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Hydrothermal synthesis and characterization of novel Sn2O3 hierarchical nanostructures.
- Source :
-
Materials Letters . Feb2016, Vol. 165, p235-238. 4p. - Publication Year :
- 2016
-
Abstract
- We report the successful synthesis of novel Sn 2 O 3 with hierarchical 3D nanostructures via a facile hydrothermal method for the first time. The as-prepared Sn 2 O 3 products transform into SnO 2 after calcinations (800 °C) and a simultaneous TGA and DSC analysis of the as-prepared Sn 2 O 3 sample determines that the main increment of mass takes place in the temperature range 534–800 °C. The well-defined nanostructures are composed of thin nanosheets. The growth mechanisms are also discussed by observing the morphology revolution at various reaction times. Furthermore, the oxidation states of the Sn 2 O 3 hierarchical nanostructures are confirmed by the shape analysis of corresponding XPS O 1 s and Sn 3 d peaks using the decomposition procedure. [ABSTRACT FROM AUTHOR]
Details
- Language :
- English
- ISSN :
- 0167577X
- Volume :
- 165
- Database :
- Academic Search Index
- Journal :
- Materials Letters
- Publication Type :
- Academic Journal
- Accession number :
- 111877619
- Full Text :
- https://doi.org/10.1016/j.matlet.2015.10.142