translational acceleration, and a rotating plane. For the first case, the motions of a point particle and a sphere are studied, and it is shown that the solution to the latter problem can be expressed in terms of the solution to the former one. Examples of constant acceleration and periodic acceleration along a fixed line, and specifically sinusoidal acceleration along a fixed line, are studied in more detail. Moreover, a situation is investigated where the friction is anisotropic, that is the friction coefficient depends on the direction of the velocity. In this situation, there may be stick–slip motions, and these are investigated in detail. For the second case, the motion of a point particle on a rough turntable is investigated. The large-time behavior of the system is studied in more detail. [ABSTRACT FROM AUTHOR]

Sunflower (Helianthus annuus L.), a vital crop for global vegetable oil production, encounters sustainability challenges in its cultivation. This study assesses the effects of incorporating a winter cover crop (CC), Avena sativa (L.), on the subsequent growth of sunflower crops and the vitality of their rhizosphere microbial communities over a two-year period. It examines the impact of two methods for suppressing winter CC—chemical suppression using glyphosate and mechanical suppression via rolling—both with and without the addition of phosphorus (P) starter fertilizer. These approaches are evaluated in comparison to the regional best management practices for sunflower cultivation, which involve a preparatory chemical fallow period and the subsequent application of starter P fertilizer. The methodology utilized Illumina sequencing for the analysis of rhizosphere bacterial 16S rRNA genes and fungal internal transcribed spacer (ITS) amplicons. Findings indicate a significant improvement (9–37%) in sunflower growth parameters (plant height, stem diameter, head diameter, and head dry weight) when cultivated after glyphosate-suppressed winter CC compared to the chemical fallows. Conversely, rolling of winter CC generally negatively affected sunflower growth. Rhizosphere bacterial communities following chemical suppression of winter CC showed greater Pielou’s evenness, indicating a uniform distribution of species. In general, this treatment had more detrimental effects on beneficial sunflower rhizosphere bacteria such as Hymenobacter and Pseudarthrobacter than rolling of the winter CC, suggesting that the overall effect on sunflower growth may be mitigated by the redundancy within the bacterial community. As for fungal diversity, measured by the Chao-1 index, it increased in sunflowers planted after winter CC and receiving P fertilization, underscoring nutrient management’s role in microbial community structure. Significant positive correlations between fungal diversity and sunflower growth parameters at the reproductive stage were observed (r = 0.41–0.72; p

This paper presents research on the changes in the mechanical and structural properties of the commercial aluminum alloy EN-AW 7075 during thermomechanical processing. The processing involved artificial aging of the alloy at a temperature of 150°C for 30 minutes, followed by cold rolling after aging. Changes in hardness and impact toughness during the experiment were monitored. Hardness was measured using the Leeb method, while impact toughness was measured using the Charpy method. In the annealed state, the lowest hardness values were recorded, while the highest-impact toughness value was achieved in the as-quenched state. By applying cold plastic deformation after artificial aging, the hardness of the alloy significantly increased, while the impact toughness continuously decreased. After deformation of 20%, cracks appearance prevented further deformation. Optical microscopy was used to follow microstructural changes during the applied processing regime. Precipitates of various sizes and morphologies were observed in the structure. The annealed state results in poorly defined grain boundaries and formation of large precipitates relatively evenly distributed throughout the matrix. Cold plastic deformation after aging has resulted in elongated grain structure aligned with the rolling direction, along with crushing of secondary phase particles.

The aging precipitated phases are of great significance for the strengthening and toughening of Al–Zn–Mg alloys. In this work, pre-precipitating was realized through equal channel angular pressing (ECAP) immediately followed by solid solution treatment at 475 °C for 6 h. Its corresponding strengthening and toughening effect on the room temperature (RT)-rolled Al–6Zn–1Mg alloy was systematically studied. The results indicate that pre-precipitating by ECAP can effectively improve the strength of the RT-rolled Al–6Zn–1Mg alloy and circumvent the strength-ductility trade-off. Microstructure characterization reveals that ECAP induces a large number of microshear bands, which can not only encourage recrystallization but also effectively promote the precipitation of the η′ phase. The synergistic effect of precipitation strengthening and dislocation strengthening contributes to the high strength of Al–6Zn–1Mg alloy, with UTS and YS increasing to ∼522 MPa and ∼400 MPa, respectively. Meanwhile, the ductility remains almost unchanged mainly due to the coordinated grain boundary sliding and the uniform and finely dispersed second phase particles. As a result, the strength-ductility trade-off is effectively avoided. The findings shed some light on optimizing the traditional aging treatment.

In this research, corrosion behavior and discharge capabilities of the AZ61-In alloy experiencing hot rolling process have been discussed in detail. The results reveal that the introduction of indium to magnesium facilitates the dissolution of magnesium by augmenting a quantity of secondary phases, generating less-protective products. The corrosion resistance of AZI plus 50 % rolling reduction is improved attributed to the preferred basal orientation and further recrystallization. Moreover, the average discharge potentials of AZI-50 % can respectively reach −1.551 V and −1.234 V at 10 mA cm−2 and 50 mA cm−2, showing potential for application in seawater activated batteries.

The application of biodegradable Zn-based vascular alloy stents proves to be an ideal solution for addressing cardiovascular diseases. In this work, a Zn-0.8Li-0.4Mn alloy is designed with no biological toxicity, and optimized microstructure and properties through a hot rolling process. The resulting alloy shows a combined enhancement in both mechanical strength and resistance to corrosion. Noteworthy is the effectiveness of rolling deformation in refining alloy grains, promoting the uniform distribution of precipitates, and enhancing strength and ductility. After 90 % deformation, the Zn-0.8Li-0.4Mn alloy demonstrates excellent mechanical properties, with peak yield strength and ultimate tensile strength of 406.0 MPa and 449.1 MPa, respectively, and elongation exceeding 75 %. Corrosion studies indicate a relationship between the degradation rate increase and grain refinement, with the primary corrosion mechanism being pitting corrosion. The corrosion product Li2CO3 exhibits high stability, providing a passivation effect on the alloy surface. This work establishes a theoretical foundation and practical reference for the development of new biodegradable Zn-based alloys tailored for biomedical applications.

The practical application of micro-alloying Zn–Mg alloys is limited due to their poor mechanical properties and evident strain softening behavior. Therefore, this paper proposed the utilization of ECAP plus rolling processing as an innovative approach to potentially address these limitations. Herein, effects of ECAP and rolling processing on the microstructures, mechanical properties and strain softening behavior were investigated. It was found that the grain refinement achieved through 1-pass ECAP and 8-pass ECAP processing differed significantly, and subsequent rolling processing can further regulate grain size and dislocation distribution. The 1-pass ECAP plus cold rolling (1p-CR), 1-pass ECAP plus hot-cold rolling (1p-HC), and 8-pass ECAP plus hot-cold rolling (8p-HC) processed alloys exhibited heterostructure characterized by fine grains encircling coarse grains. Additionally, regions with high density dislocations were uniformly distributed alongside regions with low density dislocations. This unique microstructure promoted the accumulation and interaction of dislocation during deformation, resulting in the inhibition of strain softening behavior while maintaining high strength and high elongation. Therefore, the 1p-CR, 1p-HC, and 8p-HC alloys demonstrated excellent formability and mechanical stability while meeting the required mechanical properties for implant materials, which highlight their significant potential for practical applications. [ABSTRACT FROM AUTHOR]

The characteristics of the relaxation and recrystallization processes in pure tantalum deformed by rolling at room temperature are studied. It is established that at 800°C the recovery processes are activated and nuclei of recrystallization grains appear. After 1000°C, an activation of primary recrystallization is observed, which, after annealing at 1200°C, involves the entire material volume. It is shown that the processes of structural relaxation beginning at 800°C are accompanied by a dramatic decrease in microhardness. [ABSTRACT FROM AUTHOR]

Despite their complex composition, high-entropy alloys (HEAs) have a simple structure and have been extensively researched for their ability to achieve unique properties through thermo-mechanical processing (TMP). This review studies the effects of different rolling regimes and post-annealing on single and multiphase HEAs, analyzing how TMP leads to microstructural changes and improved mechanical properties. The rolling changes the shape and utilizes different mechanisms determined by the rolling temperature to strengthen the raw materials, thus affecting the HEAs' properties. The microstructural evolution of HEAs during annealing is affected by various parameters such as annealing time, annealing temperature, and heating rate, which impact the strength–ductility combination of HEAs. According to the literature, cryogenic rolling (cryo-rolling), as opposed to cold rolling, provides greater strengthening. This is due to the faster microstructural evolution kinetics in cryo-rolling. Thus, cryo-rolling enhances the strengthening by activating deformation twinning at earlier stages through the intersection of twins and more shear banding, which is preferred to microbands for HEAs with low stacking fault energy (SFE). Rolling at high temperatures is the most suitable approach for HEAs with low workability. Warm and hot rolling enable microstructure evolution through deformation mechanisms, including grain growth, recovery, recrystallization, and phase transformation based on the process temperature. The ratio of recovery to recrystallization depends on temperature and SFE, with recovery dominating in alloys with high SFE and at lower rolling temperatures, while recrystallization is more prevalent for alloys with low SFE and at higher temperatures, leading to specific ductility–strength synergy. [ABSTRACT FROM AUTHOR]

This article investigated the formability of aluminum/copper bimetal sheets during single-point incremental forming. First, the two-layer sheets were produced by the explosive welding process; then, the rolling process was performed with 50% strain on two-layer samples. Considering the importance of examining the mechanical and metallurgical properties on the formability of the two-layer samples, the mechanical properties were first examined, including the uniaxial tensile and micro-hardness tests. Then, metallurgical tests were performed, including scanning electron microscopy equipped with energy-dispersive X-ray spectroscopy (SEM-EDX) to investigate the fracture surface and penetration depth and an X-ray diffraction (XRD) test to check the secondary phase particles in the penetration zone of Al and Cu in five different annealing temperature conditions. Considering that the forming limit diagram (FLD) is dependent on the strain path, to study the effect of the strain path, the two-layer samples were formed by three geometries: pyramid, cone, and straight groove. Simulations of FLD by Abaqus software 6.14-4 with four different methods were studied: FLDCRT, effective strain rate (ESR), second derivation of thinning (SDT), and maximum strain rate (MSR). The results showed that the FLDCRT criterion provided a more accurate estimate of the necking time. In the following, the values of the thickness distribution were carried out by experimental and numerical methods, and the results between the methods were in good agreement. [ABSTRACT FROM AUTHOR]

In this study, the effects of chemical composition and process routes on the microstructure and mechanical properties of high-Zn-content Al-Zn-Mg-Sc alloys were investigated. Aging led to the formation of nano-sized Zn phases in the grain interior and large Zn phases at the grain boundary (GB) or Al/Al3Sc interfaces in the Al-20Zn-0.5Mg-0.5Sc (20Zn-0.5Mg) alloy, and cold rolling before aging (Pre-CR) could accelerate this precipitation. Compared with the 20Zn-0.5Mg alloy, the Al-15Zn-1Mg-0.5Sc (15Zn-1Mg) alloy exhibited a more difficult Zn phase precipitation during aging, and only pre-CR could lead to the formation of intracrystalline Zn phases in this alloy during artificial aging. The transition of the η′ phases into η phases without coarsening of Zn phases occurred at the GB or Al/Al3Sc interfaces of the 15Zn-1Mg alloy during artificial aging. Pre-CR could improve the mechanical properties of high-Zn-content Al-Zn-Mg-Sc alloys, and the significant evolution of Zn phases in the 20Zn-0.5Mg alloy during processing in different routes conferred this alloy a wider range of mechanical properties than the 15Zn-1Mg alloy. [ABSTRACT FROM AUTHOR]

Introduction: The availability of high-quality gilthead seabream (Sparus aurata) larvae in larviculture represents a major bottleneck to the aquaculture. This challenge can be compounded by losses resulting from the emergence of a clinical disorder's symptomatology. In this study, the observed syndrome included a rotated positioning of the larval sagittal plane and in most cases leading eventually to death. Methods: Herein, we examined using amplicon sequencing of the 16S rDNA the bacterial communities associated with S. aurata larvae at different conditions (including both fish with no evidence of the syndrome and fish with syndrome) during the early developmental stages along with the contribution of rearing water, organic matter and provided feed in the microbiota during an experiment of 18 days. Results: Over the development of larvae, differences were observed in the bacterial composition between healthy and symptomatic larvae as well as between components of the system. A remarkable presence of members of the Psychrobacter genus was observed in symptomatic larvaewith a significant increase at 18dph. The healthy larvae harbor different bacterial profile with a dominance of Vibrio and Bacillus genera during 3-8dph, various members of Alphaproteobacteria during 11-14dph and Marinifilum at 18dph. The rearing water showed a different bacterial profile compared to the other components, with a slight effect of healthy larvae at 3-8dph. The bacteriome of feeds provided during the rearing of larvae was found to be diverse. Chlorella was mainly dominated by members of Firmicutes, while Rotifer and Artemia were mainly dominated bymembers of Proteobacteria including different species of Psychrobacter. At 18dph, Artemia feed seems to affect the symptomatic larvae bacteriome, where it enhanced the presence of Psychrobacter spp. Discussion: Interestingly, the comparative network analysis at 18dph indicated that the bacterial associations in symptomatic larvae were primarily driven by members of the Psychrobacter genus. While various phyla contributed to bacterial associations in healthy larvae with different frequencies including mainly members of Proteobacteria, Bacteroidota and Firmicutes phyla. Finally, the Gammaproteobacteria/Alphaproteobacteria ratio was found to be related to the health condition of larvae. This study provides valuable informationwhich can be used as indicators for monitoring the health status of S. aurata larvae. [ABSTRACT FROM AUTHOR]

This paper studies the behavior of a transverse through defect in an ingot during complex vortex flow of metal deformed by the radial shift rolling (RSR) method. The aim of the work was to investigate the applicability of the RSR method for the deformation treatment of oxide-dispersed strengthened steel (ODS-steel) ingots into a final semi- finished product. Vortex flow of metal promotes dispersion of alloying solid oxides and refinement of steel structure. However, the question of development or closure of possible casting defects of ODS-steel ingot remains open. For this purpose, an ODS-steel ingot with a through-hole modelling the defect was rolled according to the assumed process scheme. Also, to visualize the evolution of the defect in more detail during the rolling process, a simulation of the same defect development in an aluminum bar has been performed in 2 mm steps. The results of both rolls showed good correlation. Based on many cross-sections of the experimental bars, detailed 3D models of the defect evolution were built. An average reduction of 50 % in defect volume was found. Welding of the outer areas occurs immediately, but the central areas remain unclosed, stretching proportionally with the drawing of the rod during rolling. For this reason, RSR cannot be used with large cavity defects in the axial zone, but this method is guaranteed to weld surface defects even at low reductions. [ABSTRACT FROM AUTHOR]