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Crystal structure of (μ2-2,2′-bipyridine-3,3′-dicarboxylato)-bis(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane)-di-nickel(II) perchlorate <italic>N,N′</italic>-dimethylformamide solvate, C50H92Cl2N12Ni2O14

Authors :
Li, Huan-Yong
Lin, Wang
Han, Feng-Xian
Ou, Guang-Chuan
Source :
Zeitschrift für Kristallographie / New Crystal Structures. May2018, Vol. 233 Issue 3, p379-381. 3p.
Publication Year :
2018

Abstract

C50H92Cl2N12Ni2O14, monoclinic, &lt;italic&gt;C&lt;/italic&gt;2/&lt;italic&gt;c&lt;/italic&gt; (no. 15), &lt;italic&gt;a&lt;/italic&gt; = 25.731(5) &#197;, &lt;italic&gt;b&lt;/italic&gt; = 9.940(2) &#197;, &lt;italic&gt;c&lt;/italic&gt; = 26.574(5) &#197;, &lt;italic&gt;β&lt;/italic&gt; = 114.825(4)&#176;, &lt;italic&gt;V&lt;/italic&gt; = 6169(2) &#197;3, &lt;italic&gt;Z&lt;/italic&gt; = 4, &lt;italic&gt;R&lt;/italic&gt;gt(&lt;italic&gt;F&lt;/italic&gt;) = 0.0675, w&lt;italic&gt;R&lt;/italic&gt;ref(&lt;italic&gt;F&lt;/italic&gt;2) = 0.2209, &lt;italic&gt;T&lt;/italic&gt; = 173(2) K. [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
14337266
Volume :
233
Issue :
3
Database :
Academic Search Index
Journal :
Zeitschrift für Kristallographie / New Crystal Structures
Publication Type :
Academic Journal
Accession number :
129405550
Full Text :
https://doi.org/10.1515/ncrs-2017-0269