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Studies toward the synthesis of linear triazole linked pseudo oligosaccharides and the use of ferrocene as analytical probe.

Authors :
Schmidt, Magnus S.
Götz, Kathrin H.
Koch, Wolfgang
Grimm, Tanja
Ringwald, Markus
Source :
Carbohydrate Research. Apr2016, Vol. 425, p28-34. 7p.
Publication Year :
2016

Abstract

Three different building blocks have been synthesised and used for the synthesis of linear triazole linked pseudo oligosaccharides with copper(I)-catalysed cycloaddition (CuAAC). Ethynylferrocene has been used as analytical probe to improve the UV/Vis properties and HPLC methods have been used and optimised for the analysis of the pseudo oligosaccharides. The smallest ones have been isolated and characterised by analytical HPLC, NMR, ESI-MS and elemental analysis. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
00086215
Volume :
425
Database :
Academic Search Index
Journal :
Carbohydrate Research
Publication Type :
Academic Journal
Accession number :
114393354
Full Text :
https://doi.org/10.1016/j.carres.2016.03.005