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Identification and determination of mycotoxins and food additives in feed by HPLC-high-resolution time-of-flight mass spectrometry.
- Source :
-
Journal of Analytical Chemistry . Apr2016, Vol. 71 Issue 4, p410-417. 8p. - Publication Year :
- 2016
-
Abstract
- High-resolution time-of-flight mass spectrometry combined with high performance liquid chromatography is proposed for the detection and determination of 25 mycotoxins and 8 food additives (coccidiostats) in animal feed, using simplified and rapid sample preparation. We developed a procedure for the identification and determination of analytes by the standard addition method. The lower limit of the analytical range is 1 (400) µg/kg for mycotoxins; the analytical range for coccidiostats in feed is 10-200 mg/kg. The relative standard deviation of the results does not exceed 10%. The analysis time is 0.5-1 h. [ABSTRACT FROM AUTHOR]
Details
- Language :
- English
- ISSN :
- 10619348
- Volume :
- 71
- Issue :
- 4
- Database :
- Academic Search Index
- Journal :
- Journal of Analytical Chemistry
- Publication Type :
- Academic Journal
- Accession number :
- 114308642
- Full Text :
- https://doi.org/10.1134/S106193481604002X