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A fast response & recovery H2S gas sensor based on α-Fe2O3 nanoparticles with ppb level detection limit.

Authors :
Li, Zhijie
Huang, Yanwu
Zhang, Shouchao
Chen, Weimei
Kuang, Zhong
Ao, Dongyi
Liu, Wei
Fu, Yongqing
Source :
Journal of Hazardous Materials. Dec2015, Vol. 300, p167-174. 8p.
Publication Year :
2015

Abstract

H 2 S gas sensor based on α-Fe 2 O 3 nanoparticles was fabricated by post-thermal annealing of Fe 3 O 4 precursor which was synthesized using a facile hydrothermal route. The characteristic techniques including X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) were adopted to characterize the chemical composition and microstructure of the obtained samples. Gas-sensing performance of the sensor was investigated at different operation temperatures from 100 °C to 400 °C. Results showed that the sensor exhibited the best sensitivity, reproducibility and long-term stability for detecting H 2 S gas at an operating temperature of 300 °C. The detection limit towards H 2 S gas was 0.05 ppm, and the response time and recovery time was 30 s and 5 s, respectively. In addition, sensing mechanism of the sensor towards H 2 S was discussed. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
03043894
Volume :
300
Database :
Academic Search Index
Journal :
Journal of Hazardous Materials
Publication Type :
Academic Journal
Accession number :
111095992
Full Text :
https://doi.org/10.1016/j.jhazmat.2015.07.003