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A simple low-cost single-crystal NMR setup.
- Source :
-
Journal of Magnetic Resonance . Aug2016, Vol. 269, p120-127. 8p. - Publication Year :
- 2016
-
Abstract
- A low-cost single-crystal NMR kit is presented along with a web-based post-processing software. The kit consists of a piezo-crystal motor and a goniometer for the crystal, both embedded in a standard wide-bore NMR probe with a 3D printed scaffold. The NMR pulse program controls the angle setting automatically, and the post-processing software incorporates a range of orientation-angle discrepancies present in the kit and other single-crystal setups. Results with a NaNO 3 single-crystal show a high degree of reproducibility and excellent agreement with previous findings for the anisotropic quadrupolar interaction. [ABSTRACT FROM AUTHOR]
Details
- Language :
- English
- ISSN :
- 10907807
- Volume :
- 269
- Database :
- Academic Search Index
- Journal :
- Journal of Magnetic Resonance
- Publication Type :
- Academic Journal
- Accession number :
- 116927511
- Full Text :
- https://doi.org/10.1016/j.jmr.2016.06.004