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Synthesis of condensed pregnano[17,16-<italic>d</italic>]triazolines under high pressure.

Authors :
Sedishev, I. P.
Zharov, A. A.
Levina, I. S.
Tyurin, A. Yu.
Volkova, Yu. A.
Aksenov, A. N.
Kachala, V. V.
Tikhonova, T. A.
Zavarzin, I. V.
Source :
Russian Chemical Bulletin. Feb2018, Vol. 67 Issue 2, p308-312. 5p.
Publication Year :
2018

Abstract

Condensed pregnano[17,16-&lt;italic&gt;d&lt;/italic&gt;]triazolines were produced in 1,3-dipolar cycloaddition of 16-dehydropregnenolone acetate with organic azides at 10 kbar. The structure of the synthesized compounds was determined by using two-dimensional NMR spectroscopy (1H—1H COSY, NOESY, HSQC, and HMBC). [ABSTRACT FROM AUTHOR]

Details

Language :
English
ISSN :
10665285
Volume :
67
Issue :
2
Database :
Academic Search Index
Journal :
Russian Chemical Bulletin
Publication Type :
Academic Journal
Accession number :
129408820
Full Text :
https://doi.org/10.1007/s11172-018-2075-x